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NVP-BGJ398_LCMS_05601_MedChemExpress

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File D:\DATA\A02\MONITOR\CPK2016-713-056011-04476-LCMSA016.D Injection Date : 20 Jul 16 3:21 pm +0800 Tgt Mass(EZX) : 560.00 Sample Name : CPK2016-713-05601 Location : P1-C-03 Acq. Operator : A02-Monitor Inj : 1 Spec. Reported : MS Integration Inj Volume : 3 ul Acq. Method : D:\METHODS\1-POS-MON.M Analysis Method : D:\METHODS\1-POS-MON.M Catalog No : HY-13311 Batch#05601 Easy-Access Method: '1-POS-MON' 560.00 Method Info : Mobile Phase: A: water(0.01%TFA) B : ACN Gradient: 5%B increase to 95%B within1.5min, 95%B for 1.5min,back to 5%B within 0.01min. Flow Rate: 2.0 mL/min Column: Sunfire C18 4.6*50mm 3.5um Oven Temperature: 50 C Mass Range:103-1500

min*00.511.522.5mV

23.217523.22*ADC1 A, ELSD

min*00.511.522.5mAU

02000*DAD1 A, Sig=214,4 Ref=off

1.2981.3221.353

1.4711.684

min*00.511.522.5mAU

01000*DAD1 B, Sig=254,4 Ref=off

1.354

min00.511.522.50200000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.3542.807

min00.511.522.501000020000 Ion 561, MSD1 561,Target Mass 560 +H Positive, EIC=560.7:561.7

1.354

Integration Results for ADC1 A, ELSD RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------|

Integration Results for DAD1 A, Sig=214,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.30 0.01 5.21 9.45 0.17 1.32 0.01 7.21 10.78 0.23 1.35 0.01 3064.19 3510.69 99.02 1.47 0.01 6.97 8.23 0.23 1.68 0.01 11.04 12.94 0.36

Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 1.35 0.01 1858.89 2691.89 100.00LC/MS Report

LCMSA016 07/20/2016 3:24:41 PM A02-MonitorPage 1 of 2Ret. Time: 1.35 <<<< POSITIVE SPECTRA >>>>

m/z200400600800100012001400050001000015000200002500030000 ES-API Positive

1142.1 564.0 561.0 157.2 562.0 281.5 560.1 280.6Ret. Time: 2.81

m/z2004006008001000120014000

2500500075001000012500150001750020000 ES-API Positive

675.5 219.0 193.9 159.0 339.3 361.3 360.3 338.4LC/MS Report

LCMSA016 07/20/2016 3:24:41 PM A02-MonitorPage 2 of 2

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Pranlukast_hemihydrate_COA_22422_MedChemExpress

Pranlukast_hemihydrate_COA_22422_MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C27H23N5O4 .1/2H2OMolecular Weight:490.51Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.89%Conclusion:The product has been tested and complies with the given specifications.Product Name:Pranlukast (hemihydrate)Cat. No.:HY-B0290ACAS No.:150821-03-7Batch No.:22422Chemical Name:Benzamide, N-[4-oxo-2-(2H-tetrazol-5-yl)-4H-1-benzopyran-8-yl]-4-(4-phenylbutoxy)-, hydrate (2:1)

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

Syringaldehyde-COA-29222-MedChemExpress

Syringaldehyde-COA-29222-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C9H10O4Molecular Weight:182.17Storage:4°C, stored under nitrogenChemical Structure:ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureGC:Consistent with structurePurity (GC):99.96%Conclusion:The product has been tested and complies with the given specifications.Product Name:SyringaldehydeCat. No.:HY-N1390CAS No.:134-96-3Batch No.:29222Chemical Name:Benzaldehyde, 4-hydroxy-3,5-dimethoxy-

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

MOZ-IN-3-COA-29367-MedChemExpress

MOZ-IN-3-COA-29367-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C20H17FN2O3SMolecular Weight:384.42Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structureHPLC:Consistent with structurePurity (LCMS):99.70%Conclusion:The product has been tested and complies with the given specifications.Product Name:MOZ-IN-3Cat. No.:HY-102060CAS No.:2055397-18-5Batch No.:29367Chemical Name:[1,1'-Biphenyl]-3-carboxylic acid, 4-fluoro-5-methyl-, 2-(phenylsulfonyl)hydrazide

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Nivolumab-COA-31687-MedChemExpress

Nivolumab-COA-31687-MedChemExpress

ProductName:Inhibitors, Agonists, Screening

Nivolumab

Certificate of Analysis

Product Name:Cat. No.: CAS No.:Batch No.:Chemical Name:

Appearance:31687HY-P9903

Colorlesstolightyellow(Solution)Appearance:Purity (SEC-HPLC):10.0 mg/ml<0.5 EU/mgSterility:Storage Buffer:PBS, pH 7.298.56%Colorless to light yellow (Solution)

Concentration:Endotoxin Level:Sterilized via a 0.22 μm filter and packaged aseptically

Codon Optimization:YesExpression System:CHO stable cellPurification:Storage and Handling: after first use to avoid multiple freeze-thawsProtein was obtained from supernatant, followed by AC, CEX and SECStore at -80°C. Aliquots should be stored at the same temperature

Caution: Product has not been fully validated for medical applications. For research use only.lilhdhAddress: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852, USATel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@