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NVP-BGJ398_LCMS_11138_MedChemExpress

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File D:\CHEM32\1\DATA\CPK\CPK2016-N10-11138.D Tgt Mass (EZX): 560.00 Injection Date : 10 Nov 16 1:12 pm +0800 Seq. Line : 0 Sample Name : CPK2016-N10-11138 Location : P1-F-04 Acq. Operator : KFF(LCMS-02) Inj : 1

Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\Chem32\1\METHODS\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\METHODS\1-POS-3MIN-PROSRSS.M Catalog No : HY-13311 Batch#11138 Easy-Access Method: '1-POS-3MIN' 560.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*0.511.522.5mAU

050010001500*DAD1 B, Sig=214,4 Ref=off

1.2951.348

min*0.511.522.5mAU

0200400600800*DAD1 C, Sig=254,4 Ref=off

1.348

1.605

min0.511.522.50100000200000300000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

1.343

min0.511.522.5050001000015000 Ion 561, MSD1 561,Target Mass 560 +H Positive, EIC=560.7:561.7

1.345

Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.30 0.02 2.41 1.78 0.12 281 1.35 0.02 2002.86 2101.68 99.88 281

Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.35 0.02 945.74 1007.17 99.87 281 1.60 0.02 1.21 0.00 0.13 233MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 11/10/2016 13:17:33 KFF(LCMS-02)Page 1 of 2Ret. Time: 1.34 <<<< POSITIVE SPECTRA >>>>

m/z200300400500600700800900050001000015000200002500030000 ES-API Positive

563.2 157.3 560.3 281.6 280.7MS Report from Instrument: HY-LCMS-02

HY-LCMS-02 11/10/2016 13:17:33 KFF(LCMS-02)Page 2 of 2

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Pranlukast_hemihydrate_COA_22422_MedChemExpress

Pranlukast_hemihydrate_COA_22422_MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C27H23N5O4 .1/2H2OMolecular Weight:490.51Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.89%Conclusion:The product has been tested and complies with the given specifications.Product Name:Pranlukast (hemihydrate)Cat. No.:HY-B0290ACAS No.:150821-03-7Batch No.:22422Chemical Name:Benzamide, N-[4-oxo-2-(2H-tetrazol-5-yl)-4H-1-benzopyran-8-yl]-4-(4-phenylbutoxy)-, hydrate (2:1)

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

IBMX_COA_18139_MedChemExpress

IBMX_COA_18139_MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C10H14N4O2Molecular Weight:222.24Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.73%Conclusion:The product has been tested and complies with the given specifications.Product Name:IBMXCat. No.:HY-12318CAS No.:28822-58-4Batch No.:18139Chemical Name:1H-Purine-2,6-dione, 3,9-dihydro-1-methyl-3-(2-methylpropyl)-

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

Syringaldehyde-COA-29222-MedChemExpress

Syringaldehyde-COA-29222-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C9H10O4Molecular Weight:182.17Storage:4°C, stored under nitrogenChemical Structure:ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureGC:Consistent with structurePurity (GC):99.96%Conclusion:The product has been tested and complies with the given specifications.Product Name:SyringaldehydeCat. No.:HY-N1390CAS No.:134-96-3Batch No.:29222Chemical Name:Benzaldehyde, 4-hydroxy-3,5-dimethoxy-

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

Paquinimod-COA-31455-MedChemExpress

Paquinimod-COA-31455-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C21H22N2O3Molecular Weight:350.41Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):98.38%Conclusion:The product has been tested and complies with the given specifications.Product Name:PaquinimodCat. No.:HY-100442CAS No.:248282-01-1Batch No.:31455Chemical Name:3-Quinolinecarboxamide, N,5-diethyl-1,2-dihydro-4-hydroxy-1-methyl-2-oxo-N-phenyl-

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,