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Y-27632-LCMS-27219-MedChemExpress

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File ..\Data\20171114\20171114-1 1\ZDM4737-004-1.D Tgt Mass (CHM): Injection Date : 14 Nov 17 2:22 pm +0800 Seq. Line : 21 Sample Name : ZDM4737-004-1 Location : P1-F-07 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\LCMS03\Data\20171114\20171114-1 1\1-POS-3MIN.M Analysis Method : D:\LCMS03\Data\20171114\20171114-1 1\1-POS-3MIN.M Catalog No : HY-10071 Batch#27219 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min00.511.522.5mAU

010002000 DAD1 A, Sig=214,4 Ref=off

0.357

0.5011.0291.496

min00.511.522.5mAU

05001000 DAD1 B, Sig=254,4 Ref=off

0.2720.3110.357

0.4650.9911.0601.0901.1141.1351.2421.4961.5401.5781.6051.7911.9322.1062.1482.2352.2592.3032.408

min00.511.522.5mV

50100 ELS1 A, ELSD Signal

0.428

0.619

1.1241.289

min00.511.522.5010000002000000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

0.384

min00.511.522.5-0.1-0.0500.05 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7

Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.36 0.01 758.25 1187.16 98.56 248 0.50 0.01 5.66 6.18 0.74 303 1.03 0.02 2.05 1.69 0.27 147 1.50 0.03 3.36 1.84 0.44 303

Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.27 0.01 2.43 2.85 0.23 303 0.31 0.01 2.99 3.39 0.29 248 0.36 0.01 1022.68 1558.37 98.49 248 0.47 0.01 1.81 2.83 0.17 248 0.99 0.03 1.27 0.61 0.12 147 1.06 0.02 0.20 0.14 0.02 147 1.09 0.01 0.20 0.26 0.02 303 1.11 0.01 0.25 0.40 0.02 303 1.14 0.02 0.95 0.87 0.09 303 1.24 0.01 0.17 0.24 0.02 303MS Report from Instrument: LCMS-03

LCMS-03 11/14/2017 15:09:38 SYSTEMPage1 of4 1.50 0.02 0.31 0.28 0.03 303

1.54 0.02 0.44 0.41 0.04 303 1.58 0.01 0.17 0.21 0.02 303 1.61 0.02 0.43 0.21 0.04 303 1.79 0.02 0.74 0.57 0.07 303

1.93 0.02 0.50 0.28 0.05 303 2.11 0.01 0.25 0.27 0.02 105 2.15 0.02 0.28 0.26 0.03 105 2.23 0.01 0.30 0.32 0.03 105 2.26 0.01 0.04 0.07 0.00 105 2.30 0.03 1.24 0.29 0.12 105 2.41 0.02 0.65 0.47 0.06 105

Integration Results for MSD1 TIC, MS File

RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.38 0.06 7101828.00 1924134.25 100.00 248MS Report from Instrument: LCMS-03

LCMS-03 11/14/2017 15:09:38 SYSTEMPage2 of4Ret. Time: 0.38 <<<< POSITIVE SPECTRA >>>>m/z

100200300400500600700800900050000100000150000200000250000 ES-API Positive

303.1231.1124.7

249.1248.1MS Report from Instrument: LCMS-03

LCMS-03 11/14/2017 15:09:38 SYSTEMPage3 of4 *** End of Report ***MS Report from Instrument: LCMS-03LCMS-03 11/14/2017 15:09:38 SYSTEM

Page4 of4

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Fluralaner_LCMS_25003_MedChemExpress

Fluralaner_LCMS_25003_MedChemExpress

File ..170619 2017-06-19 09-04-59\WW4359-003-1_1.D Tgt Mass (CHM): Injection Date : 19 Jun 17 11:17 am +0800 Seq. Line : 27 Sample Name : WW4359-003-1_1 Location : P2-A-02 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 0.5 ul

Acq. Method : D:\chem32\1\DATA\20170619\20170619 2017-06-19 09-04-59\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\DATA\20170619\20170619 2017-06-19 09-04-59\1-POS-3MIN.M

Catalog No : HY-16973 Batch#25003 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min0.511.522.5mAU

05001000 DAD1 B, Sig=214,4 Ref=off

1.586

1.7472.084

min0.511.522.5mAU

0200400600 DAD1 C, Sig=254,4 Ref=off

1.455

1.482

1.7412.084

min0.511.522.5050000100000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

Fursultiamine_COA_27364_MedChemExpress

Fursultiamine_COA_27364_MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C17H26N4O3S2Molecular Weight:398.54Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.72%Conclusion:The product has been tested and complies with the given specifications.Product Name:FursultiamineCat. No.:HY-B2082CAS No.:804-30-8Batch No.:27364Chemical Name:Formamide,N–[(4–amino–2–methyl–5–pyrimidinyl)methyl]–N–[4–hydroxy–1–methyl–2–[[(tetrahydro–2–furanyl)methyl]dithio]–1–buten–1–yl]–

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852, USA

Avacopan_LCMS_25521_MedChemExpress

Avacopan_LCMS_25521_MedChemExpress

File ..70717 2017-07-17 08-21-57\FSD4462-004-1_0.D Tgt Mass (CHM): Injection Date : 17 Jul 17 10:53 am +0800 Seq. Line : 32 Sample Name : FSD4462-004-1_0 Location : P1-E-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170717\20170717 2017-07-17 08-21-57\1-POS-3MIN.M

Analysis Method : D:\chem32\1\DATA\20170717\20170717 2017-07-17 08-21-57\1-POS-3MIN.M

Catalog No : HY-17627 Batch#25521 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min0.511.522.5mAU

-20-100 DAD1 B, Sig=214,4 Ref=off

min0.511.522.5mAU

-2.502.55 DAD1 C, Sig=254,4 Ref=off

min0.511.522.5200040006000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70 **** NO MS PEAKS INTEGRATED ****

Glecaprevir_COA_27340_MedChemExpress

Glecaprevir_COA_27340_MedChemExpress

Inhibitors, Agonists, Screening Certificate of AnalysisPHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C38H46F4N6O9SMolecular Weight:838.87Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.65%Conclusion:The product has been tested and complies with the given specifications.Product Name:GlecaprevirCat. No.:HY-17634CAS No.:1365970-03-1Batch No.:27340Chemical Name:Cyclopropanecarboxamide,N–[[[(1R,2R)–2–[[4,4–difluoro–4–(3–hydroxy–2–quinoxalinyl)–2–buten–1–yl]oxy]cyclopentyl]oxy]carbonyl]–3–methyl–L–valyl–(4R)–4–hydroxy–L–prolyl–1–amino–2–(difluoromethyl)–N–[(1–methylcyclopropyl)sulfonyl]–, cyclic (1—>2)–ether, (1R,2R)–