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HAMNO-LCMS-28341-MedChemExpress

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File ..3\Data\20180120\20180120\BIZ2018-120-WYQ5.D Tgt Mass (CHM): Injection Date : 20 Jan 18 3:34 pm +0800 Seq. Line : 82 Sample Name : BIZ2018-120-WYQ5 Location : P2-A-07 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 2 ul

Acq. Method : D:\LCMS03\Data\20180120\20180120\1-POS-3MIN.M

Analysis Method : D:\LCMS03\Data\20180120\20180120\1-POS-3MIN.M

Catalog No : HY-111285 Batch#28341

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min00.511.522.5mAU

010002000 DAD1 A, Sig=214,4 Ref=off

1.4711.789

1.874

min00.511.522.5mAU

0200 DAD1 B, Sig=254,4 Ref=off

1.789

1.874

2.029

min00.511.522.5mV

50 ELS1 A, ELSD Signal

1.856

min00.511.522.510000002000000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.815

min00.511.522.50200000400000600000 Ion 264, MSD1 264,Target Mass 263 +H Positive, EIC=263.7:264.7

1.814

Integration Results for DAD1 A, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|

1.47 0.02 4.08 3.45 0.28 157 1.79 0.02 1036.73 913.07 71.78 264 1.87 0.02 403.52 342.55 27.94 264

Integration Results for DAD1 B, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|

1.79 0.02 582.03 508.74 88.50 264 1.87 0.02 74.76 64.97 11.37 264 2.03 0.02 0.87 0.74 0.13 157

Integration Results for MSD1 TIC, MS File

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|

1.82 0.06 4434636.00 1213398.38 100.00 264MS Report from Instrument: LCMS-03

LCMS-03 1/22/2018 10:49:11 AM SYSTEMPage1 of3Ret. Time: 1.82 <<<< POSITIVE SPECTRA >>>>m/z

1002003004005006007008009000250005000075000100000125000150000175000 ES-API Positive

159.1

105.1

179.1

286.1549.2157.1

265.1264.1MS Report from Instrument: LCMS-03

LCMS-03 1/22/2018 10:49:11 AM SYSTEMPage2 of3 *** End of Report ***MS Report from Instrument: LCMS-03LCMS-03 1/22/2018 10:49:11 AM SYSTEM

Page3 of3

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Pim1_AKK1-IN-1_LCMS_07342_MedChemExpress

Pim1_AKK1-IN-1_LCMS_07342_MedChemExpress

File ..711 2017-07-11 08-08-28\CPK2017-711-07342.D Tgt Mass (CHM): Injection Date : 11 Jul 17 4:38 pm +0800 Seq. Line : 107 Sample Name : CPK2017-711-07342 Location : P1-B-04 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\chem32\1\DATA\20170711\20170711 2017-07-11 08-08-28\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170711\20170711 2017-07-11 08-08-28\1-POS-3MIN.M Catalog No : HY-10371 Batch#07342 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45Cmin0.511.522.5mAU050010001500 DAD1 B, Sig=214,4 Ref=off 1.2281.4081.4541.7481.858min0.511.522.5mAU0200400 DAD1 C, Sig=254,4 Ref=off 1.1211.2281.3851.4541.5611.6281.7191.858min0.511.522.5050000100000150000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.480min0.511.522.50200004000060000 Ion 340.4, MSD1 340.4,Target Mass 339.4 +H Positive, EIC=340.1:341.1 1.4151.4801.5471.6641.7051.8021.8151.9732.0192.2892.3542.3992.4292.4592.623 Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.23 0.02 8.81 7.98 0.63 117 1.41 0.02 5.47 3.75 0.39 117 1.45 0.02 1376.39 978.75 98.10 171 1.75 0.03 4.20 2.44 0.30 117 1.86 0.03 8.17 5.11 0.58 117 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.12 0.06 0.73 0.63 0.08 117 1.23 0.02 6.60 5.99 0.70 117 1.39 0.03 3.20 0.13 0.34 117 1.45 0.02 924.01 659.15 97.46 171 1.56 0.06 1.06 0.31 0.11 117 1.63 0.06 1.06 0.67 0.11 117 1.72 0.06 2.00 0.14 0.21 117 1.86 0.03 9.44 5.66 1.00 117MS Report from Instrument: LCMS-02

Bavachinin_LCMS_18338_MedChemExpress

Bavachinin_LCMS_18338_MedChemExpress

=====================================================================

Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 27Acq. Instrument : HY-LCMS-02 Location : P1-A-08

Injection Date : 10/27/2015 2:19:52 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20151027\20151027 2015-10-27 12-25-50\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 10/27/2015 12:25:50 PM by Yang Qian(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HY-325_10-401RS02.MLast changed : 10/28/2015 10:38:45 AM by Yang Qian(LCMS-02) (modified after loading)Method Info : 10-80A,16MIN Catalog No : HY-N0234 Batch#18338 A-RP-134 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

02004006008001000 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20151027\20151027 2015-10-27 12-25-50\BIZ2015-O27-WJ21.D)

2.391 2.482 2.542 2.659

Ellagic_acid_LCMS_13283_MedChemExpress

Ellagic_acid_LCMS_13283_MedChemExpress

File ..2\1\DATA\20170228\CPK\CPK2017-228-13283-1.D Tgt Mass (EZX): 302.20

Injection Date : 1 Mar 17 8:40 am +0800 Seq. Line : 0 Sample Name : CPK2017-228-13283-1 Location : P1-D-01

Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul

Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No: HY-B0183 Batch#13283 Easy-Access Method: '1-POS-3MIN' 302.20

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min*0.511.522.5mAU

0250500750*DAD1 B, Sig=214,4 Ref=off

0.8711.333

1.472

1.547

min*0.511.522.5mAU

010002000*DAD1 C, Sig=254,4 Ref=off

0.870

1.1161.333

min0.511.522.50100002000030000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

4,5-Dicaffeoylquinic_acid_LCMS_23446_MedChemExpress

4,5-Dicaffeoylquinic_acid_LCMS_23446_MedChemExpress

File ..HEM32\1\DATA\20170208\BIZ\BIZ2017-208-WJ3.D Tgt Mass (EZX): 516.10 Injection Date : 8 Feb 17 9:25 am +0800 Seq. Line : 0 Sample Name : BIZ2017-208-WJ3 Location : P2-C-04 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M

Catalog No : HY-N0058 Batch#23446 Easy-Access Method: '1-POS-3MIN' 516.10

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min*0.511.522.5mAU

0200400600*DAD1 B, Sig=214,4 Ref=off

1.1801.393

2.122

min*0.511.522.5mAU

0200400*DAD1 C, Sig=254,4 Ref=off

1.1821.393

1.652

min0.511.522.510000200003000040000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70