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GW9508_LCMS_08442_MedChemExpress

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=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 47
Acq. Instrument : HY-LCMS-02 Location : P1-E-06Injection Date : 3/25/2015 12:36:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\100-1000MS+3MIN- 1.5_(0.02%FA).M
Last changed : 3/25/2015 9:12:23 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 3/25/2015 1:45:07 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃
Catalog No : HY-15589 Batch#08442 A-RP-132
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.53mAU 0
200400
6008001000 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150325\20150325 2015-03-25 09-12-23\CPK2015-325-08442.D)
2.085
2.279
2.494 2.560 2.630 2.687
2.794
===================================================================== Area Percent Report =====================================================================
Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000
Do not use Multiplier & Dilution Factor with ISTDs
Signal 1: DAD1 C, Sig=254,4 Ref=off
Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %
----|-------|----|-------|----------|----------|--------| 1 2.085 MM 0.0515 2.00007 6.47093e-1 0.0687 2 2.279 MM 0.0432 2900.24390 1118.81543 99.6838 3 2.494 MM 0.0390 2.00280 8.56075e-1 0.0688 4 2.560 MM 0.0399 5.71056e-1 2.38347e-1 0.0196 5 2.630 MM 0.0517 8.27010e-1 2.66358e-1 0.0284 6 2.687 MM 0.0448 2.64182 9.82754e-1 0.0908 7 2.794 MM 0.0626 1.15742 3.08003e-1 0.0398
Totals : 2909.44407 1122.11406
===================================================================== *** End of Report ***
=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 47
Acq. Instrument : HY-LCMS-02 Location : P1-E-06Injection Date : 3/25/2015 12:36:55 PM Inj : 1
Inj Volume : 3.000 µl
Acq. Method : D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\100-1000MS+3MIN- 1.5_(0.02%FA).M
Last changed : 3/25/2015 9:12:23 AM by Li Shan(LCMS-02)
Analysis Method : D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)
Last changed : 3/25/2015 1:46:20 PM by Li Shan(LCMS-02) (modified after loading)
Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃
Catalog No : HY-15589 Batch#08442 A-RP-132
Additional Info : Peak(s) manually integrated
min
0.5
1
1.5
2
2.5
3
50000
100000150000200000250000300000350000400000450000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\CPK2015-325-08442.D) ES-API, Pos, Sc
2.291
MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.
Reportable Ion Abundance: > 10%.
Retention Mol. Weight Time (MS) MS Area or Ion
2.291 2483369 348.90 I 347.90 I
m/z
100
200
300
400
500
600
20406080100*MSD1 SPC, time=2.254:2.327 of D:\AGLIENT 1260\DATA\20150325\20150325 2015-03-25 09-12-23\CPK2015-325-08442.D ES-API Max: 257664
348.9
347.9
*** End of Report ***。

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MedBio_CAS号210830-32-3 N-Me-D-Val-OH·HCl相关物理参数

MedBio_CAS号210830-32-3 N-Me-D-Val-OH·HCl相关物理参数

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≥98%
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英文名称
CAS
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MED11116
Fmoc-(2-氯苄氧基羰基)赖氨酸
Fmoc-Lys(2-Cl-Z)-OH
133970-31-7
25g
≥98%
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英文名称
CAS
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MED11078
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Fmoc-D-N-Me-Leu-OH
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CAS
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Boc-D-N-Me-Phe.DCHA
102185-45-5
25g
≥98%
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MED11002
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Boc-ON
58632-95-4
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MED11120
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Fmoc-Lys(Fmoc)-OH
78081-87-5
100g
≥98%
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MED11110
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Fmoc-Ile-OH
靶向代谢组学检测物汇总表

靶向代谢组学检测物汇总表

靶向代谢组学检测物汇总表上海鹿明生物科技有限公司靶向代谢组学检测物汇总表10大类 145种代谢物鹿明生物· 代谢部2018-9目录靶向代谢组学检测物汇总表 (2)1.胆汁酸（15种）-LCMS (2)2.胆固醇类物质-LCMS（12种） (2)3.神经递质类物质-LCMS（27种） (3)4.常见氨基酸-GCMS（20种） (4)5.羧酸类物质-LCMS（7种） (4)6.植物次级代谢物-LCMS（27种） (5)7.短链脂肪酸-GCMS（7种） (6)8.嘌呤代谢相关物质-LCMS（GCMS）（14种） (6)9.木质素代谢途径化合物-LCMS（9种） (7)10.糖类-GCMS（单糖或二糖,6种） (7)靶向代谢组学检测物汇总表1.胆汁酸（15种）-LCMS中文名英文名CAS号分子式分子量胆酸Cholic acid 81-25-4 C24H40O5408.6 鹅去氧胆酸Chenodeoxycholic acid 474-25-9 C24H40O4392.6 去氧胆酸Deoxycholic acid 83-44-3C24H40O4392.6 石胆酸Lithocholic acid 434-13-9 C24H40O3376.6 熊脱氧胆酸Ursodeoxycholic acid 128-13-2 C24H40O4392.6 甘氨胆酸Glycocholic acid 475-31-0 C26H43NO6465.6 甘氨鹅脱氧胆酸Glycochenodeoxycholic acid 640-79-9 C26H43NO5449.6 甘氨脱氧胆酸Glycodeoxycholic acid 360-65-6 C26H43NO5449.6 甘氨石胆酸Glycocholic acid 475-31-0 C26H43NO6465.6 甘氨熊脱氧胆酸Glycoursodeoxycholic acid 64480-66-6 C26H43NO5449.6 牛磺胆酸 Taurocholic acid 81-24-3 C26H45NO7S 515.7 牛磺鹅脱氧胆酸T aurochenodeoxycholic acid 516-35-8 C26H45NO6S 499.7 牛磺脱氧胆酸Tauroursodeoxycholic acid 14605-22-2 C26H45NO6S 499.7 牛磺石胆酸Taurolithocholic acid 516-90-5 C26H45NO5S 483.7 牛磺熊脱氧胆酸Tauroursodeoxycholic acid 14605-22-2 C26H45NO6S 499.72.胆固醇类物质-LCMS（12种）英文名CAS号分子式分子量Cholesterol 57-88-5 C27H46O 386.7 25-hydroxycholesterol-3-sulfate 884905-07-1 C27H46O5S 482.7 22R-Hydroxycholesterol 17711-16-9 C27H46O2402.725-hydroxycholesterol 2140-46-7 C27H46O2402.727-hydroxycholesterol 20380-11-4 C27H46O2402.724-Hydroxycholesterol 474-73-7 C27H46O2402.724,25-Epoxy-cholesterol 77058-74-3 C27H44O2400.67beta-hydroxycholesterol 566-27-8 C27H46O2402.74beta-hydroxycholesterol 17320-10-4 C27H46O2402.7 7-ketocholesterol 566-28-9 C27H44O2400.6 7alpha-hydroxycholesterol 566-26-7 C27H46O2402.7 cholesterol 3-sulfate 2864-50-8 C27H48NaO4S 491.73.神经递质类物质-LCMS（27种）中文名英文名CAS号分子式分子量3,4-二羟基苯基乙酸3,4-dihydroxyphenylacetic acid 102-32-9 C8H8O4168.1 3-羟基邻氨基苯甲酸3-hydroxyanthranilic acid 548-93-6 C7H7NO3153.1 5-羟色胺5-hydroxytryptamine 50-67-9 C10H12N2O 176.2 5-羟基吲哚乙酸5-hydroxyindoleacetic acid 54-16-0 C10H9NO3191.2 5-羟色氨酸5-hydroxytryptophan 56-69-9 C11H12N2O3220.2 α-酮戊二酸Alpha-ketoglutaric acid 328-50-7 C5H6O5146.1多巴胺Dopamine 51-61-6 C8H11NO2153.2 γ-氨基丁酸Gamma-aminobutyric acid 56-12-2 C4H9NO2103.1谷氨酸Glutamic acid 56-86-0 C5H9NO4147.1 谷氨酰胺Glutamine 61348-28-5 C10H18N2O5246.3 谷胱甘肽Glutathione 70-18-8 C10H17N3O6S 307.3犬尿酸Kynurenic acid 492-27-3 C10H7NO3189.2 犬尿氨酸Kynurenine 343-65-7 C10H12N2O3208.2 左旋多巴Levodopa 59-92-7 C9H11NO4197.2 L-苯丙氨酸L-phenylalanine 673-31-4 C10H13NO2179.2 L-酪氨酸L-tyrosine 70642-86-3 C14H19NO5281.3 N-乙酰5-羟色胺N-acetyl serotonin 1210-83-9 C12H14N2O2218.3 鸟氨酸Ornithine 70-26-8 C5H12N2O2132.2 苯乙胺Phenylethylamine 64-04-0 C8H11N 121.2琥珀酸Succinic acid 110-15-6 C4H6O4118.1色胺Tryptamine 61-54-1 C10H12N2160.2色氨酸Tryptophan 5241-64-5 C16H20N2O4304.3色醇Tryptophol 526-55-6 C10H11NO 161.2酪胺Tyramine 51-67-2 C8H11NO 137.2 香草扁桃酸Vanillylmandelic acid 55-10-7 C9H10O5198.2 去甲肾上腺素Norepinephrine 51-41-2 C8H11NO3169.2 吲哚-3-甲醛Indole-3-carboxaldehyde 487-89-8 C9H7NO 145.24.常见氨基酸-GCMS（20种）中文名英文名CAS号缩写分子式分子量酪氨酸Tyrosine 70642-86-3 Tyr C14H19NO5281.3 缬氨酸Valine 7004-03-7 Val C5H11NO2117.1 苯丙氨酸Phenprobamate 673-31-4 Phe C10H13NO2179.2 丝氨酸Serine 302-84-1 Ser C3H7NO3105.1 谷氨酰胺Glutamine 61348-28-5 Gln C10H18N2O5246.3 亮氨酸Leucine 3588-60-1 Leu C14H19NO4265.3 天冬酰胺Asparagine 70-47-3 Asn C4H8N2O3132.1 组氨酸Histidine 71-00-1 His C6H9N3O2155.2 脯氨酸Dl-proline 609-36-9 Pro C5H9NO2115.1 半胱氨酸Cysteine 52-90-4 Gys C3H7NO2S 121.2 异亮氨酸Isoleucine 7004-09-3 Ile C6H13NO2131.2 谷氨酸Glutamic acid 56-86-0 Glu C5H9NO4147.1 苏氨酸Threonine 72-19-5 Thr C4H9NO3119.1 天冬氨酸Aspartic acid 6899-03-2 Asp C4H7NO4133.1 色氨酸Tryptophan 5241-64-5 Try C16H20N2O4304.3 赖氨酸Lysine 56-87-1 Lys C6H14N2O2146.2 甘氨酸Glycine 56-40-6 Gly C2H5NO275.1 甲硫氨酸Methionine 59-51-8 Met C5H11NO2S 149.2 丙氨酸Alanine 338-69-2 Ala C3H7NO289.1 精氨酸Arginine 74-79-3 Arg C6H14N4O2174.25.羧酸类物质-LCMS（7种）中文名英文名CAS号缩写分子式分子量草酸Oxalic acid 144-62-7 OA C2H2O490.0 丙酮酸Pyruvic acid 127-17-3 PA C3H4O388.1 棕榈酸Palmitic acid 57-10-3 Pal C16H32O2256.4 油酸Oleic acid 112-80-1 Ole C18H34O2282.5 亚油酸Linoleic acid 60-33-3 Lin C18H32O2280.5 愈伤酸Traumatic Acid 6402-36-4 Tra C12H20O4228.3 亚麻酸Linolenic acid 463-40-1 Lino C18H30O2278.46.植物次级代谢物-LCMS（27种）类别中文名英文名CAS号分子式分子量植物激素Phytohormones茉莉酸(+/-)-Jasmonic acid 3572-66-5 C12H18O3210.3 水杨酸Salicylic acid 69-72-7 C7H6O3138.1 生长素Indoleacetic acid 87-51-4 C10H9NO2175.2 脱落酸Abscisic acid 14375-45-2 C15H20O4264.3 反式玉米素Trans-Zeatin 1637-39-4 C10H13N5O219.24 N-(3-吲哚乙酰基)-L-丙氨酸N-(3-Indolylacetyl)-L-alanine 57105-39-2C13H14N2O3246.266 1-氨基环丙烷-1-羧酸1-AminocyclopropanecarboxylicAcid22059-21-8 C4H7NO2101.105生物碱Alkaloids加兰他敏Galanthamine 357-70-0 C17H21NO3287.4 石蒜胺Lycoramine 21133-52-8 C17H23NO3289.4 石蒜碱Lycorine 476-28-8 C16H17NO4287.3 降孤挺花啶Norbelladine C15H17NO3259.3 4'-o-methylnorbelladine 4579-60-6 C16H19NO3273.3类黄酮Flavonoids 大豆黄素Daidzein 486-66-8 C15H10O4254.2 白杨素Chrysin 480-40-0 C15H10O4254.2 异甘草素Isoliquiritigenin 961-29-5 C15H12O4256.3 乔松素Pinocembrin 480-39-7 C15H12O4256.3 芒丙花素Formononetin 485-72-3 C16H12O4268.3 芹菜素Apigenin 520-36-5 C15H10O5270.2 高良姜素Galangin 548-83-4 C15H10O5270.2 染料木素Genistein 446-72-0 C15H10O5270.2 木犀草素Luteolin 491-70-3 C15H10O6286.2 表儿茶素(-)-Epicatechin 490-46-0 C15H14O6290.3 儿茶素(+)-Catechin 154-23-4 C15H14O6290.3 桑色素Morin 480-16-0 C15H10O7302.2 异鼠李素Isorhamnetin 480-19-3 C16H12O7316.3 牡荆素Vitexin 3681-93-4 C21H20O10432.4 芦丁Rutin 153-18-4 C27H30O16610.57.短链脂肪酸-GCMS（7种）中文名英文名CAS号分子式分子量乙酸Acetic Acid97-67-6 C2H4O260.05丙酸Propionic acid69-93-2 C3H6O274丁酸Butyric Acid68-94-0 C4H8O288.11戊酸Pentanoic acid70-18-8 C5H10O2102.13己酸Hexanoic Acid58-63-9 C6H12O2116.16异丁酸Isobutyric acid58-96-8 C4H8O288.11异戊酸Isovaleric acid3868-31-3 C5H10O2102.138.嘌呤代谢相关物质-LCMS（GCMS）（14种）中文名英文名CAS号分子式分子量L-苹果酸L-Malic acid 97-67-6 C4H6O5134.1 尿酸Uric acid 69-93-2 C5H4N4O3168.1 次黄嘌呤Hypoxanthine 68-94-0 C5H4N4O 136.1 谷胱甘肽Glutathione 70-18-8 C10H17N3O6S 307.3 肌苷Inosine 58-63-9 C10H12N4O5268.2 尿苷Uridine 58-96-8 C9H12N2O6244.2 8-羟基鸟苷8-Hydroxyguanosine 3868-31-3 C10H13N5O6299.2 8-羟基-2'-脱氧鸟苷8-Hydroxy-2′-deoxyguanosine 88847-89-6 C10H13N5O5283.2 黄嘌呤Xanthine 69-89-6 C5H4N4O2152.1 胞嘧啶Cytosine 71-30-7 C4H5N3O 111.1 吲哚-3-乳酸Indole-3-lactic acid 1821-52-9 C11H11NO3205.2 鞘氨醇D-erythro-Sphingosine 123-78-4 C18H37NO2299.5 腺苷Adenosine 58-61-7 C10H13N5O4267.2 5'-一磷酸腺苷Adenosine 5'-monophosphate 61-19-8 C10H14N5O7P 347.29.木质素代谢途径化合物-LCMS（9种）中文名英文名CAS号分子式分子量肉桂酸Cinnamic acid 140-10-3 C9H8O2148.161 咖啡酸Caffeic acid 331-39-5 C9H8O4180.159 阿魏酸Ferulic acid 1135-24-6 C10H10O4194.186 芥子酸Sinapic acid 7362-37-0 C11H12O5224.212 松柏醇Coniferyl alcohol 438-35-5 C10H12O3180.203 芥子醇Sinapyl alcohol 537-33-7 C11H14O4210.229 松柏醛Coniferyl aldehyde 458-36-6C10H10O3178.187 芥子醛Sinapaldehyde 4206-58-0 C11H12O4208.213 对香豆酸P-coumaric acid 501-98-4 C9H8O3164.1610.糖类-GCMS（单糖或二糖,6种）中文名英文名CAS号分子式分子量葡萄糖glucose50-99-7 C6H12O6180.16果糖fructose57-48-7 C6H12O6180.16半乳糖Galactose10257-28-0 C6H12O6180.16乳糖lactose14641-93-1 C12H22O11342.3麦芽糖maltose69-79-4 C12H22O11342.3海藻糖Trehalose99-20-7 C12H22O11342.3。

超高效液相色谱-串联质谱仪测定纺织品中的喹啉

超高效液相色谱-串联质谱仪测定纺织品中的喹啉

超高效液相色谱-串联质谱仪测定纺织品中的喹啉摘要：本文建立了一种采用超高效液相色谱-串联质谱仪（UPLC-MS/MS）测试纺织品中喹啉的方法，以甲醇为溶剂，通过超声波萃取，采用超高效液相色谱-串联质谱仪（UPLC-MS/MS）对萃取液分析来测定样品中的喹啉含量。

结果表明，喹啉在0.1 mg/L~2.0 mg/L范围内线性良好（r>0.9990），回收率为92.5%~99.3%，相对标准偏差<3%，方法定量限可低至3mg/kg，可用于快速定量分析纺织品中喹啉的含量。

关键词：纺织品；喹啉；超高效液相色谱-串联质谱仪（UPLC-MS/MS）Determination of Quinoline in textile by UPLC-MS/MSXiaoyingHe, Shuke He,Yanfen.HuangAbstract: A method was established for the determination of Quinoline in textile sample by UPLC-MS/MS through ultrasonicextraction with methanol. The results showed that Quinoline have good linearity in the range of 0.1 mg/L~2.0 mg/L (r>0.9990), values of recovery in the range of 92.5%~99.3%, the RSDs were less than 3%, and the LOQ of method was as low as3 mg/kg.It could be used for rapid quantitative analysis of Quinoline in textile sample.Keywords: Textile; Quinoline; UPLC-MS/MS引言喹啉（Quinoline）是一种芳香类化合物，喹啉或其衍生物常用于制取C.I.酸性黄3、C.I.直接黄22、C.I.溶剂黄33和Palanil黄3G等染料，这些染料是黄色染料的主导品种，在印染行业中，常用于纺织品的染色；另外，喹啉经过硝化、还原得到氨基喹啉，也会被用于纺织品染色辅助剂和毛发、毛坯染色剂。

一种制备阿格列汀的方法[发明专利]

一种制备阿格列汀的方法[发明专利]

专利名称：一种制备阿格列汀的方法
专利类型：发明专利
发明人：邹春兰,邓杰,张强,谢守全,王学瑞,蔡中文,叶文润申请号：CN201210313836.8
申请日：20120830
公开号：CN103664801A
公开日：
20140326
专利内容由知识产权出版社提供
摘要：本发明涉及一种阿格列汀及其苯甲酸盐和其中间体的制备方法，该方法包括在四氢呋喃溶剂和碱的催化下，用2-氰基溴苄将6-氯尿嘧啶烷基化，产生N-苄基尿嘧啶衍生物，再用甲醇通过Mitsunobu反应进一步甲基化获得1，3-二取代尿嘧啶（中间体），该方法革除了现有技术中的NaH 危险试剂和剧毒试剂碘甲烷，安全环保。

申请人：重庆医药工业研究院有限责任公司
地址：400061 重庆市南岸区涂山路565号
国籍：CN
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