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（一）开机步骤1.到402开卡同时登记开机时间2.检查氦气瓶气量是否充足，总压需＞2MPa，分压在0.4~0.6MP。
如需使用双MS则要开氮气，氮气分压需＞0.5MPa。
若气体不足，则需更换气瓶。
更换气瓶时需注意关闭总压阀与分压阀：待气瓶换好后，用检漏液检查阀门连接处是否有漏气。
3.进入重点实验室后先查看实验室卫生状况，若室内不干净必须先打扫卫生后再开启仪器。
同时确认实验室内是否有安全隐患，如是否有特殊气味、挥发性药品气味。
4.开机之前先检查泵油颜色是否清亮、油量是否在最高与最低限值内、托盘内是否有油泄露。
泵油3-6个月换一次，但也根据实际使用情况确定是否需要换泵油。
泵下不能垫纸以防运行时泵温度过高引起燃烧。
5.打开UPS电源，这时旁路电源指示灯闪烁，长按开关至逆路电源指示灯亮后打开GC/MSTriple Quad和GC System设备的开关。
如果长时间未开机，按下GC/MS Triple Quad设备开关后拧紧放空阀，用手向右侧推前段真空腔的侧板直至侧面板被紧固地吸牢（约1-2min），涡轮泵开始工作，屏幕显示启动后松开。
（后段真空腔的侧板螺丝一般是拧上的，所以抽真空时不用推紧）。
6.待系统稳定后，点击电脑桌面图标“GC-QQQ”，弹出对话框点击进入“调谐”→“手动调谐”→“真空控制”→“抽真空”。
抽真空10min左右如果涡轮泵转速需达到100%、功率达到45.5，高真空达到7.9×10E-5，低真空达到1.9×10E2，否则说明有漏气，检查侧板是否压正、柱子是否拧紧。
若离子源真空箱未打开过抽真空时间一般为40min，若打开过，则需4h。
7.开机后先检漏气象气象一般漏气点及处理方法：（1）进样口隔垫检查进样口漏气的方法是在进样口不分流的情况下，在GC键盘上按两下预运行，查看进样口总流量，如果大于5ml/min，则说明进样口漏气，需更换隔垫。
一般自动进样情况下进样100针后更换隔垫。
安捷伦GCMS1、Agilent 5975C GCMSAgilent 5975C 系列GC/MSD构建在行业领先、高可靠性和高性能的色谱分析技术坚实的基础之上，配置三轴HED—EM检测器,大大增强了产品性能，因此显著地提高了分析性能,将您的实验室的GC分析效率推向新的高度。
高温整体惰性离子源提升仪器的性能专利的惰性离子源满足三个基本要求。
化学惰性将活性组分和中性化合物的损失降至最低。
高温(350 ˚C）有助于高沸点组分的峰形改善,最大程度地降低了由于高沸点组分导致的离子源的污染。
延伸至四极杆内的新颖设计的透镜，将优化的传输离子聚焦到RF/DC场中，得到业内最佳的信噪比。
顶级标准的四极杆设计和性能独特的四极杆具有无与伦比的性能和可靠性.真正双曲面石英结构的场误差最低, 分辨率更高和在任何工作温度下都具有优异的质量轴稳定.事实上,这个非凡的整体稳定性的石英镀金四极杆允许200˚的温度，从而保证质量分析器在整个生命周期都保持干净状态.三轴检测器三轴检测器将从四极杆传输过来的离子束在进入到电子倍增器之前转两次弯.这个创新的的设计使得离子的捕集效率提高(信号增强）而中性信号被过滤。
检测器采用新型的三通道倍增器，其放大倍数和寿命都有显著的提升.安捷伦新型的电子倍增器归一化调谐优化功能保证了离子数、线性和电子倍增器寿命三者之间达到了最优的平衡。
而且归一化调谐使得在倍增器老化之后还能得到一致的灵敏度以及有利于不同气质之间的结果比对。
微量离子检测和第二代的解卷积报告软件(DRS）对于复杂样品的痕量组分的分析达到了新的水平.微量离子检测（TID）从基线，峰和谱图中过滤掉噪音以提高检测灵敏度，它可以配或不配解卷积报告软件（DRS).对于复杂样品分析中常见的共流出问题，NIST AMDIS的解卷积计算是气质分析复杂样品中痕量组分的终极工具.在解卷积处理之后，“干净"的谱图可以提供更准确的谱库检索结果,基于解卷积分析的定量分析结果降低了目标离子定量分析结果的误差。
The PerkinElmer ®Clarus ®560 D Gas Chromatograph/Mass Spectrometer (GC/MS) combines the dependable diffusion-pump and electron ionization (EI) capabilities of the high-performance Clarus 600 D MS with the robust Clarus 500 GC,enabling laboratories to conduct reliable and cost-effective routine analyses.It offers state-of-the-art electronics for the fastest scanning rates and widest mass range, coupled with the most robust,flexible GC autosampler, intuitive touch-screen interface and two GC detector channels, while maintaining a compact foot-print for minimal bench space.With the Clarus 560 D GC/MS, PerkinElmer delivers on your expectations through outstanding dependability, precision,performance and cost for everyday GC/MS applications.Advanced technology and ease-of-use mean you’ll maximize your uptime.Clarus 560 D Gas Chromatograph/Mass Spectrometer – dependable results, again and againO T EG A S C H RO M ATO G R A P H Y / M A S S S P E C T RO M E T RYState-of-the-art electronics provide the fastest scanning rates and increased productivity Easy-maintenance design, utilizing tools such as a plug-and-play ion sourceThe latest in TurboMass™ GC/MS software, including over 70 reporttemplates and customizable reporting Reliable GC with the most robust,flexible autosampler, a variety of injector/detector options, plus an intuitive touch-screen interface Compact footprint maximizes laboratory bench spaceK e y B e n e f i t sRugged design for maximum uptime The Clarus 560 D GC/MS is built tough to deliver reliability, reduced costs and easy maintenance. Our exclusive gold-component technology enhances overall instrument stability and significantly reduces downtime by minimizing contamination.Design logic saves maintenance timeThe logical design of the Clarus 560 D GC/MS means that you save time on routine maintenance tasks.•Quick source changeover reduces the risk of contami-nating the quadrupole analyzer: you have easy access to the ion source from the front of the instrument without exposing the ion optics or vacuum manifold.•Routine cleaning of electron ionization (EI) inner source: no wire connections needed.•Filament replacement is quick and easy due to the robust filament system’s self-aligning design, which also means consistent performance, analysis after analysis.•Cleanable RF-only prefilters are easy to maintain:located in front of the quadrupole analyzer.•Intelligent diffusion-pump electronics and hardware for maximum uptime and dependable operation. Design controls maximize system safeguards Built-in controls in the Clarus 560 D GC/MS reduce breakdowns and lower operating and repair costs.•Sealed, long-life photomultiplier detector lowers operat-ing costs: eliminates expensive and contamination-prone electron multipliers that need periodic replacement.•Unique programmable pneumatic control (PPC) safe-guards the system from column damage and ion-source contamination: automatically turns off the GC oven and transfer-line heating should carrier-gas pressure drop.•Independent control of the instrument ion source and transfer-line temperatures maximizes spectral quality:reduces contamination and protects thermally labile compounds from uncontrolled fragmentation. The temperatures can be set up to 350 ˚C.•Power outages will not damage the system: the Clarus 560 D GC/MS can be attached to a nitrogen purge which prohibits oxygen from entering the system during venting. This minimizes contamination and speeds pump-down.Updated diffusion-pump vacuum technology provides reliable operationThe Clarus 600 D GC/MS offers the latest in fail-safe diffusion-pump design with a reliable vacuum inside the mass analyzer chamber. This, combined with new software programming, provides enhanced dependability.•The air-cooled oil diffusion pump is combined with a powerful mechanical backing pump to achieve optimal GC/MS vacuum conditions.•Updated diffusion-pump system design uses tools such as innovative baffles and valves to ensure system integrity and maximize system uptime.•Controlled by unique software to provide seamless pump-down and venting of the mass analyzer; intelli-gent software uses fail-safe features to allow system venting only when the pump is cooled and ready,preventing potential damage to the analyzer from improper manual venting.Innovative tools boost laboratory efficiency The Clarus 560 D GC/MS features innovative and unique productivity-enhancing tools that help laboratories operate effectively and efficiently.Fast scanning for the most accurate and precise data everThe Clarus 560 D GC/MS acquires more spectra (up to 65 scans/second) across a GC peak than most GC/MS systems. Up to 100 scans/second is achieved for SelectedFigure 1.Clarus 560 D mass analyzer.Figure 2.Diffusion-pump venting sequence.Ion Monitoring (SIM). The result is the most accurate and precise data ever, easily beating the generally accepted criteria of at least 7-10 data points per chroma-tographic peak, for performance unmatched by any other competitive quadrupole GC/MS system.Improve productivity and sensitivity with SIFI scanningWith a powerful process called Selected Ion and Full Ion (SIFI ™) scanning, SIM data is collected while simultaneously acquiring data in the full-scan mode.First implemented by PerkinElmer in 1998, SIFI pro-vides significant laboratory benefits. Because only a single injection is required, laboratories will incur savings in productivity and sample preparation. Additionally, it provides laboratories the ability to detect and quantify compounds difficult to determine at low levels with greater accuracy and sensitivity, and finally the ability to reach SIM detection limits and full-scan library searching in a single run.Gain flexibility and automation capability with the integrated autosamplerThe integrated Clarus GC autosampler provides a mech-anically robust, dependable system with the flexibility and automation capability you need. It provides complete application flexibility, accommodating three syringe sizes (0.5, 5.0 and 50 µL) and three injection speeds (slow, normal and fast). Its smart design assures efficient utilization of the gas chromatograph, providing unob-structed access to either injection port, allowing any combination of analyses. It offers built-in quality assur-ance, as optical sensors consistently monitor system performance. The GC touch screen delivers smooth navi-gation: with multilingual capability, including error messages, so you can work in the language of your choice.TurboMass software drives routine or research-intensive analyses Data acquisitionTurboMass ™GC/MS software makes it easy to acquire data for either qualitative or quantitative sample analysis.•Sample-centric software is intuitive to learn and use.•Methods are easy to set up and store for the routine user.•Project-based organization collects all the necessary method information and data in one location, facilitating archiving.•Data collection uses a simple checklist. Just check off the desired steps and press the “OK” button to initiate data collection and reporting.•Use the AutoBuild feature to speed development of quantitative methods. Just a few clicks and the necessary information are transferred from the chro-matogram, spectrum and library search results to the method.Chromatogram and spectrum viewers for easy data screening during and after acquisition Screening data using the powerful chromatogram and spectrum viewers is a simple and easy process.Chromatograms and spectra can be displayed at any point during or after acquisition, saving you valuable time during post-run processing. Chromatograms from up to 16 different acquisitions (including the one cur-rently being acquired, with real-time updating) can be displayed simultaneously with a single drag-and-click ofFigure 4.SIFI scanning ensures accurate identification, while simulta-neously providing enhanced quantifiable sensitivity from the selected ion signal.Figure 3.Chromatographic signal at fast scan speed (red) compared to slow scan speed (green).the mouse. This enables quick comparison to reference chromatograms. Single mouse clicks allow selection of extracted mass ions, chromatogram overlays, peak in-tegration and more. Spectrum-peak averaging and back-ground subtraction of unwanted ions are flexible and easy, as is verification of spectrum quality to environmental method criteria. Similarly, the spectrum viewer allows for spectral comparison of up to 14 spectra from the same or different chromatograms using single mouse clicks at any time during acquisition or post run. Mass-spectral library search is just a single mouse click away.Efficient, effective post-run data review ensures correct peak selection and complianceData review is an important preliminary step in any quantitative application, to ensure that only correctly integrated and identified peaks are used in quantitation and further evaluation. The interactive data-review environment speeds this step of the process.Automated tuning optimizes mass spec performanceTuning the mass spectrometer is critical to ensure that good library-searchable spectra are generated from analyses. TurboMass software automatically tunes the mass spectrometer using a new-generation proprietary tune (UltraTune®), providing enhanced stability and reproducibility.GC detector support adds flexibilityYou can use two additional GC detectors simultaneously with your Clarus GC/MS system. All acquisition, display and quantitation can be performed by TurboMass software. You also have the option of using our TotalChrom®Chro-matography Data Systems (CDS) workstation or client/ server software for these processes.Environmental data evaluation and reporting package speeds quality resultsTurboMass software is especially designed to meetthe strict quality-assurance (QA) and quality-control (QC) compliance requirements of environmentaland other types of laboratories. Maximize yourlab’s productivity with the superior data review, evaluation and report-generating capabilities of TurboMass software, while ensuring complete compliance with required methodologies.Fast, simple and flexible reporting completesthe processMost labs must present their data in an attractive, stan-dardized format for reporting to internal or external clients. TurboMass software includes over 70 standard templates, allowing report generation with just a few clicks. Report templates are designed to meet the specific needs of labs conducting environmental, forensic, clinical or toxicological diagnostics, as well as general chemical analysis. Examples of reports are included to make the choice simple.TurboMass software is LIMS-compatible for simple data transfer of worklists from LIMS and GC/MS back to your LIMS: standard report templates for data transfer are provided to smooth the path to your LIMS, either before or after method QC evaluation.Figure 5.TIC (total ion chromatogram), extracted ions (121 and 106), and TIC integration.Figure 6.Interactive data review.Clarus 560 D MS SpecificationsHardwareMass range 1.0-1200 u (amu)Detector Sealed long-life photomultiplierAnalyzer Quadrupole with prefilter: 131 mm x 12 mm circular rods; 16 mm x 12 mm prefilter rodsMass stability±0.1 m/z mass accuracy over 48 hoursEI voltage10-100 eVPump Air-cooled oil diffusionVacuum gauge Standard, single wide-range gauge for all pumping optionsGC transfer line Settable from 50 ˚C to 350 ˚CSource Temperature settable from 50 ˚C to 350 ˚C; No wires – plug and playCalibrant gas PFTBA (FC-43), Tris(perfluoroheptyl)-s-triazine for high mass calibration (optional),or user selectableMSVent Optional accessory for MS isolationPerformanceScan rate Fully variable up to 12,500 amu/secMaximum Up to 65 scans/second full scan, depending on mass rangeAcquisition rate Up to 100 samples/second, selected ion monitoring (SIM)Linear dynamic range Electronic: 106-107depending on acquisition rateScan functions/run32 sets (full scan/SIM) of up to 32 ions per functionData systemMethods Electronically transferable between Clarus 600, Clarus 560, Clarus 500, TurboMass Gold and TurboMass GC/MS systemsAcquisition MS detector with two GC detectors (optional)SIFI Simultaneous full-scan data acquisition with selected ion monitoring (SIM)UltraTune autotune User selectable: standard (BFB/DFTPP) or custom tuningReporting Environmental: standard – Forensic: standard – Customizable: standardSensitivityTest Amount Detection Limits (S/N)EI full scan 1 pg of octafluoronaphthalene100:1 RMSOptional libraries and softwareLibraries NIST Mass Spectral LibraryWiley Mass Spectral LibraryPfleger/Maurer/Weber Drugs, Pollutants, Pesticides and Metabolites LibrarySoftware Ion Signature Deconvolution MS softwarePhysicalPower120 VAC ±10% @ 50/60 Hz ±1% 1000 VA; 230 VAC ±10% @ 50/60 Hz ±1% 1000 VAOperating 10 ˚C to 30 ˚CtemperatureRelative humidity 20-80%, non-condensingWeight Clarus 560 D GC/MS: 46.3 kg (102 lb); Forepump: 25.9 kg (57 lb)Dimensions (HxWxD) 51 x 33 x 74 cm (20 x 13 x 29 in)With Clarus 500 GC and Autosampler: 79 x 99 x 74 cm (31 x 39 x 29 in)Create an integrated analytical solutionCombine the Clarus 560 D GC/MS with our market-leading TurboMatrix™Headspace or Thermal Desorption sample handling, flexible user-friendly software and world-class service and support for an integrated, complete analytical solution.PerkinElmer – the clear choice in gas chromatographyPerkinElmer is the only chromatography supplier who develops, manufactures, supports and services every product it offers to provide a truly integrated system. This means one expert supplier – with best-in-class instruments and a world-class service and support organization – can address all of your applications and troubleshooting needs, from sample handling to data handling.PerkinElmer, Inc.940 Winter StreetWaltham, MA 02451 USAPhone: (800) 762-4000 or(+1) 203-925-4602For a complete listing of our global offices, visit /lasoffices©2007 PerkinElmer, Inc. All rights reserved. The PerkinElmer logo and design are registered trademarks of PerkinElmer, Inc. SIFI, TurboMass and TurboMatrix are trademarks and PerkinElmer, Clarus, UltraTune and TotalChrom are registered trademarks of PerkinElmer, Inc. or its subsidiaries, in the United States and other countries. All other trademarks not owned by PerkinElmer, Inc. or its subsidiaries that are depicted herein are the property of their respective owners. PerkinElmer reserves the right to change this document at any time without notice and disclaims liability for editorial, pictorial or typographical errors.。
分析与检测T logy科技使用Agilent MP-AES分析食品中的金属元素□ 安捷伦科技（中国）有限公司 供稿分析食品中的金属元素对于其中高浓度的营养元素以及痕量有毒元素而言都非常重要。
此类分析对于确保产品质量和安全，以及确定产品的来源极为重要。
重金属污染导致的食品安全危机不仅对人类健康构成威胁，还会打击消费者的信心，从而导致商家销量下降，信誉受损。
FAAS（火焰原子吸收光谱）是食品分析领域中一项行之有效的技术。
但随着实验室面临的预算压力日益增大，当今实验室更倾向于采用低成本高性能、易于使用且安全的仪器。
Agilent 4200 MP-AES是第二代微波等离子体原子发射光谱，具有改良的波导设计，能够分析含高总溶解态固体的样品，并且对检测限毫无影响。
4200 MP-AES使用氮气作为等离子体气体，显著降低了运行成本。
没有易燃性气体也增加了安全性，即可实现仪器在无人值守条件下运行。
与标准FAAS相比，4200 MP-AES易于使用且可获得更低的检出限。
它还可以测定磷之类的其他元素。
本文对使用4200 MP-AES分析食品中金属元素的研究进行了介绍。
米粉中的常量、少量和痕量金属元素大米是我们最重要的谷物之一。
世界上的大多数人口依靠大米提供日常所需的营养和卡路里，所以，任何因重金属（如镉）导致的环境污染威胁都会受到特别的关注。
本示例中，使用了经认证的参比标样——含有高浓度镉的糙米粉。
4200 M P-A ES拥有连续的波长范围，允许根据预期浓度范围选择合适、不受光谱干扰的波长。
样品引入系统由双通道玻璃旋流雾化室和Agile nt O n e N e b雾化器组成。
表1所示测量值（两台不同的4200M P-A E S仪器平行测定两次的平均值）与标准值十分吻合。
结果表明，在溶解态固体含量为2%的样品中，在较宽的浓度范围内4200 M P-AES能够表现出优异的性能。
果汁中的常量金属元素钙、镁、钠和钾等常量元素是食品中的基本营养元素，对果汁中的这些元素进行常规监测是一种常用的质量控制手段，图1显示了使用Agilent 4200MP-AES分析经认证的米粉参比标样。
Innovative, economical mixing and dilution system generates precise gas blends for analytical applications.Gas Blending SystemBlending for Process ApplicationsUsed to create customized gaseous mixtures for analytical applications, Parker’s Gas Blending System draws from five separate pure gas sources to generate a controlled blend across a broad concentration range.Automatic or manual dynamic mixing allows the creation of multiple gasconcentrations in real time, minimizing inventory of multi-component custom gas cylinders. The use of modular sampling components provides asophisticated, yet standardized mixing platform for specialty blend and inert gases. High precision gas blending provides an efficient and cost-effective approach for calibration and validation of analytical systems. One Parkerblending system can replace expensive INNOVATIVE GAS BLENDING SYSTEM SAVES 20%OVER THE PURCHASE OF PRE-BLENDED GAS• Gas chromatography• Fourier Transform Infrared (FTIR)• Mass Spectroscopy (MS)• Process instrumentation (GC, O 2, H 2, CO 2, moisture, CEMS, etc.) • Automotive (welding and laser processes)Only from Parker Instrumentation Products Division (IPD): An innovative, multi-function system that allows users to blend – or dilute – as many as five component gases to produce customized gas mixtures, saving significantly over the cost of custom pre-blended gas.Parker’s Gas Blending System consists of a single chassis supporting up to five (5) gas streams controlled either manually (Parker IPD Volumetric Flow Controllers) or electronically (Mass Flow Controllers). The system also includes a check valve to prevent back flow, a pressure gauge, and pressure regulators to provide pressure stability.FEATURES• Multiple stream integration• Volumetric and mass flowcontroller options• Compact size• Manual or remote operation• Interfacing with analytical equipment simplifiedBENEFITS• Ability to provide a range of gas concentrations • Variable flow control• Fits in small areas when space is an issue• Flexibility in operational architecture• Analytical hardware may be mounted to the blending system or located remotelyActual costs and potential savings will varywith location, gases used, and gas supplier.Dilution, Calibration in LaboratoriesParker IPD’s Gas Blending System can also be used for gas dilution, varying the concentration of both pure gases and pre-blended gases. A broad range of dilution ratios (1:1 – 10,000:1 standard) allowscalibration of most analyzer ranges from one cylinder of each gas type, minimizing gas costs, transport costs, and handling labor.From higher percent to parts per billion (ppb) levels, our Gas Blending System can achieve a variable range of concentrations to exact gas standards for quick multi-point, multi-scale automatic calibrations.TOTAL MODULARITYParker’s Gas Blending System is built on a Parker IntraFlow™ platform, an ISA/ANSI SP76.00.02 compliant modular sample conditioning solution that minimizes space requirements and lowers maintenance costs by allowing standardization of components. Consequently, additional gas circuits can be added later, reducing investment and protecting against obsolescence.Micro-analytical measurement sensors can also be added to enable remote monitoring through Parker Pilot Pro™, a communications interface designed to link plant process control operations and analyzer maintenance networks to facilitate critical process control decision-making.SPECIFICATIONSInlet pressure: 500 psig standard; higher upon request Maximum outlet flow rate: 20 slpmOperational temperature: 0º-80ºC (32º-176ºF)Operational modes: Manual or electronicCommunication protocol: Analog, Device Net, RS-485Maximum number of gases: 5BLEND OR DILUTE UP TO 5 GASES TO CREATE A CUSTOMIZED MIXTURETo ServiceGas Blending 1M 8/11© 2011 Parker Hannifin CorporationParker Hannifin CorporationInstrumentation Products Division1005 A Cleaner WayHuntsville, AL 35805phone 256 881 2040fax 256 881 5730/ipdus。
Biogas, originating from biomass, sew-age plants and landfill sites is gaining increasing worldwide importance as a recognised renewable energy source. Generally, biogas is saturated with water vapour and contains other impurities which, when used as fuel, must be re-moved to prevent corrosion and damage to equipment and systems and improve cogeneration unit efficiency.Biogas is primarily composed of meth-ane and carbon dioxide with smaller amounts of hydrogen sulphide and am-monia. Trace amounts of other gases like hydrogen, nitrogen or carbon monoxide are also present in the biogas. Usually the mixed gas is saturated with water vapour and may contain dirt particles.The selection of effective biogas treat-ment equipment is therefore particu-larly important, both in optimising the cogeneration of electrical and thermal energy, making the most of the avail-able renewable energy, and reducing energy consumption and operating costs to a minimum.Parker’s solution is to dry the gas, firstly by cooling using a water-cooled heat ex-changer working with an air-cooled water chiller and secondly, by removing the condensed water with a cyclonic water separator. The cooled gas can then be reheated to reduce the relative humidity and thus meet the technical demands of gas engines, turbines and other down-stream equipment such as the Parker PpTek Siloxane Removal System and Biogas Upgrading System componentsSkid-Mounted Packages for Biogas andLandfill Gas Cooling ApplicationsProduct Description• The Parker Biogas Dehumidification System is a compact, robust and easy to handle plug & play gas conditioning package ensuring significant cost savings in investment, management and opera-tion• Available in a wide range of sizes from 50 Nm 3/h to 1500 Nm 3/h, the Parker system has performances and flow rates aligned with typical biogas plant designs and CHP capacities• All gas-side components are constructed from stainless steel (AISI304 or AISI316L) with additional pickling and passivation treatment in order to ensure highly reli-able and continuous operation even in the harshest site conditions• Designed using thermodynamic and fluid dynamic principles to ensure a high efficiency heat exchange and separation whilst maintaining low pressure drop • Flexibility to use a wide range of cooler/chiller combinations ensures the closestmatch to customer requirements thus de-livering constant dewpoint performance regardless of fluctuations in operatingconditions.Biogas Dehumidification SystemThe standard Biogas Dehumidification Systemcools biogas to a user defined dew point, using aHypercool BioEnergy heat exchanger working withHyperchill BioEnergy chiller and removing the con-densed water with the Hypersep BioEnergy separa-tor. Insulation, Hyperfilter BioEnergy and HyperdrainBioEnergy can be provided as options.Biogas Dehumidification SystemThis configuration is designed for installationswhere a blower is installed downstream of the De-humidification System, taking advantage of its posi-tion to increase the temperature of the biogas andthus decrease its Relative Humidity.Performances refer to operation with clean cooler and separator, gas flow rate at 20 °C/1 barg. Nominal working conditions: 60 % CH4, 40 % CO2, gas inlet temperature 40 °C saturated, refrigerant inlet water temperature 1 °C, ambient temperature 35 °C, gas outlet temperature at nominal conditions8 °C (from model skd60-007 to model skd265-024) and 4 °C (from model skd240-029 to model skd1620-116). Average pressure drop without filter 11 mbar +/-2 for all models, average pressure drops with filter 14 mbar +/- 2 for all models.*Data refer to skid without filter.B C DABiogas Dehumidification Systemwith ‘Gas2Gas’ Recuperator The Biogas Dehumidification System with ‘Gas-2Gas’ Recuperator BioEnergy cools biogas to auser-defined dew point and reheats the gas to aRelative Humidity lower than 50%. Insulation, Hy-perfilter BioEnergy and Hyperdrain BioEnergy canbe provided as options.This configuration is designed for installationswhere a blower is installed upstream of the De-humidification System with the ‘Gas2Gas’ Recu-perator providing free-cooling to save energy andfree-heating to reduce the Relative Humidity of thebiogas - without the need for auxiliary heating.Performances refer to operation with clean cooler and separator, gas flow rate at 20 °C/1 barg. Nominal working conditions: 55 % CH4, 45 % CO2,gas inlet temperature 50 °C (40 °C saturated), gas inlet pressure 75 mbarg, refrigerant inlet water temperature 1 °C, ambient temperature 35 °C, gasdew point at nominal conditions 8 °C (from model skd60-007 to model skd265-024) and 4 °C (from model skd240-029 to model skd1620-116), gasoutlet relative humidity below 50 %.*Data refer to skid without filter.B DABULBIOSKID-00-EN© 2016 Parker Hannifi n Corporation. All rights reserved.EMEA Product Information CentreFree phone: 00 800 27 27 5374(from AT , BE, CH, CZ, DE, DK, EE, ES, FI, FR, IE, IL, IS, IT , LU, MT , NL, NO, PL, PT , RU, SE, SK, UK, ZA)US Product Information Centre Toll-free number: 1-800-27 27 537/hzfdThe Key Components of the Parker Biogas Dehumidifi cation SystemHyperchill BioEnergy (ICE series)• Chiller Output 5 – 360 kW;• Special coating for corrosive environment;• Pump & tank installed in casing;• Microprocessor controlled;• Ambient range -20 °C to +45 °C • Compliant scroll refrigerant compressor;• IP54 protection as standard.Hypercool BioEnergy (WFB Series)• High cooling effi ciency with low pressure drop design;• Material: Parts in contact with biogas in AISI304 or AISI316L, parts not in contact with biogas in AISI304;• Max. working pressure: 0,5 barHypersep BioEnergy (CSB Series)• Cyclonic separator optimized for biogas applications • High separation effi ciency with very low pressure drop;• Material: Parts in contact with biogas in AISI304 or AISI316L, • Max. working pressure: 0,5 bar g.Optional Additions to Standard Skid PackageInstalled on a hot-galvanized steel frame, the water-chiller (Hyperchill BioEnergy), cooler (Hypercool Bio-Energy) and centrifugal separator (Hypersep BioEnergy) are the key components of the Biogas De-humidifi cation System: they havebeen specifi cally designed forbiogas applications and provide safe and reliable operation in the harsh environments typically found at AD and Landfi ll biogas produc-tion sites.Furthermore, the standard biogasThe standard Biogas Dehumidifi cation System can be extended to include additional components such as a particulate fi lter, condensate drain and/or energy-saving, 'Gas2Gas’ recuperator.Hyperfi lter BioEnergy (FFB)• Particle removal size 5 • or 20 μm • Filtration Effi ciency 99,999 % • Differential pressure 2 mbar • Material: AISI304 or AISI316L, with additional pickling and passivation treatment• Max. working pressure: 0,5 bar g .Gas2Gas Recuperator BioEnergy (RBB)• Free-cools incoming biogas to reduce chiller cooling load• Free-heats outgoing biogas to reduce relative humidity thus eliminating the need for auxiliary heating• High thermal transfer effi ciency with very low pressure drop • Material: AISI304 or AISI316L, with additional pickling andHyperdrain BioEnergy (HDF220BE)• Designed to work with dirtycondensate and for low pressureoperation• No electrical wiring• No gas loss• Parts in contact with condensate in stainless steel and reinforced polyamide, body treated with special Hiroshield treatmentfor optimal operation in harsh environmentspassivation treatmentdehumidifi cation package includes water connections between Hy-perchill and Hypercool, water isolating valves, water expansion tank, and counterfl anges kit with gaskets for easier connection of the system to the customer pipes.。
气体分析仪预处理系统TR系列气体分析仪预处理系统TR系列气体分析仪样品预处理系统产品说明：TR系列样品预处理系统主要应用于合成氨、尿素、甲醇、炼油化工及煤化工行业工艺过程分析采样系统当中，预处理系统针对样品介质高温、高压、含油、含水、含粉尘进行处理，同时对样品介质进行伴热、除硫等特殊处理，使样品介质完全满足过程分析仪表的分析要求，使气体分析仪的使用寿命及分析精度能更加长久和准确。
为了保证在线分析仪表能长期稳定的工作，除了分析器的稳定的样品预处理系统，样品预处理的目的主要实现以下几点：减压：对于工艺管线中压力较高的样品必须进行降压处理。
降温和升温：对于工艺管线中温度较高的样品必须进行降温温处理。
过滤：对于含杂质的样品必须过滤，方法是：采用过滤器或干燥：对于有水气的样品，必须进行干燥处理。
汽化：对于液体样品，必须进行汽化处理。
本公司可以根据用户的特殊要求，根据样品的不同特性介质要求的样品预处理，从而更加满足和适应现场的工艺需要。
如：焦炉煤气中除去多于的焦油和萘为了在样品传输过程中，取样管不易堵塞。
硫磺装置的硫分析、催化裂化装置的烟道抽风的目的，保证样品的正确分析。
应用范围：专用气体分析系统，全自动控制、自动排水、自动反吹、自动标定等，用于窑尾气体分析、一级筒气体分析、煤粉仓气体分析、磨煤机气体分析、天然气分析、合成氨过程分析、甲醛过程分析、尿素循环气分析、催化裂化装置再生烟气分析、硫回收装置过程分析、烯炔、芳炔过程气体分析、炼油过程分析、原料气检测、氧化反映气体分析、甲烷转化分析、伴水煤气气体分析、低温甲醛洗气体分析、变换脱碳气体分析、CEMS烟气分析、等各种气体分析场所。
高品质的预处理装置，保证了系统可靠的运行。
测量组份：CO、O2、CH4、H2、C2H2、C3H8、NH3、SO2、HC、HE、CO2、NO等量程：0-100%或者0-1000ppm等TR系列预处理相关配置:1.带有专用专利配套取样探头；2.气体分析过程专业开关、排液阀件和联接件；3.专业的气动阀件；4.蒸汽或电保温箱；5.专用高压减压箱；6.提供特殊型样品预处理系统的设计方案。
