英文文献翻译
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01搜狗翻译搜狗翻译的文档翻译功能有三个优点:第一,可以直接上传文档,流程操作简单化,这才是一键翻译哇,我之前只能说是很多键……;第二,在线阅读翻译结果时,系统可实时提供原文与译文的双屏对照,方便对比查看;第三,译文可直接免费下载,方便进一步研读或分享。
02Google Chrome浏览器假设一个情景,你想在PubMed上找到以清华大学为第一单位的施一公教授的文章,那么,可以在Chrome浏览器上,登上PubMed,搜索格式为Yigong Shi Tsinghua University,即可找到其发表的文章。
接着,看上一篇蛮不错的,点击进去看看,然后,还是全英文。
这时候,你可以试下Chrome自带的网页翻译,真的可以秒翻译,将英文翻译为中文,而且还可以快速转换中/英界面。
03Adobe Acrobat笔者在这里给大伙介绍另一款秒翻译PDF文档的神器(笔者使用的Adobe Acrobat Pro DC,至于具体的下载和安装方式,读者可自行百度)。
但是,需要注意一点,这是Adobe Acrobat,而不是Adobe Reader。
在这里,请应许笔者介绍下开发出Adobe Acrobat的公司——Adobe。
Adobe,在软件界绝对是巨头中巨头的存在。
打个比方,我们常用的PS、PR、AE、In、LR等,无一例外都是领域中的顶尖水平,而且都是Adobe家的。
其中,Adobe家中就有一款几位出色的PDF编辑及处理软件——Adobe Acrobat。
(据说PDF作为国际通用的文件存储格式,也是依它而起)OK,进入主题,Adobe Acrobat是长这个样子的。
它可能干嘛呢?PDF 转word、图片合拼为PDF、编辑PDF等等,可以说,与PDF相关的,它都可以搞定。
那如何使用它来帮助我们翻译文献PDF呢?第一步,用它打开文献PDF文件;第二步,点击使用界面上的“文件”,接着点击“另存为”,选择存储格式为“HTML”,如下图;第三步,PDF文档在导出完成后,会得到两个文件,一是将PDF转为HTML格式的网页文件,另一个则是支持网页文件里面的图片(若删,网页里面的图片显示不出来)第四步,找到网页文件,打开方式选择Google Chrome浏览器,接着,结合Chrome浏览器的网页翻译,即可秒翻。
外文文献原稿和译文原稿Sodium Polyacrylate:Also known as super-absorbent or “SAP”(super absorbent polymer), Kimberly Clark used to call it SAM (super absorbent material). It is typically used in fine granular form (like table salt). It helps improve capacity for better retention in a disposable diaper, allowing the product to be thinner with improved performance and less usage of pine fluff pulp. The molecular structure of the polyacrylate has sodium carboxylate groups hanging off the main chain. When it comes in contact with water, the sodium detaches itself, leaving only carboxylions. Being negatively charged, these ions repel one another so that the polymer also has cross-links, which effectively leads to a three-dimensional structure. It has hige molecular weight of more than a million; thus, instead of getting dissolved, it solidifies into a gel. The Hydrogen in the water (H-O-H) is trapped by the acrylate due to the atomic bonds associated with the polarity forces between the atoms. Electrolytes in the liquid, such as salt minerals (urine contains 0.9% of minerals), reduce polarity, thereby affecting superabsorbent properties, especially with regard to the superabsorbent capacity for liquid retention. This is the main reason why diapers containing SAP should never be tested with plain water. Linear molecular configurations have less total capacity than non-linear molecules but, on the other hand, retention of liquid in a linear molecule is higher than in a non-linear molecule, due to improved polarity. For a list of SAP suppliers, please use this link: SAP, the superabsorbent can be designed to absorb higher amounts of liquids (with less retention) or very high retentions (but lower capacity). In addition, a surface cross linker can be added to the superabsorbent particle to help it move liquids while it is saturated. This helps avoid formation of "gel blocks", the phenomenon that describes the impossibility of moving liquids once a SAP particle gets saturated.History of Super Absorbent Polymer ChemistryUn til the 1980’s, water absorbing materials were cellulosic or fiber-based products. Choices were tissue paper, cotton, sponge, and fluff pulp. The water retention capacity of these types of materials is only 20 times their weight – at most.In the early 1960s, the United States Department of Agriculture (USDA) was conducting work on materials to improve water conservation in soils. They developed a resin based on the grafting of acrylonitrile polymer onto the backbone of starch molecules (i.e. starch-grafting). The hydrolyzed product of the hydrolysis of this starch-acrylonitrile co-polymer gave water absorption greater than 400 times its weight. Also, the gel did not release liquid water the way that fiber-based absorbents do.The polymer came to be known as “Super Slurper”.The USDA gave the technical know how several USA companies for further development of the basic technology. A wide range of grating combinations were attempted including work with acrylic acid, acrylamide and polyvinyl alcohol (PVA).Since Japanese companies were excluded by the USDA, they started independent research using starch, carboxy methyl cellulose (CMC), acrylic acid, polyvinyl alcohol (PVA) and isobutylene maleic anhydride (IMA).Early global participants in the development of super absorbent chemistry included Dow Chemical, Hercules, General Mills Chemical, DuPont, National Starch & Chemical, Enka (Akzo), Sanyo Chemical, Sumitomo Chemical, Kao, Nihon Starch and Japan Exlan.In the early 1970s, super absorbent polymer was used commercially for the first time –not for soil amendment applications as originally intended –but for disposable hygienic products. The first product markets were feminine sanitary napkins and adult incontinence products.In 1978, Park Davis (d.b.a. Professional Medical Products) used super absorbent polymers in sanitary napkins.Super absorbent polymer was first used in Europe in a baby diaper in 1982 when Schickendanz and Beghin-Say added the material to the absorbent core. Shortly thereafter, UniCharm introduced super absorbent baby diapers in Japan while Proctor & Gamble and Kimberly-Clark in the USA began to use the material.The development of super absorbent technology and performance has been largely led by demands in the disposable hygiene segment. Strides in absorption performance have allowed the development of the ultra-thin baby diaper which uses a fraction of the materials – particularly fluff pulp – which earlier disposable diapers consumed.Over the years, technology has progressed so that there is little if any starch-grafted super absorbent polymer used in disposable hygienic products. These super absorbents typically are cross-linked acrylic homo-polymers (usually Sodium neutralized).Super absorbents used in soil amendments applications tend to be cross-linked acrylic-acrylamide co-polymers (usually Potassium neutralized).Besides granular super absorbent polymers, ARCO Chemical developed a super absorbent fiber technology in the early 1990s. This technology was eventually sold to Camelot Absorbents. There are super absorbent fibers commercially available today. While significantly more expensive than the granular polymers, the super absorbent fibers offer technical advantages in certain niche markets including cable wrap, medical devices and food packaging.Sodium polyacrylate, also known as waterlock, is a polymer with the chemical formula [-CH2-CH(COONa)-]n widely used in consumer products. It has the ability to absorb as much as 200 to 300 times its mass in water. Acrylate polymers generally are considered to possess an anionic charge. While sodium neutralized polyacrylates are the most common form used in industry, there are also other salts available including potassium, lithium and ammonium.ApplicationsAcrylates and acrylic chemistry have a wide variety of industrial uses that include: ∙Sequestering agents in detergents. (By binding hard water elements such as calcium and magnesium, the surfactants in detergents work more efficiently.) ∙Thickening agents∙Coatings∙Fake snowSuper absorbent polymers. These cross-linked acrylic polymers are referred to as "Super Absorbents" and "Water Crystals", and are used in baby diapers. Copolymerversions are used in agriculture and other specialty absorbent applications. The origins of super absorbent polymer chemistry trace back to the early 1960s when the U.S. Department of Agriculture developed the first super absorbent polymer materials. This chemical is featured in the Maximum Absorbency Garment used by NASA.译文聚丙烯酸钠聚丙烯酸钠,又可以称为超级吸收剂或者又叫高吸水性树脂,凯博利克拉克教授曾经称它为SAM即:超级吸收性物质。
英文文献整篇翻译Title: The Impact of Climate Change on BiodiversityClimate change is a pressing issue that has significant impacts on biodiversity worldwide. Changes in temperature, precipitation patterns, and extreme weather events are altering ecosystems and threatening the survival of many species. The loss of biodiversity not only affects the natural world but also has implications for human societies.One of the major impacts of climate change onbiodiversity is the shifting of habitats. As temperatures rise, many species are forced to move to higher latitudesor elevations in search of suitable conditions. This can disrupt ecosystems and lead to the decline or extinction of species that are unable to adapt to the new conditions.In addition to habitat loss, climate change is also causing changes in the timing of biological events such as flowering, migration, and reproduction. These changes can disrupt the delicate balance of ecosystems and lead to mismatches between species that depend on each other for survival.Furthermore, climate change is exacerbating otherthreats to biodiversity such as habitat destruction, pollution, and overexploitation. The combination of these factors is putting immense pressure on many species and pushing them closer to extinction.It is essential that we take action to mitigate the impacts of climate change on biodiversity. This includes reducing greenhouse gas emissions, protecting and restoring habitats, and implementing conservation measures to safeguard vulnerable species. By addressing the root causes of climate change and protecting biodiversity, we canensure a sustainable future for both the natural world and human societies.气候变化对生物多样性的影响气候变化是一个紧迫的问题,对全球的生物多样性产生重大影响。
((英文参考文献及译文)二〇一六年六月本科毕业论文 题 目:STATISTICAL SAMPLING METHOD, USED INTHE AUDIT学生姓名:王雪琴学 院:管理学院系 别:会计系专 业:财务管理班 级:财管12-2班 学校代码: 10128 学 号: 201210707016Statistics and AuditRomanian Statistical Review nr. 5 / 2010STATISTICAL SAMPLING METHOD, USED IN THE AUDIT - views, recommendations, fi ndingsPhD Candidate Gabriela-Felicia UNGUREANUAbstractThe rapid increase in the size of U.S. companies from the earlytwentieth century created the need for audit procedures based on the selectionof a part of the total population audited to obtain reliable audit evidence, tocharacterize the entire population consists of account balances or classes oftransactions. Sampling is not used only in audit – is used in sampling surveys,market analysis and medical research in which someone wants to reach aconclusion about a large number of data by examining only a part of thesedata. The difference is the “population” from which the sample is selected, iethat set of data which is intended to draw a conclusion. Audit sampling appliesonly to certain types of audit procedures.Key words: sampling, sample risk, population, sampling unit, tests ofcontrols, substantive procedures.Statistical samplingCommittee statistical sampling of American Institute of CertifiedPublic Accountants of (AICPA) issued in 1962 a special report, titled“Statistical sampling and independent auditors’ which allowed the use ofstatistical sampling method, in accordance with Generally Accepted AuditingStandards (GAAS). During 1962-1974, the AICPA published a series of paperson statistical sampling, “Auditor’s Approach to Statistical Sampling”, foruse in continuing professional education of accountants. During 1962-1974,the AICPA published a series of papers on statistical sampling, “Auditor’sApproach to Statistical Sampling”, for use in continuing professional educationof accountants. In 1981, AICPA issued the professional standard, “AuditSampling”, which provides general guidelines for both sampling methods,statistical and non-statistical.Earlier audits included checks of all transactions in the period coveredby the audited financial statements. At that time, the literature has not givenparticular attention to this subject. Only in 1971, an audit procedures programprinted in the “Federal Reserve Bulletin (Federal Bulletin Stocks)” includedseveral references to sampling such as selecting the “few items” of inventory.Statistics and Audit The program was developed by a special committee, which later became the AICPA, that of Certified Public Accountants American Institute.In the first decades of last century, the auditors often applied sampling, but sample size was not in related to the efficiency of internal control of the entity. In 1955, American Institute of Accountants has published a study case of extending the audit sampling, summarizing audit program developed by certified public accountants, to show why sampling is necessary to extend the audit. The study was important because is one of the leading journal on sampling which recognize a relationship of dependency between detail and reliability testing of internal control.In 1964, the AICPA’s Auditing Standards Board has issued a report entitled “The relationship between statistical sampling and Generally Accepted Auditing Standards (GAAS)” which illustrated the relationship between the accuracy and reliability in sampling and provisions of GAAS.In 1978, the AICPA published the work of Donald M. Roberts,“Statistical Auditing”which explains the underlying theory of statistical sampling in auditing.In 1981, AICPA issued the professional standard, named “Audit Sampling”, which provides guidelines for both sampling methods, statistical and non-statistical.An auditor does not rely solely on the results of a single procedure to reach a conclusion on an account balance, class of transactions or operational effectiveness of the controls. Rather, the audit findings are based on combined evidence from several sources, as a consequence of a number of different audit procedures. When an auditor selects a sample of a population, his objective is to obtain a representative sample, ie sample whose characteristics are identical with the population’s characteristics. This means that selected items are identical with those remaining outside the sample.In practice, auditors do not know for sure if a sample is representative, even after completion the test, but they “may increase the probability that a sample is representative by accuracy of activities made related to design, sample selection and evaluation” [1]. Lack of specificity of the sample results may be given by observation errors and sampling errors. Risks to produce these errors can be controlled.Observation error (risk of observation) appears when the audit test did not identify existing deviations in the sample or using an inadequate audit technique or by negligence of the auditor.Sampling error (sampling risk) is an inherent characteristic of the survey, which results from the fact that they tested only a fraction of the total population. Sampling error occurs due to the fact that it is possible for Revista Română de Statistică nr. 5 / 2010Statistics and Auditthe auditor to reach a conclusion, based on a sample that is different from the conclusion which would be reached if the entire population would have been subject to audit procedures identical. Sampling risk can be reduced by adjusting the sample size, depending on the size and population characteristics and using an appropriate method of selection. Increasing sample size will reduce the risk of sampling; a sample of the all population will present a null risk of sampling.Audit Sampling is a method of testing for gather sufficient and appropriate audit evidence, for the purposes of audit. The auditor may decide to apply audit sampling on an account balance or class of transactions. Sampling audit includes audit procedures to less than 100% of the items within an account balance or class of transactions, so all the sample able to be selected. Auditor is required to determine appropriate ways of selecting items for testing. Audit sampling can be used as a statistical approach and a non- statistical.Statistical sampling is a method by which the sample is made so that each unit consists of the total population has an equal probability of being included in the sample, method of sample selection is random, allowed to assess the results based on probability theory and risk quantification of sampling. Choosing the appropriate population make that auditor’ findings can be extended to the entire population.Non-statistical sampling is a method of sampling, when the auditor uses professional judgment to select elements of a sample. Since the purpose of sampling is to draw conclusions about the entire population, the auditor should select a representative sample by choosing sample units which have characteristics typical of that population. Results will not extrapolate the entire population as the sample selected is representative.Audit tests can be applied on the all elements of the population, where is a small population or on an unrepresentative sample, where the auditor knows the particularities of the population to be tested and is able to identify a small number of items of interest to audit. If the sample has not similar characteristics for the elements of the entire population, the errors found in the tested sample can not extrapolate.Decision of statistical or non-statistical approach depends on the auditor’s professional judgment which seeking sufficient appropriate audits evidence on which to completion its findings about the audit opinion.As a statistical sampling method refer to the random selection that any possible combination of elements of the community is equally likely to enter the sample. Simple random sampling is used when stratification was not to audit. Using random selection involves using random numbers generated byRomanian Statistical Review nr. 5 / 2010Statistics and Audit a computer. After selecting a random starting point, the auditor found the first random number that falls within the test document numbers. Only when the approach has the characteristics of statistical sampling, statistical assessments of risk are valid sampling.In another variant of the sampling probability, namely the systematic selection (also called random mechanical) elements naturally succeed in office space or time; the auditor has a preliminary listing of the population and made the decision on sample size. “The auditor calculated a counting step, and selects the sample element method based on step size. Step counting is determined by dividing the volume of the community to sample the number of units desired. Advantages of systematic screening are its usability. In most cases, a systematic sample can be extracted quickly and method automatically arranges numbers in successive series.”[2].Selection by probability proportional to size - is a method which emphasizes those population units’recorded higher values. The sample is constituted so that the probability of selecting any given element of the population is equal to the recorded value of the item;Stratifi ed selection - is a method of emphasis of units with higher values and is registered in the stratification of the population in subpopulations. Stratification provides a complete picture of the auditor, when population (data table to be analyzed) is not homogeneous. In this case, the auditor stratifies a population by dividing them into distinct subpopulations, which have common characteristics, pre-defined. “The objective of stratification is to reduce the variability of elements in each layer and therefore allow a reduction in sample size without a proportionate increase in the risk of sampling.” [3] If population stratification is done properly, the amount of sample size to come layers will be less than the sample size that would be obtained at the same level of risk given sample with a sample extracted from the entire population. Audit results applied to a layer can be designed only on items that are part of that layer.I appreciated as useful some views on non-statistical sampling methods, which implies that guided the selection of the sample selecting each element according to certain criteria determined by the auditor. The method is subjective; because the auditor selects intentionally items containing set features him.The selection of the series is done by selecting multiple elements series (successive). Using sampling the series is recommended only if a reasonable number of sets used. Using just a few series there is a risk that the sample is not representative. This type of sampling can be used in addition to other samples, where there is a high probability of occurrence of errors. At the arbitrary selection, no items are selected preferably from the auditor, Revista Română de Statistică nr. 5 / 2010Statistics and Auditthat regardless of size or source or characteristics. Is not the recommended method, because is not objective.That sampling is based on the auditor’s professional judgment, which may decide which items can be part or not sampled. Because is not a statistical method, it can not calculate the standard error. Although the sample structure can be constructed to reproduce the population, there is no guarantee that the sample is representative. If omitted a feature that would be relevant in a particular situation, the sample is not representative.Sampling applies when the auditor plans to make conclusions about population, based on a selection. The auditor considers the audit program and determines audit procedures which may apply random research. Sampling is used by auditors an internal control systems testing, and substantive testing of operations. The general objectives of tests of control system and operations substantive tests are to verify the application of pre-defined control procedures, and to determine whether operations contain material errors.Control tests are intended to provide evidence of operational efficiency and controls design or operation of a control system to prevent or detect material misstatements in financial statements. Control tests are necessary if the auditor plans to assess control risk for assertions of management.Controls are generally expected to be similarly applied to all transactions covered by the records, regardless of transaction value. Therefore, if the auditor uses sampling, it is not advisable to select only high value transactions. Samples must be chosen so as to be representative population sample.An auditor must be aware that an entity may change a special control during the course of the audit. If the control is replaced by another, which is designed to achieve the same specific objective, the auditor must decide whether to design a sample of all transactions made during or just a sample of transactions controlled again. Appropriate decision depends on the overall objective of the audit test.Verification of internal control system of an entity is intended to provide guidance on the identification of relevant controls and design evaluation tests of controls.Other tests:In testing internal control system and testing operations, audit sample is used to estimate the proportion of elements of a population containing a characteristic or attribute analysis. This proportion is called the frequency of occurrence or percentage of deviation and is equal to the ratio of elements containing attribute specific and total number of population elements. WeightRomanian Statistical Review nr. 5 / 2010Statistics and Audit deviations in a sample are determined to calculate an estimate of the proportion of the total population deviations.Risk associated with sampling - refers to a sample selection which can not be representative of the population tested. In other words, the sample itself may contain material errors or deviations from the line. However, issuing a conclusion based on a sample may be different from the conclusion which would be reached if the entire population would be subject to audit.Types of risk associated with sampling:Controls are more effective than they actually are or that there are not significant errors when they exist - which means an inappropriate audit opinion. Controls are less effective than they actually are that there are significant errors when in fact they are not - this calls for additional activities to establish that initial conclusions were incorrect.Attributes testing - the auditor should be defining the characteristics to test and conditions for misconduct. Attributes testing will make when required objective statistical projections on various characteristics of the population. The auditor may decide to select items from a population based on its knowledge about the entity and its environment control based on risk analysis and the specific characteristics of the population to be tested.Population is the mass of data on which the auditor wishes to generalize the findings obtained on a sample. Population will be defined compliance audit objectives and will be complete and consistent, because results of the sample can be designed only for the population from which the sample was selected.Sampling unit - a unit of sampling may be, for example, an invoice, an entry or a line item. Each sample unit is an element of the population. The auditor will define the sampling unit based on its compliance with the objectives of audit tests.Sample size - to determine the sample size should be considered whether sampling risk is reduced to an acceptable minimum level. Sample size is affected by the risk associated with sampling that the auditor is willing to accept it. The risk that the auditor is willing to accept lower, the sample will be higher.Error - for detailed testing, the auditor should project monetary errors found in the sample population and should take into account the projected error on the specific objective of the audit and other audit areas. The auditor projects the total error on the population to get a broad perspective on the size of the error and comparing it with tolerable error.For detailed testing, tolerable error is tolerable and misrepresentations Revista Română de Statistică nr. 5 / 2010Statistics and Auditwill be a value less than or equal to materiality used by the auditor for the individual classes of transactions or balances audited. If a class of transactions or account balances has been divided into layers error is designed separately for each layer. Design errors and inconsistent errors for each stratum are then combined when considering the possible effect on the total classes of transactions and account balances.Evaluation of sample results - the auditor should evaluate the sample results to determine whether assessing relevant characteristics of the population is confirmed or needs to be revised.When testing controls, an unexpectedly high rate of sample error may lead to an increase in the risk assessment of significant misrepresentation unless it obtained additional audit evidence to support the initial assessment. For control tests, an error is a deviation from the performance of control procedures prescribed. The auditor should obtain evidence about the nature and extent of any significant changes in internal control system, including the staff establishment.If significant changes occur, the auditor should review the understanding of internal control environment and consider testing the controls changed. Alternatively, the auditor may consider performing substantive analytical procedures or tests of details covering the audit period.In some cases, the auditor might not need to wait until the end audit to form a conclusion about the effectiveness of operational control, to support the control risk assessment. In this case, the auditor might decide to modify the planned substantive tests accordingly.If testing details, an unexpectedly large amount of error in a sample may cause the auditor to believe that a class of transactions or account balances is given significantly wrong in the absence of additional audit evidence to show that there are not material misrepresentations.When the best estimate of error is very close to the tolerable error, the auditor recognizes the risk that another sample have different best estimate that could exceed the tolerable error.ConclusionsFollowing analysis of sampling methods conclude that all methods have advantages and disadvantages. But the auditor is important in choosing the sampling method is based on professional judgment and take into account the cost / benefit ratio. Thus, if a sampling method proves to be costly auditor should seek the most efficient method in view of the main and specific objectives of the audit.Romanian Statistical Review nr. 5 / 2010Statistics and Audit The auditor should evaluate the sample results to determine whether the preliminary assessment of relevant characteristics of the population must be confirmed or revised. If the evaluation sample results indicate that the relevant characteristics of the population needs assessment review, the auditor may: require management to investigate identified errors and likelihood of future errors and make necessary adjustments to change the nature, timing and extent of further procedures to take into account the effect on the audit report.Selective bibliography:[1] Law no. 672/2002 updated, on public internal audit[2] Arens, A şi Loebbecke J - Controve …Audit– An integrate approach”, 8th edition, Arc Publishing House[3] ISA 530 - Financial Audit 2008 - International Standards on Auditing, IRECSON Publishing House, 2009- Dictionary of macroeconomics, Ed C.H. Beck, Bucharest, 2008Revista Română de Statistică nr. 5 / 2010Statistics and Audit摘要美国公司的规模迅速增加,从第二十世纪初创造了必要的审计程序,根据选定的部分总人口的审计,以获得可靠的审计证据,以描述整个人口组成的帐户余额或类别的交易。
英文文献pdf翻译成中文
对于将英文文献PDF翻译成中文,有几种常见的方法可以实现。
首先,你可以使用在线翻译工具,如Google翻译或百度翻译,直接
上传PDF文件并选择需要翻译的语言。
这些工具可以快速将整个文
档翻译成中文,但需要注意的是,由于自动翻译的限制,可能会出
现一些翻译不准确或不通顺的情况,特别是对于专业术语或复杂句子。
其次,你也可以雇佣专业的翻译人员或翻译公司来完成这项任务。
他们可以提供更准确、流畅的翻译,尤其是对于专业领域的文献,这种方式会更可靠。
然而,这需要一定的成本和时间,因为翻
译人员需要逐字逐句地进行翻译,并且可能需要进行专业术语的翻
译和校对。
另外,如果你自己对英文和中文都比较熟悉,也可以考虑自行
翻译。
这种方式可以确保翻译的准确性和流畅性,但需要花费较多
的时间和精力。
无论采用哪种方式,翻译文献需要保证准确性和完整性,尤其
是对于学术文献或专业领域的文献。
希望这些信息能够帮助你找到合适的方法来将英文文献PDF翻译成中文。
Adult【成年人】Aged【老年人】Aged, 80 and over【老年人, 80以上】Catheterization, Central Venous/*instrumentation/methods【*导管插入术, 中心静脉/*仪器/方法】Cost-Benefit Analysis【费用效益分析】Equipment Design【设备设计】Equipment Failure【设备失效】Equipment Safety【设备安全性】Female【女(雌)性】Humans【人类】Infusion Pumps, Implantable/adverse effects/*economics【*输注泵, 植入型/副作用/*经济学】Male【男(雄)性】Middle Aged【中年人】Neoplasms/*drug therapy/pathology【*肿瘤/*药物疗法/病理学】Probability【概率】Prospective Studies【前瞻性研究】Risk Assessment【危险性评估】Sensitivity and Specificity【敏感性与特异性】Treatment Outcome【治疗结果】Vascular Patency【血管未闭】Venous Thrombosis/prevention & control【静脉血栓形成】Adolescent【青少年】Adult【成年人】Aged【老年人】Aged, 80 andover【老年人, 80以上】AntineoplasticAgents/*administration& dosage【*抗肿瘤药】*Catheters,Indwelling/adverseeffects/economics【*导管, 留置/副作用/经济学】Female【女(雌)性】Humans【人类】*Infusion Pumps,Implantable/adverse。
英文文献全文翻译全文共四篇示例,供读者参考第一篇示例:LeGuin, Ursula K. (December 18, 2002). "Dancing at the Edge of the World: Thoughts on Words, Women, Places".《世界边缘的舞蹈:关于语言、女性和地方的思考》Introduction:In "Dancing at the Edge of the World," Ursula K. LeGuin explores the intersection of language, women, and places. She writes about the power of words, the role of women in society, and the importance of our connection to the places we inhabit. Through a series of essays, LeGuin invites readers to think critically about these topics and consider how they shape our understanding of the world.Chapter 1: LanguageConclusion:第二篇示例:IntroductionEnglish literature translation is an important field in the study of language and culture. The translation of English literature involves not only the linguistic translation of words or sentences but also the transfer of cultural meaning and emotional resonance. This article will discuss the challenges and techniques of translating English literature, as well as the importance of preserving the original author's voice and style in the translated text.Challenges in translating English literature第三篇示例:Title: The Importance of Translation of Full English TextsTranslation plays a crucial role in bringing different languages and cultures together. More specifically, translating full English texts into different languages allows for access to valuable information and insights that may otherwise be inaccessible to those who do not speak English. In this article, we will explore the importance of translating full English texts and the benefits it brings.第四篇示例:Abstract: This article discusses the importance of translating English literature and the challenges translators face when putting together a full-text translation. It highlights the skills and knowledge needed to accurately convey the meaning and tone of the original text while preserving its cultural and literary nuances. Through a detailed analysis of the translation process, this article emphasizes the crucial role translators play in bridging the gap between languages and making English literature accessible to a global audience.IntroductionEnglish literature is a rich and diverse field encompassing a wide range of genres, styles, and themes. From classic works by Shakespeare and Dickens to contemporary novels by authors like J.K. Rowling and Philip Pullman, English literature offers something for everyone. However, for non-English speakers, accessing and understanding these works can be a challenge. This is where translation comes in.Translation is the process of rendering a text from one language into another, while striving to preserve the original meaning, tone, and style of the original work. Translating afull-length English text requires a deep understanding of both languages, as well as a keen awareness of the cultural andhistorical context in which the work was written. Additionally, translators must possess strong writing skills in order to convey the beauty and complexity of the original text in a new language.Challenges of Full-text TranslationTranslating a full-length English text poses several challenges for translators. One of the most significant challenges is capturing the nuances and subtleties of the original work. English literature is known for its rich and layered language, with intricate wordplay, metaphors, and symbolism that can be difficult to convey in another language. Translators must carefully consider each word and phrase in order to accurately convey the author's intended meaning.Another challenge of full-text translation is maintaining the author's unique voice and style. Each writer has a distinct way of expressing themselves, and a good translator must be able to replicate this voice in the translated text. This requires a deep understanding of the author's writing style, as well as the ability to adapt it to the conventions of the target language.Additionally, translators must be mindful of the cultural and historical context of the original work. English literature is deeply rooted in the history and traditions of the English-speaking world, and translators must be aware of these influences in orderto accurately convey the author's intended message. This requires thorough research and a nuanced understanding of the social, political, and economic factors that shaped the work.Skills and Knowledge RequiredTo successfully translate a full-length English text, translators must possess a wide range of skills and knowledge. First and foremost, translators must be fluent in both the source language (English) and the target language. This includes a strong grasp of grammar, syntax, and vocabulary in both languages, as well as an understanding of the cultural and historical context of the works being translated.Translators must also have a keen eye for detail and a meticulous approach to their work. Every word, sentence, and paragraph must be carefully considered and translated with precision in order to accurately convey the meaning of the original text. This requires strong analytical skills and a deep understanding of the nuances and complexities of language.Furthermore, translators must possess strong writing skills in order to craft a compelling and engaging translation. Translating a full-length English text is not simply a matter of substituting one word for another; it requires creativity, imagination, and a deep appreciation for the beauty of language. Translators mustbe able to capture the rhythm, cadence, and tone of the original work in their translation, while also adapting it to the conventions of the target language.ConclusionIn conclusion, translating a full-length English text is a complex and challenging task that requires a high level of skill, knowledge, and creativity. Translators must possess a deep understanding of both the source and target languages, as well as the cultural and historical context of the work being translated. Through their careful and meticulous work, translators play a crucial role in making English literature accessible to a global audience, bridging the gap between languages and cultures. By preserving the beauty and complexity of the original text in their translations, translators enrich our understanding of literature and bring the works of English authors to readers around the world.。
Characterization of production of Paclitaxel and related Taxanes in Taxus Cuspidata Densiformis suspension cultures by LC,LC/MS, and LC/MS/MSCHAPTER THEREPLANT TISSUE CULTUREⅠ. Potential of Plant cell Culture for Taxane ProductionSeveral alternative sources of paclitaxel have been identified and are currently the subjects of considerable investigation worldwide. These include the total synthesis and biosynthesis of paclitaxel, the agriculture supply of taxoids from needles of Taxus species, hemisynthesis (the attachment of a side chain to biogenetic precursors of paclitaxel such as baccatin Ⅲ or 10-deacetylbaccatin Ⅲ), fungus production, and the production of taxoids by cell and tissue culture. This reciew will concentrate only on the latter possibility.Plant tissue culture is one approach under investigation to provide large amounts and a stable supply of this compound exhibiting antineoplastic activity. A process to produce paclitaxel or paclitaxel-like compounds in cell culture has already been parented. The development of fast growing cell lines capable of producing paclitaxel would not only solve the limitations in paclitaxel supplies presently needed for clinical use, but would also help conserve the large number of trees that need to be harvested in order to isolate it. Currently, scientists and researchers have been successful in initiating fast plant growth but with limited paclitaxel production or vice versa. Therefore, it is the objective of researchers to find a method that will promote fast plant growth and also produce a large amount of paclitaxel at the same time.Ⅱ. Factors Influencing Growth Paclitaxel ContentA.Choice of Media for GrowthGamborg's (B5) and Murashige & Skoog's (MS) media seem to be superior for callus growth compared to White's (WP) medium. The major difference between these two media is that the MS medium contains 40 mM nitrate and 20mM ammonium, compared to 25mM nitrate and 2mM ammonium. Many researchers have selected the B5 medium over the MS medium for all subsequent studies, although they achieve similar results.Gamborg's B5 media was used throughout our experiments for initiation of callus cultures and suspension cultures due to successful published results. It was supplemented with 2% sucrose, 2 g/L casein hydrolysate, 2.4 mg/L picloram, and 1.8 mg/L α-naphthalene acetic acid. Agar (8 g/L) was used for solid cultures.B. Initiation of Callus CulturesPrevious work indicated that bark explants seem to be the most useful for establishing callus. The age of the tree did not appear to affect the ability to initiate callus when comparing both young and old tree materials grown on Gamborg's B5 medium supplemented with 1-2 mg/L of 2,4-dichlorophenoxyacetic acid. Callus cultures initiated and maintained in total darkness were generally pale-yellow to light brown in color. This resulted in sufficient masses of friable callus necessary for subculture within 3-4 weeks. However, the growth rate can decline substantially following the initial subculture and result in very slow-growing, brown-colored clumps of callus. It has been presumed that these brown-colored exudates are phenolic in nature and can eventually lead to cell death. This common phenomenon is totally random and unpredictable. Once this phenomenon has been triggered, the cells could not be saved by placing them in fresh media. However, adding polyvinylpyrrolidone to the culture media can help keep the cells alive and growing. Our experience with callus initiationwas similar to those studies.Our studies have found that callus which initiated early (usually within 2 weeks ) frequently did not proliferate when subcultured and turned brown and necrotic. In contrast, calli which developed from 4 weeks to 4 months after explants were fist placed on initiation media were able to be continuously subcultured when transferred at 1-2 month intervals. The presence of the survival of callus after subsequent subculturing. The relationship between paclitaxel concentration and callus initiation, however, has not been clarified.C. Effect of SugarSucrose is the preferred carbon source for growth in plant cell cultures, although the presence of more rapidly metabolized sugar such as glucose favors fast growth. Other sugars such as lactose, galactose, glucose, and fructose also support cell growth to some extent. On the other hand, sugar alcohols such as mannitol and sorbital which are generally used to raise the sugars added play a major role in the production of paclitaxel. In general, raising the initial sugar levels lead to an increase of secondary metabolite production. High initial levels of sugar increase the osmotic potential, although the role of osmotic pressure on the synthesis of secondary metabolites is not cleat. Kim and colleagues have shown that the highest level of paclitaxel was obtained with fructosel. The optimum concentration of each sugar for paclitaxel production was found to be the same at 6% in all cases. Wickremesinhe and Arteca have provided additional support that fructose is the most effective for paclitaxel production. However, other combinations of sugars such as sucrose combined with glucose also increased paclitaxel production.The presence of extracellular invertase activity and rapid extracellular sucrose hydrolysis has been observed in many cell cultures. These reports suggest that cells secrete or possess on their surface excess amounts of invertase, which result in the hydrolysis of sucrose at a much faster rate. The hydrolysis of sucrose coupled with the rapid utilization of fructose in the medium during the latter period of cell growth. This period of increased fructose availability coincided with the faster growth phase of the cells.D. Effect of Picloram and Methyl JasmonatePicloram (4-amino-3.5.6-trichloropicolinic acid) increases growth rate while methyl jasmonate has been reported to be an effective elicitor in the production of paclitaxel and other taxanes. However, little is known about the mechanisms or pathways that stimulate these secondary metabolites.Picloram had been used by Furmanowa and co-workers and Ketchum and Gibson but no details on the effect of picloram on growth rates were given. Furmanowa and hid colleagues observed growth of callus both in the presence and absence of light. The callus grew best in the dark showing a 9.3 fold increase, whereas there was only a 2-4 fold increase in the presence of light. Without picloram, callus growth was 0.9 fold. Unfortunately,this auxin had no effect on taxane production and the high callus growth rate was very unstable.Jasmonates exhibit various morphological and physiological activities when applied exogenously to plants. They induce transcriptional activation of genes involved in the formation of secondary metabolites. Methyl jasmonate was shown to stimulate paclitaxel and cephalomannine (taxane derivative) production in callus and suspension cultures. However, taxane production was best with White's medium compared to Gamborg's B5 medium. This may be due to the reduced concentration of potassium nitrate and a lack of ammonium sulfate with White's medium.E. Effect of Copper Sulfate and Mercuric ChlorideMetal ions have shown to play significant roles in altering the expression of secondary metabolic pathways in plant cell culture. Secondary metabolites,such as furano-terpenes, have been production by treatment of sweet potato root tissue with mercuric chloride. The results for copper sulfate, however, have not been reported. F. Growth Kinetics and Paclitaxel ProductionLow yields of paclitaxel may be attributed to the kinetics of taxane production that is not fully understood. Many reports stated inconclusive results on the kinetics of taxane production. More studies are needed in order to quantitate the taxane production. According to Nett-Fetto, the maximum instantaneous rate of paclitaxel production occurred at the third week upon further incubation. The paclitaxel level either declined or was not expected to increase upon further incubation. Paclitaxel production was very sensitive to slight variations in culture conditions. Due to this sensitivity, cell maintenance conditions, especially initial cell density, length of subculture interval, and temperature must be maintained as possible.Recently, Byun and co-workers have made a very detailed study on the kinetics of cell growth and taxane production. In their investigation, it was observed that the highest cell weight occurred at day 7 after inoculation. Similarly, the maximum concentration for 10-deacetyl baccatin Ⅲ and baccatin Ⅲ were detected at days 5 and 7, respectively. This result indicated that they are metabolic intermediates of paclitaxel. However, paclitaxel's maximum concentration was detected at day 22 but gradually declined. Byun and his colleagues suggested that paxlitaxel could be a metabolic intermediate like 10-deacetyl baccatin Ⅲ and baccatin Ⅲ or that pacliltaxel could be decomposed due to cellular morphological changes or DNA degradation characteristic of cell death.Pedtchanker's group also studied the kinetics of paclitaxel production by comparing the suspension cultures in shake flasks and Wilson-type reactors where bubbled air provided agitation and mixing. It was concluded that these cultures of Taxus cuspidata produced high levels of paclitaxel within three weeks (1.1 mg/L per day ). It was also determined that both cultures of the shake flask and Wilson-type reactor produced similar paclitaxel content. However, the Wilson-type reactor had a more rapid uptake of the nutrients (i.e. sugars, phosphate, calcium, and nitrate). This was probably due to the presence of the growth ring in the Wilson reactor. Therefor, the growth rate for the cultures from the Wilson reactor was only 135 mg./L while the shake flasks grew to 310 mg/L in three weeks.In retrospect, strictly controlled culture conditions are essential to consistent production and yield. Slight alterations in media formulations can have significant effects upon the physiology of cells, thereby affecting growth and product formation. All of the manipulations that affect growth and production of plant cells must be carefully integrated and controlled in order to maintain cell viability and stability.利用LC,LC/MS和LC/MS/MS悬浮培养生产紫杉醇及邓西佛米斯红豆杉中相关紫杉醇类的特征描述第三章植物组织培养Ⅰ.利用植物细胞培养生产紫杉的可能性紫杉醇的几个备选的来源已被确定,而且目前是全球大量调查的主题。
Geotextile reinforced by soft soil1. IntroductionGeotextile known, it has high tensile strength, durability, corrosion resistance, texture, flexibility, combined with good sand, to form reinforced composite foundation, effectively increase the shear strength , tensile properties, and enhance the integrity and continuity of soil. Strengthening mechanism for the early 60's in the 20th century, Henri Vidal on the use of triaxial tests found a small amount of fiber in the sand, the soil shear strength can improve the image of more than 4 times in recent years, China's rock Laboratory workers also proved in the reinforced sand can effectively improve the soil's bearing capacity, reduce the vertical ground settlement, effectively overcome the poor soil and continuity of overall poor performance. As with the above properties of reinforced soil and the characteristics of its low price, so the project has broad application prospects.2.1 Project OverviewThe proposed retaining wall using rubble retaining wall of gravity, the wall is 6 meters high, the bearing capacity of foundation soil required to 250kPa, while the basement geology from the top down as follows: ①clay to a thickness of 0.7 to 2 meters saturated, soft plastic; ② muddy soil, about 22 - 24 meters thick, saturated, mainly plastic flow, local soft plastic; ③ sand layer to a thickness of 5 to 10 meters, containing silty soil and organic matter, saturated, slightly wet; ④ gravel layer, the thickness of the uneven distribution points, about 0 to 2.2 meters, slightly dense; ⑤ weathered sandstone. Including clay and silty soil bearing capacity is 70kPa, obviously do foundation reinforcement.2.2 Enhanced Treatment of reinforced foundation cushion Reinforcement replacement method can be used for sand and gravel used forsoil treatment, but due to loose bedding, based on past experience, witha gravel mat to treat a large settlement of the foundation always exist, even the characteristics of poor, often resulting in cracks in the superstructure, differential settlement of the image, this works for6-meter-high rubble retaining walls, height and large, and because the walls are 3 meters high wall, if there is differential settlement of retaining walls, cracks, will result in more serious consequences and thus should be used on the cushion reinforcement through economic and technical analysis, decide on the sand and gravel stratum were reinforced hardening. Reinforcement treatment method: first the design elevation and the basement excavation to 200mm thick layer of gravel bedding, and then capped with a layer of geotextile, and then in the thick sand and gravel on the 200, after leveling with the yellow sand using roller compaction; second with loaded bags of sand and gravel laying of geotextile, the gap filled with slag, geotextile bags capped 100 thick gravel, roller compaction. Its on repeat laying geotextile → → compacted gravel, until the design thickness of the cushion, the bridge is 1 m thick cushion, a total of 4 layers of geotextile, two bags of sand.This method works fast, simple machine, investment, after years of use, that reinforce good effect, building and construction units are satisfied.3 ExperienceTo achieve the reinforced soil reinforcement effect, must be reinforced earth construction technology, construction strict quality control: 1, geotextile should increase the initial pre-stress, and its end should be a reliable anchor to play the tensile strength of geotextile, anchoring more firmly, more capacity to improve, the foundation of the stress distribution more uniform, geotextile side Ministry of fixed length by laying end to ensure the fold, the folded end wrapped sand to increase its bond strength to ensure that the use will not be pulled out duringthe period.Second, the construction process have a significant effect on the reinforcement effect, the construction should be as soon as possible so that geotextile in tension, tensile strength geotextile can be played only when the deformation, so do not allow construction of geotextile crease occurs, the earth Fabric tension leveling as much as possible. Geotextile in order to have enough by the early Dutch strain, according to the following procedure works: ① laying geotextile; ② leveled the tension at both ends; both ends of the folded package gravel and sand filling at both ends; ③ center fill sand; ④ 2 higher end of sand; ⑤ Finally, the center of sand filling. Click here to enable the construction method of forming corrugated geotextile being stretched as soon as possible, to play a role in the early loaded.Third, the construction of geotextile-reinforced cushion should the level of shop using geotextile geotextile and laying of gravel bags cushion the turn to play bag cushion integrated turn out good, flexural rigidity, and dispersion of good and peace bedding layer of the overall continuity of good advantages.4 ConclusionGeotextile reinforced by soft soil is an effective, economical, safe, reliable, simple method, but the literature describes only qualitative, experience more components, yet the lack of rigorous The theoretical formula, reliable test data to be adequate, these are yet to be theoretical workers and the general engineering and technical personnel continue to explore.土工织物加筋垫层加固软土地基1. 引言土工织物又称土工聚合物,它具有高抗拉强度,耐久性、耐腐蚀性,质地柔韧,能与砂土很好地结合,组合成加筋土复合地基,有效地提高土的抗剪强度、抗拉性能,增强土体的整体性和连续性。
你值得拥有的八大英文文献翻译神器不管是做科研还是写SCI论文,开始都需要阅读大量的文献,做课题至少查阅600篇,粗看300篇,细看100篇,研读50篇,在看到一叠叠论文后,由于语言问题,往往会觉得无从下手,下面分享几款常用的文献翻译神器。
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毕业设计(论文)译文题目名称:院系名称:班级:学号:学生姓名:指导教师:年月铝-硅-镁铸造合金的凝固、沉淀性能镁成份对于未做处理的Al-7Si-Mg铸造合金和加锶(Sr)处理的Al-7Si-Mg铸造合金的凝固和沉淀性能的影响已经在各种凝固速率下做过实验。
实验采用了冷却曲线分析仪,差式扫描量热法,以及光学显微镜和电子显微镜。
镁成份集中从0.3wt%(质量分数)到0.7wt%。
结果表明:增加镁含量或提高冷却速率都会降低液相线和铝-硅共晶转变温度。
这些合金的熔化潜热很大程度上依赖于硅的存在水平,但是未发现对于镁成份的依赖。
在差式扫描量热法条件下观察到的凝固的反应被识别,并注意到三元共晶反应L→Al+Si+Mg2Si只有在镁水平在0.6%和更高水平下才能被观察到。
在凝固过程中那些次生相可以被识别。
它们对于溶液温度的热处理反应可以被检测出来。
通常增加镁含量可以加强沉淀强度。
但是,当镁水平增加到0.5wt%以上,镁对于屈服强度的增加就不明显了。
这与溶化的镁含量和释放的能量有关。
――2001年克吕韦尔学术出版社的一篇文献1.简介铝-硅-镁铸造合金越来越多的应用于汽车、航空工业关键结构件。
这是由于这种铸造合金在热处理条件下表现出来的优良的铸造性能和抗腐蚀性,尤其是良好的机械性能。
在这种铸造合金中,镁被加入并通过形成镁-硅合金来诱发时效硬化。
但是,增加镁含量会降低材料的延展性和断裂韧性。
这说明,当达到铝基时效硬化时,可能会影响到显微结构,特别是脆相的结构和形态。
这已经被一些优秀的出版文献所证实。
Back等人研究了三种铝-硅-镁铸造合金(A356.1,A3562.2和A357.2)讨论了这三种合金在三种不同冷却曲线下的凝固特点。
实验得到,添加镁可以改变凝固顺序和金属间化合物Fe-bearing 的类型。
但是很难总结镁的实际效应,因为镁含量高于0.56%会包含少量铍。
铍对铁的形为有强烈的影响。
Granger等人在他们的实验中发现合A357.0有一个包含镁的不溶相Fe-bearing,而合金A357.2却没有这种情况。
Tan等人也得到了相似的结果。
Joenoes 和Gruzleski在一个固定的冷却速率下研究了镁成份在一种合成合金中的影响。
他们发现极少量的镁就能改变硅相的形态和晶粒大小。
在改进合金中,镁可以结合锶形成一种复杂的金属间化合物Mg2SrAl4Si。
这种化合物被认为先于共晶转变形成。
尽管镁成份对于硅共晶颗粒有影响已经在一些文献中被认识,但是还没有形成一种添加镁含量的最优方案。
镁影响次元相的形成和分布的原理还没有被很好的理解,特别是对于中间相Fe-bearing。
最近的一次实验中为了解决这个问题,Mackay 和Gruzleski对于未做处理的Al-7.2%Si合金研究了冷却曲线特点和铁、镁的相互关系。
他们指出镁水平低于0.5wt%时,仅仅凝固反应(包括在冷却曲线中可以被认识镁基相)发生三元反应形成铝、硅、镁二硅,开始温度大约在555摄氏度。
当镁水平高于0.5wt%时(除非铁含量非常高),一个单独的反应被发现。
该反应开始在10摄氏度以上,形成的Al8Mg3FeSi6会附加在上面的三种相上。
就在最近,Taylor等人详细研究了镁对于铸造合金固相热处理的影响并指出了每一个次生相的相对体积分数。
只考虑到镁水平,在镁体积分数在1%左右时,毛坏铸件中可以发现π相。
Β相和Mg2Si一般都小于0.1vol%,在镁达到0.7wt%时Mg2Si能够增加到0.2vol%。
固溶热处理可以防止在所有组成成份中产生大量的镁二硅,但是只有在镁含量在0.3或0.4wt%时才能阻止产生大量π相。
此次工作旨在评估镁在不同冷却速率下对于商业铝硅镁铸件凝固、沉淀性能的影响并为镁添加最佳方案提供一个基础。
2实验过程2.1材料未做处理的商业Al-7%Si-0.3 ∼ 0.7%Mg 铸造合金(601和603,按美国命名法相当于A356.0A357.0)被使用。
处理过的合金(对上面合金溶化并在排气前加入Al-10%Sr合金)。
这些合金的化学成份都被表示在表1中。
标有下标“um”表示未做处理,标有下标“Sr”表示加锶处理的合金。
冷砂模铸件的样品会产生枝晶叉间隔,其他文献有详细描述。
实验用Al-7%Si合金和商业Al-12%Si合金在差式扫描量热法测量下用做参考。
2.2热分析对加锶处理的601和603合金进行传统冷却曲线分析,这些合金是用直径50mm的圆柱砂型和金属型模具铸造。
冷却曲线的获得是通过在模具中心和边缘放置两个k型热电偶和记录温度改变,以此作为在凝固过程中的一个数据采集系统功能。
这些热电偶被放置在距模具底部相同距离(25mm)以保证记录全部热量。
所有实验的浇铸温度控制在745摄氏度。
用埃尔默差式扫描量热仪对所有试样用差式扫描量热法进行测量。
根据温度、扫描速率、测试类型,试样一般采用直径约为4mm的磁盘,重10mg到25mg。
潜热测量在不同冷却速率下,从每分钟2摄氏度到每分钟60摄氏度。
对纯从工铝进行温度校正,用每千克397Kj对铝溶化热进行校正。
能量刻度要有良好的线性范围,并在实验中反复校正。
设一个空盘作为一个参考盘。
对于凝固和溶化过程中的相变研究,差式扫描量热仪应用于500~650摄氏度,扫描速率设定为每分钟10摄氏度。
相同重量的高纯铝磁盘被放置在参考盘里做为参考。
对于沉淀特点,对T4热处理样品进行DSC热分析,加热速率为每分钟30摄氏度,做DSC热分析图从50~500摄氏度。
这次热处理在540摄氏度下保温20小时,之后水冷至室温。
淬火样品也可用DSC设备,如果没有条件,可以放置在-10摄氏度的冰箱内。
淬火和DSC测量在室温下的总时间不能超过10分钟。
任何样品在冰箱的总时间不超过30分钟。
DSC设备的温度报告对设计很重要。
样品放在一个有温度检测的盘里。
含铍的电阻温度计记录温度,并被设备所记录。
另一个类似的加热器提供一个参考并显示一两个系统之间的区别。
简单的冷对曲线不能直接测量样品的温度。
样品和温度传感器之间总是会有一个温度滞后,这种温度滞后会降低传热质量以及样品和传感器之间的热阻抗。
在常规操作下只要热通量速率不发生改变,校正就运行的非常准确。
但是热通量明显低于运行状态时,滞后温度会显著降低。
因此在凝固过程中,当热通量在基线上好几个W/g时,温度变的顺序是可期的。
而且,样品整体有一个温度梯度可以表示反应温度范围。
随着能量的吸收、释放速率的降低,这种效果会变得更明显。
改变这种效果非常困难,还没有尝试结果。
起始温度和范围应该被考虑。
2.3显微分析所有进行金相分析的样品使用用标准技术,用商业二氧化硅泥浆(司特尔OP-U)抛光,最终得到1微米的菱形光滑试样。
对抛光样品进行铝基和Fe-bearing中间合金相的化学组成和成份检测。
配备有日本6400F的扫描电镜的能量分散x射线能谱仪(EDX)用于定性分析,配备有日本JXA-8800的扫描电镜的能量分散x射线能谱仪(EDX)用于定量分析。
原始样品用作一个对照标准。
3.结果3.1冷却曲线图表1显示了合金601和603不同镁含量的冷却曲线以及凝固的冷却速率。
为了便于对比,图表1中标明了冷却速率。
温度与时间的比值表示了枝晶生长阶段的生长速率。
可以看出合金601/603的凝固顺序包含了三种相变反应:第一,铝树枝晶的形成与冷却曲线中生成物的第一个极点相一致;第二,主要共晶反应,代表第二个极点;第三,三元或四元共晶反应,如Mg2Si或Fe-bearing中间合金,这在冷却曲线中不能被观察出来,特别是铸造时采用较高的冷却速率。
从冷却曲线分析中可以看出镁成份和凝固时的冷却速率对溶液液相线、共晶转变温度的影响,并在图表2中表示出来了。
即降低镁含量和冷却速率会降低液相线和二元共晶反应。
这里不会提及到铝硅共晶反应,但是液相线附近富铝、富硅的温度范围与铝硅共晶相比较相似。
当然,次要元素也会对相变和固相结构有额外不同程度的影响,并使固相比残余溶料更贫镁和铁。
3.2显微结构铸态组织出现了预期的次生相(π–AlFeMgSi, β-AlFeSi and Mg2Si),不同程度上取决于镁的含量。
铸态条件下的π相是整个组成范围内的主导相。
但是随着镁水平的降低,Mg2Si的比例也会下降。
图表3显示了采用缓慢凝固的调高镁603合金的散射电子扫描电镜图像。
从图中可以看出π相的生长通常与β相颗粒比较相关。
图表4对进行过时效处理和固溶处理的低镁、高镁合金进行显微分析。
在低镁合金601中的Fe-bearing晶粒大致是β相(Al5FeSi),但是它们以不同的形式存在:毛坯铸件板材(主要是小程度的球化处理);精加工的板材,从图表4中可以看出因为太小而不能进行显微探针分析。
同样也可以发现一种很小的球状颗粒,可能是π -AlFeMgSi,与细小的板材有关。
在高镁合金603中Fe-bearing晶粒主要是π–AlFeMgSi。
Fe-bearing中间合金的数量和尺寸随着镁的降低而降低。
对于T6热处理得到的Fe-bearing中间合金的数量和尺寸在其它文献中已经被研究。
用电子探针分析对毛坯铸件和T6条件的π相进行研究得到了相似的FeMg3Si5,而不是理论得到的Al8FeMg3Si6。
这符合了Simensen以及Rolfsen等人的研究。
Tan等人总结到铝(一定程度上)和镁可以取代π相中的硅。
表2比较了铝基材料在进行T4固溶热处理前后镁和铁的含量。
图表5中对镁在大部分合金中的价值做了划分。
因为在毛坯铸件中不显示显微分析,镁水平只表现出一般的价值取向。
与预测的一样,固溶热处理会降低固溶体中大量的镁。
合金603中镁含量为0.5%,固溶热处理后的基体存在许多的镁,大约为0.49%。
增加镁的量超过0.5%只能增加基体上的少量的镁含量——大约0.5%。
基体上的铁成份非常低,热处理也不能改变。
事实上,数值十分接近极限检测条件下的值,而且微小差异不显著。
图表6图6显示在经过一个小时的固溶热处理的含0.4%镁的两个枝晶上进行的一个电子探针扫描。
在中间部分扫描到了一个π晶粒。
在50µm距离中心一边50µm的地方,镁水平下降到0.37 wt %,但是在另一边镁含量维持在0.41 wt %。
显微结构显示其他π相粒子在−60µm的位置接近硅粒子,而在+ 60µm的位置没有出现类似的结果。
3.3差式扫描热分析图3.3.1凝固特点图表7是一个典型的做锶处理的铸造合金603溶化和凝固的差式扫描热分析图,加热和冷却速率均为每分钟10摄氏度。
图中极点反应了具体的相位变化,极点范围与相变反应成正比。
极限的正峰值是由于加热过程中的共晶反应,负值是由于凝固过程中潜热的降低。
如图表7中显示的,对于高镁合金的加热和冷却过程中有四个极限。