核磁氢谱化学位移对照表
在氯仿（CHCl3）中，甲基氢的化学位移范围约为3.5-4.0 ppm，亚甲基氢的化学位移范围约为1.5-2.5 ppm；
在二甲基甲酰胺（DMF）中，甲基氢的化学位移范围约为2.5-2.8 ppm，亚甲基氢的化学位移范围约为1.9-2.5 ppm；
在乙醇（EtOH）中，甲基氢的化学位移范围约为0.8-1.0 ppm，羟基氢的化学位移范围约为3.3-4.5 ppm。
需要注意的是，化学位移受溶剂、温度、溶液浓度等因素的影响，因此在进行核磁共振实验时，需要对这些因素进行控制和考虑。同时，不同化合物中氢原子的化学环境不同，因此其化学位移也会有所不同。在解读核磁氢谱时，需要结合化学位移、积分峰面积和耦合常数等信息，综合分析确定化合物的结构和性质。
总的来说，核磁氢谱化学位移对照表是化学工作者在解读核磁共振实验结果时的重要参考，能够帮助他们确定化合物的结构和特性。希望这些信息能够对你有所帮助。
美国CIL新版氘代试剂化学位移表 氢谱/碳谱 2011-8-23
Solvent 1H
Chemical Shift
(ppm from
TMS)
(multiplicity) JHD
(Hz) Carbon-13
Chemical Shift
(ppm from
TMS)
(multiplicity) JCD
(Hz) 1H
Chemical
Shift
of HOD
(ppm from
TMS) Density
at 20°C
20°C密度 Melting
point
(°C) Boiling
point
(°C) Dielectric
Constant
Molecular
Weight
Acetic Acid-d4
氘代乙酸 11.65 (1)
2.04 (5) /
2.2 178.99 (1)
20.0 (7) /
20 11.5
/ 1.12
/ 16.7
/ 118
/ 6.1
/ 64.08
/
Acetone-d6
氘代丙酮 /
2.05 (5) /
2.2 206.68 (1)
29.92 (7) 0.9
19.4 2.8
/ 0.87
/ -94
/’ 56.5
/ 20.7
/ 64.12
/
Acetonitrile-d3
氘代乙腈 /
1.94 (5) /
2.5 118.69 (1)
1.39 (7)
21 2.1
/ 0.84
/ -45
/ 81.6
/ 37.5
/ 44.07
/
Benzene-d6 氘代苯 7.16 (1) / 128.39 (3) 24.3 0.4 0.95 5.5 80.1 2.3 84.15
Chloroform-d 氘代氯仿 7.24 (1) / 77.23 (3) 32.0 1.5 1.50 -63.5 61-62 4.8 120.38
Cyclohexane-d12
氘代环己烷 1.38 (1) / 26.43 (5) 19 0.8 0.89 6.47 80.7 2.0 96.24
13C谱最新氘代试剂（核磁试剂）化学位移表 2010-7-17
13C氘代试剂（核磁试剂）化学位移表
碳原子 氘代四氢呋喃 氘代二氯甲烷 氘代氯仿 氘代甲苯 氘代苯 氘代氯苯 氘代丙酮 氘代DMSO 氘代乙腈 氘代三氟乙醇 氘代甲醇 氘代水
氘代试剂位移 67.21 53.84 77.16 137.48 128.06 134.19 29.84 39.52 1.32 61.50 49.00
25.31 128.87 129.26 206.26 118.26 126.28
127.96 128.25
125.13 125.96
20.43
乙酸 CO 171.69 175.85 175.99 175.30 175.82 175.67 172.31 171.93 173.21 177.96 175.11 177.21
CH3 20.13 20.91 20.81 20.27 20.37 20.40 20.51 20.95 20.73 20.91 20.56 21.03
丙酮 CO 204.19 206.78 207.07 204.00 204.43 204.83 205.87 206.31 207.43 32.35 209.67 215.94
CH3 30.17 31.00 30.92 30.03 30.14 30.12 30.60 30.56 30.91 214.98 30.67 30.89
乙腈 CN 116.79 116.92 116.43 115.76 116.02 115.93 117.60 117.91 118.26 118.95 118.06 119.68
CH3 0.45 2.03 1.89 0.03 0.20 0.63 1.12 1.03 1.79 1.00 0.85 1.47
氘代四氢呋喃氘代二氯甲烷氘代氯仿氘代甲苯氘代苯氘代氯苯氘代丙酮1.725.327.262.087.166.962.053.586.976.997.017.147.09水峰OHs2.461.521.560.430.41.032.84b乙酸aceticacidCH3s1.892.062.11.571.52丙酮CH3s2.052.122.171.571.551.772.09乙腈CH3s1.951.972.10.690.581.212.05苯CHs7.317.357.367.127.157.27.36正丁醇CH3s1.151.241.281.031.051.121.18OHsc3.160.580.631.3氯仿CHs7.897.327.266.16.156.748.0218-冠醚-6CH2s3.573.593.673.363.393.413.59DMFCHs7.917.968.027.577.637.737.96CH3s2.882.912.962.372.362.512.94CH3s2.762.822.881.961.862.32.78二恶烷CH2s3.563.653.713.333.353.453.59DMECH3s3.283.343.43.123.123.173.28CH2s3.433.493.553.313.333.373.46乙烷CH3s0.850.850.870.810.80.790.83乙醇CH3t, 71.11.191.250.970.961.061.12CH2q, 7d3.513.663.723.363.343.513.57OHsc,3.31.331.320.830.51.393.39环己胺CH2s1.441.441.431.41.41.371.43二氯乙烷CH2s3.773.763.732.912.93.263.87二氯甲烷CH2s5.515.335.34.324.274.775.63乙醚CH3t, 71.121.151.211.11.111.11.11CH2q, 73.383.433.483.253.263.313.41二甘醇二甲醚CH2m3.433.573.653.433.463.493.56CH2m3.533.53.573.313.343.373.47OCH3s3.283.333.393.123.113.163.28乙酸乙酯CH3COs1.9422.051.691.651.781.97CH2q, 74.044.084.123.873.893.964.05CH3t, 71.191.231.260.940.921.041.2乙烯CH2s5.365.45.45.255.255.295.38乙二醇CH2se3.483.663.763.363.413.583.28六甲基苯CH3s2.182.22.242.12.132.12.17正己烷CH3t, 70.890.890.880.880.890.850.88CH2m1.291.271.261.221.241.191.28吡啶CH(2,6)m8.548.598.628.478.538.518.58CH(3,5)m7.257.287.296.676.666.97.35CH(4)m7.657.687.686.996.987.257.76吡咯NHbrt9.968.698.47.717.88.61CH(2,5)m6.666.796.836.436.486.626.771H谱最新氘代试剂（核磁试剂）化学位移表碳原子氘代试剂位移CH(3,4)m6.026.196.266.276.376.276.07吡咯啉CH2(2,5)m2.752.822.872.542.542.64CH2(3,4)m1.591.671.681.361.331.43硅脂CH3s0.110.090.070.260.290.140.13四氢呋喃CH2(2,5)m3.623.693.763.543.573.593.63CH2(3,4)m1.791.821.851.431.41.551.79甲苯CH3s2.312.342.362.112.112.162.32CH(2,4,6)m7.17.157.176.96-7.017.027.01-7.087.10-7.20CH(3,5)m7.197.247.257.097.137.10-7.177.10-7.20三乙胺CH3t0.970.991.030.950.960.930.96CH2q2.462.482.532.392.42.392.45六甲基二硅醚CH3s0.070.070.070.10.120.10.07HMPAcCH3d2.582.62.652.422.42.472.59咪唑H2s4.554.594.624.54.474.494.54甲烷CH4s0.190.210.220.170.160.150.17甲醇CH3s3.273.423.493.033.073.253.31OHS3.021.091.091.33.12硝基甲烷CH3s4.314.314.333.012.943.594.43正戊烷CH3t0.890.890.880.870.870.840.88CH2m1.311.31.271.251.231.231.27丙烷CH3t0.90.90.90.890.860.840.88CH2sept1.331.321.321.321.261.261.312-丙醇CH3d1.081.171.220.950.951.041.1CHsept3.823.974.043.653.673.823.9丙烯CH3dt1.691.711.731.551.551.581.68CH2(1)dm4.894.934.944.924.954.914.9CH2(2)dm4.995.035.034.985.014.985CHm5.795.845.835.75.725.725.81吡啶CH(2,6)m8.548.598.628.478.538.518.58CH(3,5)m7.257.287.296.676.666.97.35CH(4)m7.657.687.686.996.987.257.76氘代DMSO氘代乙腈氘代三氟乙醇氘代甲醇氘代水2.51.945.023.314.793.883.33b2.133.664.871.761.961.911.962.062.092.082.192.152.222.071.961.952.032.067.377.377.367.331.111.161.281.41.244.192.182.28.327.587.337.93.513.513.643.643.87.957.927.867.977.922.892.892.982.993.012.732.772.882.862.853.573.63.763.663.753.243.283.43.353.373.433.453.613.523.60.820.850.850.850.821.061.121.221.191.173.443.543.713.63.654.632.4759.6858.2658.051.41.441.471.453.93.813.713.785.765.445.245.491.091.121.21.181.173.383.423.583.493.563.513.533.673.613.673.383.453.623.583.613.243.293.413.353.371.991.972.032.012.074.034.064.144.094.141.171.21.261.241.245.415.415.45.395.443.343.513.723.593.652.142.192.242.190.860.890.910.9 1.251.281.311.298.588.578.458.538.527.397.337.47.447.457.797.737.827.857.8710.0210.75119.61118.28119.066.736.756.846.726.93移表6.016.16.246.086.262.672.753.112.83.071.551.611.931.721.87-0.060.080.160.13.63.643.783.713.741.761.81.911.871.882.32.332.332.327.187.10-7.307.10-7.307.167.187.10-7.307.10-7.307.160.930.961.311.050.992.43a2.453.122.582.570.060.070.080.070.282.532.572.632.642.614.614.574.534.56H20.20.20.180.23.163.283.443.343.344.012.164.424.314.284.344.40.860.890.90.91.271.291.331.290.870.90.90.910.881.291.331.331.341.31.041.091.21.51.173.783.874.053.924.021.681.71.71.71.74.944.934.934.914.955.035.045.035.015.065.85.855.875.825.98.588.578.458.538.527.397.337.47.447.457.797.737.827.857.87
精品文档交流 核磁共振1H化学位移图表
质子类型 化学位移值文字需求请找字伯虎文字创意，Q为17-3125-3445
烷烃质子 (1) -C-C-H 0.9~1.5 ppm
(2) -C=C-CH
-C≡C-CH
(3)与N、S、C=O、-Ar相连 2.0~2.5 ppm
(4)与O、卤素相连 3~4 ppm
烯烃质子 4.5~8.0 ppm
利用1H-NMR可有效确定双键的取代及构型。
H=5.28+Zgem+Zcis+Ztrans
炔烃质子 4.5~8.0 ppm利用1H-NMR可有效确定双键的取代及构型。
炔烃质子 不特征， 1.8~3.0 ppm ，与烷烃重叠，应结合IR解析。
芳烃质子 1H-NMR信息非常特征 6.5~8.0 ppm，未取代芳环
7.26 ppm，呈现单峰 1.6~2.1 ppm
CCRcisRtransHRgem
精品文档交流
其它质子
醛基 -CO-H 9.0~10.0 ppm
羟基 R-OH 0.5~1.0ppm （稀溶液）
4~ 5.5 ppm （浓溶液）
Ar-OH 3.5~7.7 ppm
10~16 ppm（分子内氢键）
-COOH 10.5~13 ppm
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