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TM5275_sodium_LCMS_24958_MedChemExpress

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File ..0615 2017-06-15 08-37-23\BIZ2017-615-WYQ5.D Tgt Mass (CHM): Injection Date : 15 Jun 17 2:47 pm +0800 Seq. Line : 78 Sample Name : BIZ2017-615-WYQ5 Location : P1-C-08 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170615\20170615 2017-06-15 08-37-23\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\DATA\20170615\20170615 2017-06-15 08-37-23\1-POS-3MIN.M

Catalog No : HY-100447 Batch#24958 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min0.511.522.5mAU

05001000 DAD1 B, Sig=214,4 Ref=off

0.519

1.337

1.466

1.5161.616

1.757

2.049

min0.511.522.5mAU

0200400600 DAD1 C, Sig=254,4 Ref=off

1.383

1.5211.616

1.757

2.050

min0.511.522.50100000200000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.607

min0.511.522.50100020003000 Ion 544.1, MSD1 544.1,Target Mass 543.1 +H Positive, EIC=543.8:544.8

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|

0.52 0.02 3.04 2.11 0.14 ND 1.34 0.02 0.68 0.70 0.03 340 1.47 0.03 2.49 1.45 0.12 ND 1.52 0.02 0.60 0.54 0.03 233 1.62 0.02 2116.13 1715.92 99.05 522 1.76 0.02 11.91 10.45 0.56 233 2.05 0.02 1.67 1.55 0.08 233

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|

1.38 1.66 0.18 0.21 0.02 ND 1.52 0.02 0.28 0.26 0.03 233 1.62 0.02 933.50 765.81 99.14 522 1.76 0.14 5.42 4.62 0.58 558 2.05 0.55 2.18 1.43 0.23 233

Integration Results for MSD1 TIC, MS FileMS Report from Instrument: LCMS-02

LCMS-02 6/15/2017 15:14:00 CLJ_701Page 1 of 3 RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------| 1.61 0.03 568789.56 1115.51 100.00 522

MS Report from Instrument: LCMS-02

LCMS-02 6/15/2017 15:14:00 CLJ_701Page 2 of 3Ret. Time: 1.61 <<<< POSITIVE SPECTRA >>>>

m/z200300400500600700800900010000200003000040000 ES-API Positive

525.2 523.2 522.2MS Report from Instrument: LCMS-02

LCMS-02 6/15/2017 15:14:00 CLJ_701Page 3 of 3

合集下载

AZD2858_LCMS_15985_MedChemExpress

AZD2858_LCMS_15985_MedChemExpress

=====================================================================

Acq. Operator : Li Shan(LCMS-02) Seq. Line : 18Acq. Instrument : HY-LCMS-02 Location : P2-F-05

Injection Date : 5/8/2015 5:07:05 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150508-1\20150508-1 2015-05-08 15-51-47\100-1000MS+ 3MIN-1.5_(0.02%FA).MLast changed : 5/8/2015 3:51:47 PM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\1.MLast changed : 5/11/2015 11:25:26 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-15761 Batch#15985 A-RP-132 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

0200400600800 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...ATA\20150508-1\20150508-1 2015-05-08 15-51-47\BIZ2015-508-DJL6.D) 1.510

CCG-1423_LCMS_14741_MedChemExpress

CCG-1423_LCMS_14741_MedChemExpress

=====================================================================

Acq. Operator : Li Shan(LCMS-02) Seq. Line : 39Acq. Instrument : HY-LCMS-02 Location : Vial 37

Injection Date : 1/19/2015 12:41:52 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\100-1000MS+3MIN( 0.02%FA).MLast changed : 1/19/2015 9:28:05 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_45-H01P(RP-HPLC).MLast changed : 1/19/2015 1:39:23 PM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13991 Batch#14741 A-RP-124 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

0200400600800 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL1.D)

1.637 2.036 2.189

===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.637 MM 0.0440 6.46704e-1 2.44930e-1 0.0233 2 2.036 MM 0.0430 1.14979 4.46148e-1 0.0414 3 2.189 MM 0.0432 2774.82788 1070.50586 99.9353 Totals : 2776.62438 1071.19694 ===================================================================== *** End of Report ***Data File D:\AGLIENT 1260\DATA\20150119\20150119 2015-01-19 09-28-05\BIZ2015-119-DJL1.DSample Name: BIZ2015-119-DJL1

NSC_405020_LCMS_12741_MedChemExpress

NSC_405020_LCMS_12741_MedChemExpress

File ..710 2017-07-10 08-26-50\CPK2017-707-12741.D Tgt Mass (CHM): Injection Date : 10 Jul 17 7:29 pm +0800 Seq. Line : 146 Sample Name : CPK2017-707-12741 Location : P1-F-06 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170710\20170710 2017-07-10 08-26-50\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\DATA\20170710\20170710 2017-07-10 08-26-50\1-POS-3MIN.M

Catalog No : HY-15827 Batch#12741 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min0.511.522.5mAU

05001000 DAD1 B, Sig=214,4 Ref=off

0.377

0.703

1.8742.032

min0.511.522.5mAU

0200400 DAD1 C, Sig=254,4 Ref=off

1.9022.032

min0.511.522.50200000400000600000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

MK-4827_tosylate_NP-HPLC_25385_MedChemExpress

MK-4827_tosylate_NP-HPLC_25385_MedChemExpress

=====================================================================

Acq. Operator : CSS Seq. Line : 19Acq. Instrument : HPLC-04 Location : Vial 4

Injection Date : 7/13/2017 5:45:27 PM Inj : 1 Inj Volume : 5.0 µlAcq. Method : D:\CHEM\DATA\20170713\20170713 2017-07-13 09-00-13\OJ,80B-ETOH,220NM,C2.MLast changed : 7/13/2017 4:36:40 PM by CSSAnalysis Method : D:\CHEM\METHODS\AD,80-ETOH,220NM.MLast changed : 7/14/2017 8:35:23 AM by CSS (modified after loading)Catalog No : HY-10619B Batch#25385 C-NP-22 Additional Info : Peak(s) manually integrated

min0510152025mAU

-50-40-30-20-10010203040 VWD1 A, Wavelength=220 nm (D:\CHEM\DATA\20170713\20170713 2017-07-13 09-00-13\004-1901.D)

===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier: : 1.0000Dilution: : 1.0000Use Multiplier & Dilution Factor with ISTDs No peaks found ===================================================================== *** End of Report ***Data File D:\CHEM\DATA\20170713\20170713 2017-07-13 09-00-13\004-1901.DSample Name: BIZ2017-713-WYQ4_0