Prinaberel_HNMR_15857_MedChemExpress

p

p

m (t1)0.0

2.5

5.0

7.5

8.5288.5238.3878.3838.3747.8487.8287.3927.3797.3727.3606.0885.4015.3894.8703.4083.3062.2632.2562.0752.0711.8971.7871.7011.6161.6001.4941.091

1.0000.9761.0041.0021.0081.0271.0993.1173.1203.1396.2338.284Date:20 Oct 2014

Document's Title:

&DWDORJ󰀇1R󰀊󰀇+<󰀍󰀎󰀏󰀏󰀐󰀑󰀇%DWFK󰀔󰀐󰀑󰀖󰀗󰀑

Spectrum Title:

wxz2228-25-2-meod-141017

Frequency (MHz):

(f1) 400.132

Original Points Count:

(f1) 32768

Actual Points Count:

(f1) 32768

Acquisition Time (sec):

(f1) 3.2768

Spectral Width (ppm):

(f1) 24.992

Pulse Program:

Unknown

6DPSOH󰀃,'󰀝:;=󰀕󰀕󰀕󰀛󰀐󰀕󰀘󰀐󰀕󰀏+0󰀐󰀓󰀕󰀚󱤟󰀔󰀗󰀐󰀕󰀓󰀔󰀗󰀔󰀓󰀔󰀚󰀏&'󰀖2'

N

HOHHH

Sample ID:WXZ2228-25-2,Catalog No: HY-70013 Batch#13453,CD3OD

File ..ta\20171204\20171204-2 2\BIZ2017-D04-WYQ5.D Tgt Mass (CHM): Injection Date : 4 Dec 17 6:36 pm +0800 Seq. Line : 45 Sample Name : BIZ2017-D04-WYQ5 Location : P2-B-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\LCMS03\Data\20171204\20171204-2 2\1-POS-3MIN.M Analysis Method : D:\LCMS03\Data\20171204\20171204-2 2\1-POS-3MIN.M Catalog No : HY-12874 Batch#27609 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min00.511.522.5mAU010002000 DAD1 A, Sig=214,4 Ref=off1.4421.6461.7071.7961.967

min00.511.522.5mAU0500 DAD1 B, Sig=254,4 Ref=off1.1571.4421.5621.6611.6941.7321.7741.8501.9101.9922.087

min00.511.522.5mV50 ELS1 A, ELSD Signal1.513

Inhibitors, Agonists, Screening

Safety Data SheetRevision Date:Jul.-03-2017Print Date:Jul.-03-2017

1. PRODUCT AND COMPANY IDENTIFICATION1.1 Product identifierProduct name :Dronedarone

Catalog No. :HY-A0016

CAS No. :141626-36-01.2 Relevant identified uses of the substance or mixture and uses advised againstIdentified uses :Laboratory chemicals, manufacture of substances.1.3 Details of the supplier of the safety data sheetCompany:MedChemExpress USA

Tel:609-228-6898

Fax:609-228-5909

E-mail:sales@1.4 Emergency telephone numberEmergency Phone #:609-228-6898

2. HAZARDS IDENTIFICATION2.1 Classification of the substance or mixtureNot a hazardous substance or mixture.2.2 GHS Label elements, including precautionary statementsNot a hazardous substance or mixture.2.3 Other hazardsNone.

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C20H22N2OMolecular Weight:306.40Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:Grayish brown to reddish brown (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):98.64%Conclusion:The product has been tested and complies with the given specifications.Product Name:CASINCat. No.:HY-12874CAS No.:425399-05-9Batch No.:27609Chemical Name:Ethanol, 2-[(2,3,4,9-tetrahydro-6-phenyl-1H-carbazol-1-yl)amino]-

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,