abt-263-06-hplc 奥默生物

GBT_20769 2021_液质法测蔬菜中450种农药残留所有项目仪器参数gbt_20769-2021_液质法测蔬菜中450种农药残留-所有项目仪器参数e序号24459958343375383287283英文中文isoprocarb异丙威3,4,5-trimethacarb3,4,5-混杀威cycluron环路莠隆carbaryl甲萘威propachlor毒草胺rabenzazole吡咪唑simetryn西草净monolinuron绿谷隆mevinphos速攻灭磷a序号tr母离子114.90194.1215.00194.2313.40199.2413.70202.1515.40212.1614.10213.2711.00214.28 14.30215.1910.70225.029aziprotryne叠氮津380secbumeion嘧草通103cyprodinil嘧菌磺胺55buturon播土隆60carbetamide双酰草胺331pirimicarb抗蚜威88clomazonedimethazo异恶草松95cyanazine氰草津341prometrync扑草净306paraoxonmethyl甲基对氧磷74,4'-dichlorobenzop4,4'-二氯二苯甲酮412thiacloprid噻虫啉236imidacloprid吡虫啉166ethidimuron磺噻隆243isomethiozin丁嗪草酮116diallatc燕麦敌9acetochlor乙草胺294nitenpyram烯啶虫胺277methoprotryne盖草津135dimethenamid二甲酚草胺400terbucarb特草灵309penconazole戊菌唑289myclobutanil腈菌唑305paclobutrazol多效唑196fenthionsulfoxide倍硫磷亚砜426triadimenol三唑醇54butralin仲丁灵386spiroxamine螺恶茂胺421tolclofosmethyl甲基立枯磷113desmedipham甜菜胺273methidathion杀扑磷16allethrin烯丙菊酯427triallate野麦畏117diazinon二嗪磷160edifenphos敌瘟磷335pretilachlor丙草胺214flusilazole呋硅唑1018.501110.601217.601315.001411.40159.861616.001712.301814.401911.202127.1021 11.302210.202310.102423.302528.102621.80278.342812.302918.203026.703120.403218 .603316.303412.703516.103631.503711.503826.303916.904017.504129.604231.504325. 404422.704527.504619.80226.1226.2226.2237.1237.1239.2240.1241.1242.2248.0251.1 253.1256.1265.1269.1270.0270.2271.1272.2276.1278.2284.1289.1294.2295.1296.1296 .1298.2301.2301.2303.0303.2304.0305.1311.1312.1316.1240iprovalicarb丙森锌32benodanil麦锈灵217flutolanil氟酰胺178famphur氨磺磷30benalyxyl苯霜灵124diclobutrazole苄氯三唑醇165etaconazole乙环唑182fenarimol氯苯嘧啶醇324phthalicacid,dicyc邻苯二甲酸二环己酯409tetramethirn 胺菊酯122dichlofluanid杀菌灵89cloquintocetmexyl解草酯42bitertanol联苯三唑醇27azinphos-ethyl益棉磷86clodinafoppropargy炔草酯439triflumuron杀死铃脲250isoxaflutole异恶氟草20anilofos莎稗磷374quizalofop-ethyl喹禾灵227haloxyfopmethyl精氟吡甲禾灵201fluazifopbutyl吡氟禾草灵46bromophos-ethyl乙基溴硫磷115dialifos燕麦敌34bensulide地散磷429ttiasulfuron醚苯磺隆45bromfenvinfos溴苯烯磷357pyrazophos吡菌磷207flufenoxuron氟虫脲237indoxacarb茚虫威161emamectinbenzoate甲氨基阿维菌素苯甲酸盐174ethylenethiourea乙撑硫脲107dazomet棉隆293nicotine烟碱198fenuron非草隆104cyromazine灭蝇胺92crimidine鼠立克285molinate禾草敌59carbendazim多菌灵351propoxur残杀威248isouron异唑隆76chlorotoluron氯麦隆416thiofanox久效威66chlorbufam氯草灵31bendiocarb恶虫威348propazine扑灭津404terbuthylazine特丁津156diuron敌草隆4718.004816.404921.305017.005123.805219.505318.305417.505533.305629.205723.60582 7.705920.506022.206124.806224.106318.306424.606527.906627.006730.006833.206927 .507024.907112.907223.607324.807430.307527.307615.90772.13781.69791.688010.208 12.058210.408318.80842.148513.108612.008713.408813.908919.009013.109116.509217 .209314.20321.1324.1324.2326.0326.2328.0328.1331.0331.2332.2332.8336.1338.2346 .0350.1359.0360.0368.0373.0376.0384.1393.0394.0398.0402.1402.9413.0489.0528.08 86.2103.0163.1163.2165.1167.0172.1188.1192.1210.1212.2213.1219.3224.1224.1230. 1230.1233.172chlormephos氯甲硫磷62carboxin萎锈灵130difenzoquat-methyl野燕枯90clothianidin噻虫胺342pronamide拿草特133dimethachloro二甲草胺274methobromuron溴谷隆314phorate甲拌磷11aclonifen苯草醚262mephosfolan地安磷235imibenconazole-desb脱苯基亚胺唑292neburon草不隆259mefenoxam精甲霜灵354prothoate发硫磷172ethofumesate乙氧呋草黄239iprobenfos异稻瘟净398tepp特普102cyproconazole环丙唑醇413thiamethoxam噻虫嗪93crufomate育畜磷176etrimfos乙嘧硫磷105cythioate赛灭磷320phosphamidon磷胺311phenmedipham甜菜宁218flutriafol粉唑醇224furalaxyl抑菌丙胺酯40bioallerthrin生物丙烯菊酯96cyanofenphos苯腈磷332pirimiphosmethyl甲基嘧啶磷50buprofezin噻嗪酮151disulfotonsulfone乙拌磷砜183fenazaquin喹螨醚430triazophos三唑磷108def脱叶磷365pyriftalid环酯草醚269metconazole叶菌唑369pyriproxyfen蚊蝇醚249isoxaben异恶酰草胺213flurtamone呋草酮440trifluralin氟乐灵199flampropmethyl甲基麦草氟异丙酯41bioresmethrin生物汴呋菊酯350propiconazole丙环唑80chlorpyrifos毒死蜱204fiuchloralin氯乙氟灵81chlorsulfuron氯磺隆407tetrachlorvinphos杀虫畏9423.209514.20969.92979.999819.509915.7010014.9010126.4010223.0010311.7010411. 6010522.3010614.2021715.7010820.0010920.8011011.2021116.901129.4011318.2021416 .9011512.5011611.3011716.8011913.3012021.2021129.7012225.7012326.1012426.60125 16.4012630.2021721.3012833.6012918.8013020.9013129.7013219.9013317.3013430.901 3520.2021634.0013721.6013830.4013928.4014013.2021121.20235.0236.1249.1250.2256 .1256.1259.0261.0265.1270.1271.0275.1280.1286.1287.0289.1291.1292.1292.1292.1293.1298.0300.1301.1302.1302.2303.1304.0306.2306.2307.0307.2314.1315.1319.0320. 2322.1322.1334.1336.0336.1339.2342.1350.0256.0358.0365.0347propargite炔螨特48bromuconazole糠菌唑327picolinafen氟吡酰草胺216fluthiacetmethyl氟噻乙草酯438trifloxystrobin肟菌酯229hexaflumuron氟铃脲297novaluron双苯氟脲202fluazuron啶蜱脲272methamidophos甲胺磷164eptc菌草敌129diethylroluamide避蚊胺288monuron灭草隆366pyrimethanil嘧霉胺185fenfuram黑穗胺372quinoclamine灭藻醌187fenobucarb仲丁威171ethirimol乙菌定345propanil 敌稗61carbofuran克百威8acetamiprid啶虫脒261mepanipyrim嘧菌胺340prometon扑灭通281metoxuron甲氧隆137dimethoate乐果209fluometuron伏草隆127dicrotophos 白治磷286monalide庚酰草胺147diphenamid双苯酰草胺173ethoprophos灭线磷221fonofos地虫硫磷225furmecyclox拌种胺230hexazinone环嗪酮134dimethametryn阔草净433tricholorphon敌百虫109demeton（o+s）内吸磷33benoxacor解草酮44bromacil除草定316phoratesulfoxide甲拌磷亚砜47brompyrazon溴莠敏303oxycarboxin氧化萎锈灵264mepronil灭锈胺150disulfoton乙拌磷194fenthion倍硫磷266metalaxyl甲霜灵299ofurace甲呋酰胺159dodemorph吗菌灵222fosthiazate噻唑硫磷14231.8014317.8014428.6014523.0014627.7014726.5014827.6014929.202102.1415122.8015 214.2021312.0015414.3015514.5015612.3015717.101589.1715916.2021013.2021110.501 6219.9016310.6016411.5016510.4016613.701679.1016823.3016915.7017019.2021125.80 17222.5017311.4017416.101759.7217615.3017718.2021811.801799.7318010.4018111.30 18220.7018331.3018424.5018514.2021614.2021711.1018813.80368.1376.0377.0404.040 9.3461.0493.0506.0142.1190.2192.2199.0200.2202.1208.1208.2210.2218.0222.3223.2 224.2226.2229.1230.0233.1238.1240.1240.1243.1247.1252.2253.2256.2257.0259.1260 .0261.0261.1266.0268.0270.2275.0279.0280.1282.1282.3284.1233imazamethabenzmethy甲基咪草酯189152disulfoton-sulfoxid乙拌磷-亚砜190246isoprothiolane稻瘟灵191232imazalil抑霉唑192321phoxim辛硫磷193371quinalphos赚硫磷194153ditalimfos杀菌磷195189fenoxycarb双氧威196368pyrimitate嘧啶磷197193fensulfothin丰索磷198210fluorochloridone氯咯草酮19951butachlor丁草胺200252kresoxim-methyl亚胺菌202144triticonazole戊叉菌唑202181fenamiphossulfoxid苯线磷亚砜203410thenylchlor噻吩草胺204359pyrethrin除虫菊素205188fenoxanil氰菌胺206211fluridone杀死草吡啶207163epoxiconazole氟环唑20878chlorphoxim氯辛硫磷209180fenamiphossulfone苯线磷砜210184fenbuconazole 腈苯唑211242isofenphos异柳磷212312phenothrin苯醚菊酯213197fentin-chloride氯化薯瘟锡214330piperophos呱草磷215329piperonylbutoxide提质醚216304oxyflurofen 乙氧氟草醚21791coumaphos蝇毒磷218206flufenacet氟噻草胺219317phosalone伏杀硫磷220278methoxyfenozide甲氧虫酰肼221336prochloraz咪酰胺22221aspon丙硫特普223169cthion乙硫磷224155dithiopyr氟硫草定225385spirodiclofen螺螨酯226192fenpyroximate唑螨酯227208flumiclorac-pentyl胺氟草酯228397temephos双硫磷22952butafenacil氟丙嘧草酯230384spinosad多杀菌素231263mepiquatchloride甲呱金翁23217allidochlor二丙烯草胺233344propamocarb霜霉威234435tricyclazole三环唑23510.90289.113.30291.021.10291.110.50297.023.70299.023.70299.115.10300.021.10 302.124.00306.114.30309.021.80312.130.00312.223.70314.116.90318.210.90320.121. 70324.131.90329.123.40329.116.80330.118.60330.127.20333.012.30336.120.10337.12 7.80346.135.10351.111.70351.127.20354.129.10356.229.60362.025.50363.122.00364. 026.60368.120.40369.217.50376.133.60379.130.90385.028.90402.033.90411.131.1042 2.229.50441.130.10467.023.10475.013.40732.41.90114.112.40174.12.36189.210.7019 0.1。

ABTS自由基清除能力检测试剂盒说明书货号：UPLC-MS-4571规格：100T/48S微量法产品内容：使用前请认真核对试剂体积与瓶内体积是否一致，有疑问请及时联系工作人员。

试剂名称规格保存条件提取液液体80mL×1瓶2-8℃保存试剂一液体40mL×1瓶2-8℃保存试剂二粉剂×1支2-8℃保存试剂三液体20μL×1支2-8℃保存试剂四液体 1.5mL×1支-20℃保存试剂五粉剂×1支2-8℃保存溶液的配制：1、试剂二：临用前加入1mL蒸馏水，充分溶解；用不完的试剂可分装后保存，-20℃可保存四周，避免反复冻融；2、试剂三工作液的配制：液体置于试剂瓶内EP管中。

临用前根据样本量按试剂三（μL）：蒸馏水（mL）=1μL:12mL的比例配成试剂三工作液，现用现配，用多少配多少，尽量在4h之内用完；3、试剂四工作液的配制：可先将试剂四-20℃分装保存。

临用前根据样本量按试剂四：试剂一（V:V）=1:9的比例配成试剂四工作液，现配现用，用不完的试剂放于-20℃可保存两周。

4、试剂五：粉剂置于试剂瓶内玻璃瓶中，含有5mg维生素C，临用前加入2.8mL提取液，充分振荡溶解；配成10mmol/L维生素C溶液，用于阳性对照。

2-8℃可保存两周。

5、ABTS工作液的配制：临用前根据试验所需量按试剂一：试剂二：试剂三工作液（V:V:V）=76:5:4的比例配成ABTS工作液，现用现配，室温避光保存，务必在30分钟内使用。

产品说明：ABTS法可用于亲水性和亲脂性物质抗氧化能力测定，是使用最广泛的间接检测方法。

ABTS经氧化后生成稳定的蓝绿色阳离子ABTS自由基，在405nm或734nm处有最大吸收峰。

被测物质加入ABTS自由基溶液后，所含抗氧化成分能与ABTS自由基发生反应而使反应体系褪色，405nm的吸光度下降，在一定范围内其吸光度的变化与自由基被清除的程度成正比。

植物游离脂肪酸（FFA）酶联免疫分析(ELISA)试剂盒使用说明书本试剂仅供研究使用目的：本试剂盒用于测定植物血清、血浆、组织等样本中游离脂肪酸（FFA）的含量。

实验原理：本试剂盒应用双抗体夹心法测定标本中植物游离脂肪酸（FFA）水平。

用纯化的植物游离脂肪酸（FFA）捕获抗体包被微孔板，制成固相抗体，往包被的微孔中依次加入植物游离脂肪酸（FFA），再与HRP标记的检测抗体结合，形成抗体-抗原-酶标抗体复合物，经过彻底洗涤后加底物TMB显色。

TMB在HRP酶的催化下转化成蓝色，并在酸的作用下转化成最终的黄色。

颜色的深浅和样品中的植物游离脂肪酸（FFA）呈正相关。

用酶标仪在450nm波长下测定吸光度（OD值），通过标准曲线计算样品中植物游离脂肪酸（FFA）含量。

试剂盒组成：样本处理及要求：1. 血清：室温血液自然凝固10-20分钟，离心20分钟左右（2000-3000转/分）。

仔细收集上清，保存过程中如出现沉淀，应再次离心。

2. 血浆：应根据标本的要求选择EDTA或柠檬酸钠作为抗凝剂，混合10-20分钟后，离心20分钟左右（2000-3000转/分）。

仔细收集上清，保存过程中如有沉淀形成，应该再次离心。

3. 尿液：用无菌管收集，离心20分钟左右（2000-3000转/分）。

仔细收集上清，保存过程中如有沉淀形成，应再次离心。

胸腹水、脑脊液参照实行。

4. 细胞培养上清：检测分泌性的成份时，用无菌管收集。

离心20分钟左右（2000-3000转/分）。

仔细收集上清。

检测细胞内的成份时，用PBS（PH7.2-7.4）稀释细胞悬液，细胞浓度达到100万/ml左右。

通过反复冻融，以使细胞破坏并放出细胞内成份。

离心20分钟左右（2000-3000转/分）。

仔细收集上清。

保存过程中如有沉淀形成，应再次离心。

5. 组织标本：切割标本后，称取重量。

加入一定量的PBS，PH7.4。

用液氮迅速冷冻保存备用。

标本融化后仍然保持2-8℃的温度。

HPLC法测定糠酸莫米松乳膏中的有关物质曹玉明【摘要】Objective To develop a method for the related substances in mometasone furoate cream(Eloson).Methods HPLC was a-dopted for the limits determination of the related substances.An Amethyst C18 -Pcolumn(250 mm ×4.6 mm,5 μm)was used as the stationary phase,with a mobile phase of acetonitrile-water solution(53∶47),the flow rate was 1 mL·min-1 ,the detection wavelength was 254 nm and the injection volume was 20 μL.Results For each impurity was not more than 1 .0%,the total was not more than 2.0%.Five batches of Eloson were analyzed under the established method,all of results were that for each impurity was not more than 1.0% and the total was not more than 2.0%.Conclusion The developed method is accurate and reliable,which could be used for thelimit control of the related substances in Eloson.%目的：建立糠酸莫米松乳膏（艾洛松）中有关物质的检测方法。