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Inauhzin_LCMS_12063_MedChemExpress

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File D:\CHEM32\1\DATA\CPK\CPK2017-216-12063.D Tgt Mass (EZX): 469.60 Injection Date : 16-Feb-17, 15:03:47 Seq. Line : 0 Sample Name : CPK2017-216-12063 Location : P1-E-08 Acq. Operator : GZZ_718 Inj : 0 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\METHODS\SIM-HM-174C_005-H01GI03(0.0.05%TFA).M

Catalog No : HY-15869 Batch#12063 Easy-Access Method: '1-POS-3MIN' 469.60

Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃

min0.511.522.5mAU

05001000 DAD1 B, Sig=214,4 Ref=off

1.523

1.677

1.740

1.933

2.0102.066

2.201

2.439

2.554

min0.511.522.5mAU

05001000 DAD1 C, Sig=254,4 Ref=off

1.610

1.676

1.742

1.930

2.0132.066

2.200

2.298

2.372

2.439

2.572

min0.511.522.50100000200000300000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

2.122

min0.511.522.502000040000 Ion 470.6, MSD1 470.6,Target Mass 469.6 +H Positive, EIC=470.3:471.3

1.678

1.763

1.967

2.0262.113

2.281

2.301

2.347

2.360

2.421

2.455

2.517

2.574

2.600

2.634

2.666

2.684

2.713

2.768

2.797

2.820

2.873

2.893

Integration Results for DAD1 B, Sig=214,4 Ref=off

RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------|

1.52 0.03 2.46 1.48 0.08 274

1.68 0.02 0.84 0.61 0.03 141

1.74 0.02 0.99 0.27 0.03 141

1.93 0.03 4.35 0.31 0.15 233

2.01 0.02 1.55 1.46 0.05 141

2.07 0.03 2930.14 1695.74 98.91 470

2.20 0.03 8.32 4.93 0.28 470

2.44 0.03 11.14 5.86 0.38 233

2.55 0.03 2.65 0.64 0.09 141

Integration Results for DAD1 C, Sig=254,4 Ref=off

RetTim Width Area Height Area% MS(+)

|-------|--------|--------------|--------------|--------|------|

1.61 0.05 1.75 0.64 0.07 141

1.68 0.03 0.65 0.41 0.03 141

1.74 0.03 1.59 0.18 0.07 141

1.93 0.03 2.47 0.04 0.10 233

2.01 0.02 2.05 1.59 0.09 141MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 2/16/2017 3:26:52 PM GZZ_718Page 1 of 3 2.07 0.03 2333.48 1343.41 98.62 470

2.20 0.03 9.39 4.51 0.40 470 2.30 0.02 1.03 0.71 0.04 141 2.37 0.03 2.82 0.40 0.12 141 2.44 0.03 7.52 3.81 0.32 233

2.57 0.05 3.47 0.96 0.15 141MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 2/16/2017 3:26:52 PM GZZ_718Page 2 of 3Ret. Time: 2.12 <<<< POSITIVE SPECTRA >>>>

m/z200300400500600700800900020000400006000080000 ES-API Positive

472.1 470.1MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 2/16/2017 3:26:52 PM GZZ_718Page 3 of 3

合集下载

MOZ-IN-3-COA-29367-MedChemExpress

MOZ-IN-3-COA-29367-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C20H17FN2O3SMolecular Weight:384.42Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structureHPLC:Consistent with structurePurity (LCMS):99.70%Conclusion:The product has been tested and complies with the given specifications.Product Name:MOZ-IN-3Cat. No.:HY-102060CAS No.:2055397-18-5Batch No.:29367Chemical Name:[1,1'-Biphenyl]-3-carboxylic acid, 4-fluoro-5-methyl-, 2-(phenylsulfonyl)hydrazide

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

Olaparib_LCMS_15156_MedChemExpress

Olaparib_LCMS_15156_MedChemExpress

File ..0150303 2015-03-03 09-16-07\WYF2560-003-1.D Tgt Mass (CHM): Injection Date : 3 Mar 15 1:53 pm +0800 Seq. Line : 39 Sample Name : WYF2560-003-1 Location : Vial 28 Acq. Operator : Li Shan(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul

Acq. Method : D:\Aglient 1260\Data\20150303\20150303 2015-03-03 09-16-07\100-1000MS+3MIN( Analysis Method : D:\AGLIENT 1260\METHOD\HM-342_52A-H01P-35MIN(RP-HPLC).M Catalog No : HY-10162 Batch#15156 A-RP-32 Method Info : HPLC

min0.511.522.53mAU

0500100015002000 DAD1 B, Sig=214,4 Ref=off 1.521

1.6721.7691.985

min0.511.522.53mAU

05001000 DAD1 C, Sig=254,4 Ref=off

Area: 4602.35

Area: 1.21347 Area: 12.5685 Area: 2.610361.521

1.6721.7702.154

min0.511.522.530100000200000300000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 501.523

min0.511.522.53-0.1-0.0500.05 Ion 0, MSD1 0,Target Mass 0 Positive, EIC=-0.30:0.70

Carbendazim_LCMS_27106_MedChemExpress

Carbendazim_LCMS_27106_MedChemExpress

File ..ata\20171107\20171107\BIZ2017-N07-WYQ11.D Tgt Mass (CHM): Injection Date : 7 Nov 17 7:49 pm +0800 Seq. Line : 140 Sample Name : BIZ2017-N07-WYQ11 Location : P1-F-11 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 4 ul

Acq. Method : D:\LCMS03\Data\20171107\20171107\1-POS-3MIN.M

Analysis Method : D:\LCMS03\Data\20171107\20171107\1-POS-3MIN.M

Catalog No : HY-13582 Batch#27106

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min00.511.522.5mAU

0250500 DAD1 A, Sig=214,4 Ref=off

1.149

1.207

1.283

1.361

1.457

1.482

1.500

min00.511.522.5mAU

050 DAD1 B, Sig=254,4 Ref=off

1.148

1.460

1.481

1.500

1.562

1.603

1.673

2.047

min00.511.522.5mV

102030 ELS1 A, ELSD Signal

Alisertib_LCMS_18919_MedChemExpress

Alisertib_LCMS_18919_MedChemExpress

=====================================================================

Acq. Operator : Yang Qian(LCMS-02) Seq. Line : 46Acq. Instrument : HY-LCMS-02 Location : P2-F-06

Injection Date : 12/14/2015 12:14:04 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20151214\20151214 2015-12-14 08-45-47\100-1000MS+3MIN- 1.5_(0.02%FA)-BD.MLast changed : 12/14/2015 8:45:47 AM by Yang Qian(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\1000-2000MS+3MIN_1.5(0.02%FA).MLast changed : 12/14/2015 12:56:06 PM by Yang Qian(LCMS-02) (modified after loading)Method Info : Postive,MS:1000-2000,Column ID:A-RP-132,40℃ Catalog No : HY-10971 Batch#18919 A-RP-134 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

0500100015002000 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT 1260\DATA\20151214\20151214 2015-12-14 08-45-47\BIZ2015-D12-WJ3.D)