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Material Safety Data Sheet1.Product and company identificationa)Product Name YD-171b)Recommended use of the chemical and restrictions on useGeneral Use Paints,coatings and adhesives,composite,electronic devices.Limit use No datac)Manufacturer/Supplier/Distributor InformationManufacturer KUKDO Chemical Co.,Ltd.Address345-35,Gasan dong,Gumcheon gu,Seoul,KoreaEmergency or Information Contact Tel:+82-2-3282-1560 Fax:+82-2-3282-1586Responsible department R&D Institute2.Hazards identificationa)Hazard·Risk Classification No datab)Label elements including precautionary statementsSymbol No dataSignal Word No dataHazard·Risk Statement No dataPrecautionary StatementPrevention No dataResponse No dataStorage No dataDisposal No datac)Other Hazard·Risk which are not included in the classification criteriaHealth3Fire1Reactivity0position/Information on ingredientsChemical Name Fatty acids,C18-unsatd.,dimers,oligomeric reaction products with1-chloro-2,3-epoxypropaneOther name No dataCAS number68475-94-5Content(%)100%4.First aid measuresa)Eye contact Flush eyes with plenty of water for at least15minutes while holdingeyelids open.b)Skin contact Consult a physician immediately.Immediately remove contaminated clothing or shoes,wash skin withc)Inhalation Move person to fresh air area and provide oxygen if breathing isdifficult.Provide oxygen if breathing is difficult.Consult a physician immediately.d)Ingestion Do not induce vomitingGive one glass of water unless victim is drowy,convulsing,orunconscious.e)Acute and delayed symptoms/effectsInhalationShort-term exposure irritationLong-term exposure No dataIngestionShort-term exposure No dataProlonged exposure No dataSkin contactShort-term exposure irritation,rashProlonged exposure No dataEye contactShort-term exposure irritationProlonged exposure No dataf)Indication of immediate medical attention and notes for physician In the case of ingestion,gastric lavage a cuffed endotracheal tube should be considered.5.Fire-Fighting measuresa)Suitable(and unsuitable)extinguishing mediaSuitable extinguishing media Dry chemical,carbon dioxide,foam in use,waterUnsuitable extinguishing media No dataConflagration Use foaming agent in use or water spray.b)Specific hazards arising from the chemicalCombustion product carbon oxide,aldehyde,acid,unidentified organic compounds Fire-fighting hazard May cause fire.c)Special protective equipment and precautions for fire-fighters Containers exposed to intense heat from fires should be cooled with water to prevent vapor pressure buildup which could result in container repture.6.Accidental release measuresa)Personal precautions,protective equipment and emergency proceduresNo datab)Environmental precautions and protective proceduresAir No dataSoil No dataUnderwater No datac)Methods and materials for containment and cleaning upLittle leakage Ventilate areaAbsorpt with sand or nonflammable material.Sweep spilled material into non-leaking containers.Store away from water supply and drainage Enormous leakage No data7.Handling and storagea)Precautions for safe handling No datab)Conditions for safe storage Store in a dry and cool place.Store and handle in accordance with the exgisting law and regulation.Avoid the contact with a banned material.8.Exposure controls&personal protectiona)Control parametersDomestic regulation No dataACGIH No databiological limit values No datab)Appropriate engineering controls Install a local ventilation.Check the exposure limit.c)Personal protective equipmentRespiratory protection Wear respiratory protection in the case of heavy use or overexpose.Eye protection Wear protective gogles.Hands protection Wear chemical resistant gloves.Body protection Wear chemical resistant clothing.9.Physical and chemical propertiesa)Appearancephysical state Liquidcolor Light Yellowb)Odour Irritating odourc)Odour threshold No datad)pH No datae)Meting point/freezing point No dataf)Initial boiling point and boilingNo datarangeg)Flashing point280℃h)Evaporation rate No datai)Flammability(solid,gas)No dataj)Upper/lower flammability orNo dataexplosive limitsk)Vapor pressure No datal)Solubility Negligible(in water)m)Vapor density No datan)Relative density 1.1o)Partition coefficient:No datan-octanol/waterp)Auto-ignition temperature No dataq)Decomposition temperature No datar)Viscosity400-900cps(25)℃s)Formula mass800-1,00010.Stability and reactivitya)Chemical stability Stable at normal temperature and pressure.b)Possibility of hazardousWill not occurreactionsc)Conditions to avoid Keep away from heat/sparks/open flames/hot surfaces.Avoid the contact with a banned material.d)Incompatible materials Acid,base,oxidizing agente)Hazardous decomposition products carbon oxide,aldehyde,acid,unidentified organic compounds11.Toxicological informationa)Information on the likely routes of exposureby respiratory organ No databy mouth No databy skin and contact No databy eye and contact No datab)Delayed and immediate effects as well as chronic effects from short-and long-term exposureAcute toxicOral No dataDermal No dataInhalation No dataSkin corrosive/irritant No dataSerious eye damage/eye irritation No dataRespiratory sensitization No dataSkin sensitization No dataCarcinogenicityIARC No dataNTP No dataOSHA No dataWISHA No dataACGIH No dataGerm Cell Mutagenicity No dataReproductive toxicity No dataSpecific target organ toxicityNo data(single exposure)Specific target organ toxicityNo data(repeated exposure)Aspiration hazard No datac)Numerical measures of toxicity No data12.Ecological informationa)Aquatic and terrestrial ecotoxicityfish No datacrustacea No dataaquatic plant No datab)Persistence and degradabilityPersistence No dataResolvability No datac)Bioaccumulative potentialConcentration No dataBio resolvability No datae)Other adverse effects No data13.Disposal considerationsa)Disposal method Dispose of contents/container to the regulationsb)Disposal precaution No data14.Transport informationa)UN number Not applicableb)UN proper shipping name Not applicablec)Transport hazard class Not applicabled)Packing group Not applicablee)Marin pollution Not applicablef)Special precaution which a user to be aware of or needs to comply with in connection with transport or conveyance either within or outside their premisesEmergency procedure at fire Not applicableEmergency procedure at leakage Not applicable15.Regulatory informationa)Industrial Safety and Health Act No datab)Toxic Chemical Control Actc)Dangerous Material Safety ControlNo dataActd)Wastes Management Act No datae)Other requirements in domestic and other countriesDomestic regulationLaw of Persistent Organic Pollutant Not applicableOther countriesUSA(OSHA)Not applicableUSA(CERCLA)Not applicableUSA(EPCRA302)Not applicableUSA(EPCRA304)Not applicableUSA(EPCRA313)Not applicableUSA(Rotterdam Convention material)Not applicableUSA(Stockholm Convention material)Not applicableUSA(Substance Montreal Protocol)Not applicableEU(Classification)Not applicableEU(Risk Phrases)Not applicableEU(Safety Phrases)Not applicable16.Other informationa)Information source and references No datab)Issuing date2010-06-08c)Revision number and dateRevision No.0Revision date2010-06-08。
国内外环氧树脂增韧的研究进展李永杰;安曼;田丛;姜伟【摘要】近年来环氧树脂的增韧研究已经取得了可喜的进展.本文主要通过对国内外现阶段所采取的橡胶弹性体、热塑性树脂、互穿网络聚合物、刚性纳米粒子、柔性链段固化剂、超支化聚合物、核壳聚合物等几种环氧树脂增韧方式进行了总结和比较,并展望了环氧树脂增韧方法的研究方向.【期刊名称】《信息记录材料》【年(卷),期】2016(017)005【总页数】5页(P36-40)【关键词】环氧树脂;增韧;改性;机理【作者】李永杰;安曼;田丛;姜伟【作者单位】中国乐凯集团有限公司研究院河北保定 071054;中国乐凯集团有限公司研究院河北保定 071054;中国乐凯集团有限公司研究院河北保定 071054;中国乐凯集团有限公司研究院河北保定 071054【正文语种】中文【中图分类】TP304环氧树脂是一类重要的热固性树脂，在胶黏剂、复合材料及涂料等领域得到广泛的应用。
环氧树脂经胺类和酸酐类等固化剂固化后，可具有优异的热性能和机械强度。
但是纯环氧树脂固化后形成高度交联的三维网状结构，分子链间不易滑动，导致固化后树脂质脆、抗冲击韧性差，不足以满足工程技术的要求，使用范围受到限制[1,2]。
为了确保环氧树脂的实际应用，对其进行增韧改性成为重要的研究课题。
通常可通过加入刚性材料或弹性体改善材料的能量吸收能力实现环氧树脂的增韧。
采用橡胶弹性体对环氧树脂增韧的研究开展较早，已取得了大量研究成果。
随着市场对材料性能要求的不断提升，研究者对环氧树脂的增韧研究也有了新的突破。
目前环氧树脂的增韧方式主要包括：橡胶弹性体增韧、热塑性树脂增韧、互穿网络聚合物增韧、热致液晶聚合物增韧、刚性纳米粒子增韧、柔性链段固化剂增韧、超支化聚合物增韧、核壳聚合物增韧等[3,4]。
本文主要介绍近年来环氧树脂增韧改性方法的研究进展及其增韧机理。
2.1 橡胶弹性体增韧环氧树脂橡胶弹性体增韧环氧树脂是目前较成熟的一种方法。
聚丁二烯环氧树脂
英文名称：polybutadiene epoxy resin
化学名称：聚丁二烯环氧树脂[1]、环氧化聚丁二烯树脂、D-17型环氧树脂、理化性能
分子量：800~900(低黏度)
外观：琥珀色黏稠液体
相对密度：0.9012
熔点：90~120℃
环氧值：117g/mol
溶解性：溶于甲苯、丙酮、乙醇等
化学特性：由于分子结构中除含有环氧基、羟基外，还含有不饱和键，因此不仅通常的固化剂能使其固化，而且烯类单体在过氧化物引
发下也可进行交联，固化产物热变形温度250℃。
应用
用作环氧树脂胶黏剂的稀释剂。
也用于配制环氧树脂胶黏2000#5%~30%E-51环氧树脂95%~70%、低分子聚酰胺、改性胺固化剂等可配成室温固化耐化学品及耐水胶黏剂，粘接钢板，室温/24h固化后剪切强度21MPa;100℃/1h固化后剪切强度39MPa。
80℃浸水3d和7d。
剪切强度分别为29.5MPa和31MPa。
CYD环氧树脂品种牌号岳阳环氧树脂产品说明书1.液体环氧树脂双酚a型液体环氧树脂属基础环氧树脂，杀虫剂、无色或淡黄色黏稠流体，主要用作涂料、胶粘剂、防腐、电器绝缘、层压板、浇筑等领域，也可以做为高档环氧树脂加工的原材料。
◆双酚a型液体环氧树脂序号牌号环氧当量(g/eq)可水解氯%(质量分数)≤无机氯%(质量分数)≤粘度(mpas25℃)挥发份%(质量分数)≤%色度(加德纳法)≤1cyd-128184～1940.10--11000～140000.200.52cyd-134230～2700.10--21～27--0.3013e-44210～2400.300.018012～20--0.6024e-42230～2800.300.010021～27--0.6025e-39d244～2630.070.00524～29--0.5026cyd-127180～1900.10--8000～110000.200.57cyd-128y187～1930.1--12000～150000.200.28cyd-128e184～1940.02～0.04--11000～140000.200.59cyd-128s205～2251.8～2.40--19000～240000.200.510cyd-115180～1940.10--700～1100100.511cyd-115c195～2151.70～2.00--8000～16000120.5注1：密度由供需双方商定。
备注2：e-39d凝胶时间由供需双方商定。
注3：e-44、e-42环氧树脂的钠离子含量分别为≤0.001%(质量分数)、≤0.002%(质量分数)。
2.液态环氧树脂双酚a型中、高分子量固体环氧树脂属于基础环氧树脂，低毒、无色或淡黄色，用途广泛，可用于涂料、油漆、防腐等领域。
◆双酚a型中、高分子量固体环氧树脂序号牌号熔化粘度(mpas25℃)软化点(℃)环氧当量(g/eq)可以水解氯%(质量分数)≤软化点(℃)挥发份%(质量分数)≤%色度(加德纳法)≤附注1cyd-011450～5000.1060～70d～f0.60.5中分子量2cyd-011a530～5700.1565～75g～j0.60.513cyd-012600～7000.1075～85g～k0.60.54cyd-013700～8000.1585～95l～q0.60.55cyd-014900～10000.1091～102q～v0.60.56cyd-014u710～8750.1088～96l～q0.60.57cyd-014a710～8000.1088～92l～q0.60.58cyd-014t750～8100.1092～100l～q0.60.59cyd-0171750～21000.10117～127y～z10.60.5低分子量10cyd-0192400～33000.10130～145z3～z50.60.511cyd-020n4000～60000.10135～150z5～z60.613.溶剂型环氧树脂溶剂型环氧树脂主要便利储藏和运输，也便利用户的采用，它的用途广为，可以用在淋粘剂、涂料、防腐等领域。
含柔性链段环氧树脂的合成与性能采用甲苯二异氰酸酯（TDI）与聚丙二醇（PPG）合成端异氰酸酯基聚醚（ITPs），利用ITPs与环氧树脂反应，合成了含柔性链段环氧树脂。
使用FT-IR、DSC、SEM对产物结构及改性后固化物的玻璃化转变温度（Tg）和断面形貌进行了表征，并探讨了柔性链段对提高环氧树脂固化物粘接性能和韧性的作用机理。
结果表明，ITPs可与环氧树脂链上的仲羟基反应，生成含柔性链段环氧树脂。
少量ITPs的引入可阻碍固化物中分子内氢键的产生，使粘接性能提高，同时ITPs的引入可钝化裂纹的失稳扩展，使固化物韧性提高，但拉伸强度略有降低。
标签：环氧树脂；甲苯二异氰酸酯；端异氰酸酯基聚醚；增韧改性环氧树脂固化后交联密度大，易导致其内应力大，因此其固化物存在柔韧性差的缺点[1]。
为提高环氧树脂的柔韧性，国内外学者对其做了大量的改性研究[2～5]。
其中柔性链聚合物增韧环氧树脂是将柔性链段键合至环氧树脂交联网络中，形成紧密、疏松相间的两相网络结构[6]，从而增加固化体系对应力的分散能力，在提高环氧树脂固化物柔韧性的同时简化了固化成型工艺。
目前柔性链聚合物增韧环氧树脂的报道主要是合成含柔性链段的环氧树脂固化剂来增韧环氧树脂[7]，而将柔性链直接引入环氧树脂链段间增韧环氧树脂的研究还鲜有报道。
本文利用TDI分子中2个异氰酸酯基（-NCO）反应活性存在差异的特点[8]，将聚醚柔性链段直接引入到环氧树脂链段间，使柔性链段能均匀分布于环氧树脂固化后形成的交联网络中，以期在改善环氧树脂固化物柔韧性的同时，提高其粘接性能。
1 实验部分1.1 实验原料甲苯-2，4-二异氰酸酯（TDI），分析纯，武汉江北化工厂；环氧树脂（E51），工业级，湖北奥生新材料科技有限公司，110 ℃真空脱水干燥备用；聚丙二醇（PPG2000），工业级，壳牌公司，110 ℃真空脱水干燥备用；二月桂酸二丁基锡（DBTDL），分析纯，中国医药上海化学试剂公司；固化剂（DL19）、苄基缩水甘油醚（BGE），工业级，湖北奥生新材料科技有限公司。
J—171无溶剂糊状环氧树脂结构胶粘剂
佚名
【期刊名称】《《化工科技市场》》
【年(卷),期】2002(025)009
【总页数】1页(P60)
【正文语种】中文
【中图分类】TQ433.439
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因版权原因，仅展示原文概要，查看原文内容请购买。
嘉盛德DX7160评估报告前言：DX7160是一款高柔韧性环氧树脂，具有优良的柔韧性，常温高弹性、高延伸率，优异的粘结性；可用于挠性覆铜板等行业改善材料韧性。
一、实验目的：在FCCL（挠性覆铜板）覆盖膜配方中，分别使用我司DX7160产品与日本DIC EXA-4816产品，与原配方体系进行对比实验，以评估两者在柔韧性方面的差异。
二、实验步骤：1、树脂基本性能对比IQC检验，基本数据如下表：测试项目DX7160 EXA-4816 环氧当量(g/eq) 430 403水解氯(ppm) 714 5422、覆盖膜性能对比试验2.1实验步骤①实验室配制各100g胶水，置于混合机上搅拌均匀，静置消泡待用。
配方1为现用覆盖膜配方，配方2为4816取代20%双酚A环氧，配方3为7160取代取代20%双酚A环氧。
②在聚酰亚胺薄膜上进行涂布，涂布的干胶厚度约为15μm，干燥条件为160℃/5min，固化条件为170℃/1h。
③基本性能：按IPC-4202标准测试。
2.2覆盖膜的基本性能：检验项目 测试条件 现配方 20% 4816 20% 7160 干胶厚度 （μm ）耐浸焊性300℃/5minPASS PASS PASS 15剥离强度 A0.98残胶 1.06T 1.35J 热应力(288℃/10s)0.71T 0.76T1.04T 拉PI1.07T 0.95T 1.11T 溢胶量 A 0.0641 0.0587 0.0739 线路间溢胶 A(4/4) 0.0500 0.0430 0.0420 覆型性A PASS PASS PASS 剥离强度 A1.18J 1.15J 1.30J 10热应力(288℃/10s)0.90T 1.03T 0.99T 拉PI 1.12J 1.08J 1.42J 剥离强度 A0.91J 1.04残胶 1.07J 7热应力(288℃/10s)0.70T 0.79T 0.89T 拉PI0.93J0.76T1.01J备注：表中“A ”--指常态（无前处理）。
Material Safety Data Sheet1.Product and company identificationa)Product Name YD-171b)Recommended use of the chemical and restrictions on useGeneral Use Paints,coatings and adhesives,composite,electronic devices.Limit use No datac)Manufacturer/Supplier/Distributor InformationManufacturer KUKDO Chemical Co.,Ltd.Address345-35,Gasan dong,Gumcheon gu,Seoul,KoreaEmergency or Information Contact Tel:+82-2-3282-1560 Fax:+82-2-3282-1586Responsible department R&D Institute2.Hazards identificationa)Hazard·Risk Classification No datab)Label elements including precautionary statementsSymbol No dataSignal Word No dataHazard·Risk Statement No dataPrecautionary StatementPrevention No dataResponse No dataStorage No dataDisposal No datac)Other Hazard·Risk which are not included in the classification criteriaHealth3Fire1Reactivity0position/Information on ingredientsChemical Name Fatty acids,C18-unsatd.,dimers,oligomeric reaction products with1-chloro-2,3-epoxypropaneOther name No dataCAS number68475-94-5Content(%)100%4.First aid measuresa)Eye contact Flush eyes with plenty of water for at least15minutes while holdingeyelids open.b)Skin contact Consult a physician immediately.Immediately remove contaminated clothing or shoes,wash skin withc)Inhalation Move person to fresh air area and provide oxygen if breathing isdifficult.Provide oxygen if breathing is difficult.Consult a physician immediately.d)Ingestion Do not induce vomitingGive one glass of water unless victim is drowy,convulsing,orunconscious.e)Acute and delayed symptoms/effectsInhalationShort-term exposure irritationLong-term exposure No dataIngestionShort-term exposure No dataProlonged exposure No dataSkin contactShort-term exposure irritation,rashProlonged exposure No dataEye contactShort-term exposure irritationProlonged exposure No dataf)Indication of immediate medical attention and notes for physician In the case of ingestion,gastric lavage a cuffed endotracheal tube should be considered.5.Fire-Fighting measuresa)Suitable(and unsuitable)extinguishing mediaSuitable extinguishing media Dry chemical,carbon dioxide,foam in use,waterUnsuitable extinguishing media No dataConflagration Use foaming agent in use or water spray.b)Specific hazards arising from the chemicalCombustion product carbon oxide,aldehyde,acid,unidentified organic compounds Fire-fighting hazard May cause fire.c)Special protective equipment and precautions for fire-fighters Containers exposed to intense heat from fires should be cooled with water to prevent vapor pressure buildup which could result in container repture.6.Accidental release measuresa)Personal precautions,protective equipment and emergency proceduresNo datab)Environmental precautions and protective proceduresAir No dataSoil No dataUnderwater No datac)Methods and materials for containment and cleaning upLittle leakage Ventilate areaAbsorpt with sand or nonflammable material.Sweep spilled material into non-leaking containers.Store away from water supply and drainage Enormous leakage No data7.Handling and storagea)Precautions for safe handling No datab)Conditions for safe storage Store in a dry and cool place.Store and handle in accordance with the exgisting law and regulation.Avoid the contact with a banned material.8.Exposure controls&personal protectiona)Control parametersDomestic regulation No dataACGIH No databiological limit values No datab)Appropriate engineering controls Install a local ventilation.Check the exposure limit.c)Personal protective equipmentRespiratory protection Wear respiratory protection in the case of heavy use or overexpose.Eye protection Wear protective gogles.Hands protection Wear chemical resistant gloves.Body protection Wear chemical resistant clothing.9.Physical and chemical propertiesa)Appearancephysical state Liquidcolor Light Yellowb)Odour Irritating odourc)Odour threshold No datad)pH No datae)Meting point/freezing point No dataf)Initial boiling point and boilingNo datarangeg)Flashing point280℃h)Evaporation rate No datai)Flammability(solid,gas)No dataj)Upper/lower flammability orNo dataexplosive limitsk)Vapor pressure No datal)Solubility Negligible(in water)m)Vapor density No datan)Relative density 1.1o)Partition coefficient:No datan-octanol/waterp)Auto-ignition temperature No dataq)Decomposition temperature No datar)Viscosity400-900cps(25)℃s)Formula mass800-1,00010.Stability and reactivitya)Chemical stability Stable at normal temperature and pressure.b)Possibility of hazardousWill not occurreactionsc)Conditions to avoid Keep away from heat/sparks/open flames/hot surfaces.Avoid the contact with a banned material.d)Incompatible materials Acid,base,oxidizing agente)Hazardous decomposition products carbon oxide,aldehyde,acid,unidentified organic compounds11.Toxicological informationa)Information on the likely routes of exposureby respiratory organ No databy mouth No databy skin and contact No databy eye and contact No datab)Delayed and immediate effects as well as chronic effects from short-and long-term exposureAcute toxicOral No dataDermal No dataInhalation No dataSkin corrosive/irritant No dataSerious eye damage/eye irritation No dataRespiratory sensitization No dataSkin sensitization No dataCarcinogenicityIARC No dataNTP No dataOSHA No dataWISHA No dataACGIH No dataGerm Cell Mutagenicity No dataReproductive toxicity No dataSpecific target organ toxicityNo data(single exposure)Specific target organ toxicityNo data(repeated exposure)Aspiration hazard No datac)Numerical measures of toxicity No data12.Ecological informationa)Aquatic and terrestrial ecotoxicityfish No datacrustacea No dataaquatic plant No datab)Persistence and degradabilityPersistence No dataResolvability No datac)Bioaccumulative potentialConcentration No dataBio resolvability No datae)Other adverse effects No data13.Disposal considerationsa)Disposal method Dispose of contents/container to the regulationsb)Disposal precaution No data14.Transport informationa)UN number Not applicableb)UN proper shipping name Not applicablec)Transport hazard class Not applicabled)Packing group Not applicablee)Marin pollution Not applicablef)Special precaution which a user to be aware of or needs to comply with in connection with transport or conveyance either within or outside their premisesEmergency procedure at fire Not applicableEmergency procedure at leakage Not applicable15.Regulatory informationa)Industrial Safety and Health Act No datab)Toxic Chemical Control Actc)Dangerous Material Safety ControlNo dataActd)Wastes Management Act No datae)Other requirements in domestic and other countriesDomestic regulationLaw of Persistent Organic Pollutant Not applicableOther countriesUSA(OSHA)Not applicableUSA(CERCLA)Not applicableUSA(EPCRA302)Not applicableUSA(EPCRA304)Not applicableUSA(EPCRA313)Not applicableUSA(Rotterdam Convention material)Not applicableUSA(Stockholm Convention material)Not applicableUSA(Substance Montreal Protocol)Not applicableEU(Classification)Not applicableEU(Risk Phrases)Not applicableEU(Safety Phrases)Not applicable16.Other informationa)Information source and references No datab)Issuing date2010-06-08c)Revision number and dateRevision No.0Revision date2010-06-08。
