Osilodrostat_LCMS_24980_MedChemExpress

=====================================================================Acq. Operator : CLJ_701 Seq. Line : 36Acq. Instrument : LCMS-02 Location : P1-F-06Injection Date : 5/16/2017 16:05:53 Inj : 1Inj Volume : 1.000 µl Different Inj Volume from Sample Entry! Actual Inj Volume : 2.500 µlAcq. Method : D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\1-POS-3MIN.M Last changed : 5/16/2017 13:25:15 by CLJ_701Analysis Method : D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\1-POS-3MIN.M (Sequence Method)Last changed : 5/16/2017 18:21:45 by CLJ_701 (modified after loading)Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45CCatalog No : HY-10228 Batch#24601 A-RP-186Additional Info : Peak(s) manually integratedmin*0.51 1.52 2.53mAU 02004006008001000*DAD1 B, Sig=214,4 Ref=off (D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\BIZ2017-516-WJ5-2.D)0.6421.3371.567 1.612min*0.511.522.53mAU200400600800*DAD1 C, Sig=254,4 Ref=off (D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\BIZ2017-516-WJ5-2.D) 1.3371.484 1.503 1.5691.7432.2072.4062.541===================================================================== Area Percent Report =====================================================================Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDsSignal 1: DAD1 B, Sig=214,4 Ref=offSignal has been modified after loading from rawdata file!Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 0.642 MM 0.0202 5.22468 4.31826 0.2269 2 1.337 MM 0.0341 2277.05762 1113.49768 98.8836 3 1.567 MM 0.0222 10.16209 7.62597 0.4413Peak RetTime Type Width Area Height Area# [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------|4 1.612 MM 0.0176 10.32018 9.75218 0.4482Totals : 2302.76456 1135.19410Signal 2: DAD1 C, Sig=254,4 Ref=offSignal has been modified after loading from rawdata file!Peak RetTime Type Width Area Height Area# [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------|1 1.337 MF R 0.0470 1891.27673 928.95624 96.24832 1.484 MF R 0.0121 21.76458 22.09819 1.10763 1.503 FM R 0.0299 26.54858 14.90156 1.35114 1.569 FM R 0.0332 14.45967 7.49148 0.73595 1.743 MM R 0.5784 1.91948 1.22552 0.09776 2.207 MM R 0.0178 2.89327 2.70821 0.14727 2.406 MM R 0.1913 2.50237 2.20635e-1 0.12738 2.541 MM R 0.0422 3.63265 1.43360 0.1849Totals : 1964.99733 979.03543===================================================================== *** End of Report ***=====================================================================Acq. Operator : CLJ_701 Seq. Line : 36Acq. Instrument : LCMS-02 Location : P1-F-06Injection Date : 5/16/2017 16:05:53 Inj : 1Inj Volume : 1.000 µl Different Inj Volume from Sample Entry! Actual Inj Volume : 2.500 µlAcq. Method : D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\1-POS-3MIN.M Last changed : 5/16/2017 13:25:15 by CLJ_701Analysis Method : D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\1-POS-3MIN.M (Sequence Method)Last changed : 5/16/2017 18:22:12 by CLJ_701 (modified after loading)Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45CCatalog No : HY-10228 Batch#24601 A-RP-186Additional Info : Peak(s) manually integratedmin0.511.522.51000020000300004000050000600007000080000 MSD1 TIC, MS File (D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\BIZ2017-516-WJ5-2.D) ES-API, Pos, Scan, F1.421MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 70 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.Reportable Ion Abundance: > 10%.Retention Mol. Weight Time (MS) MS Area or Ion1.421 596297 374.10 I 187.70 Im/z10020030040050060070080020406080100*MSD1 SPC, time=1.369:1.474 of D:\CHEM32\1\DATA\20170516\20170516 2017-05-16 13-25-15\BIZ2017-516-WJ5-2.D ES-API, PoMax: 54625374.1187.7*** End of Report ***。

Inhibitors, Agonists, Screening Librarieswww.MedChemExpress.com

Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES 

Molecular Formula:C20H22O9

Molecular Weight:406.38

Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA 

Appearance:Light yellow to yellow (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):98.72%Conclusion:The product has been tested and complies with the given specifications.

Product Name:2,3,5,4'-Tetrahydroxystilbene 2-O-β-D-glucosideCat. No.:HY-N0652CAS No.:82373-94-2Batch No.:24358Chemical Name:β-D-Glucopyranoside, 2,4-dihydroxy-6-[(1E)-2-(4-hydroxyphenyl)ethenyl]phenyl

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@MedChemExpress.comAddress: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852, USA

=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 43Acq. Instrument : HY-LCMS-02 Location : P1-A-03Injection Date : 4/21/2015 6:05:06 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150421\20150421 2015-04-21 15-02-14\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/21/2015 3:02:15 PM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\100-1000MS+3MIN-1.5-286NM_(0.02%FA).M Last changed : 4/22/2015 10:37:19 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃Catalog No : HY-14981 Batch#06980 A-RP-132Additional Info : Peak(s) manually integratedmin0.511.522.53mAU 0100200300400500600700 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150421\20150421 2015-04-21 15-02-14\CPK2015-421-06980.D)1.4061.5461.6872.0122.2472.579===================================================================== Area Percent Report =====================================================================Sorted By : Signal Multiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDsSignal 1: DAD1 C, Sig=254,4 Ref=offPeak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.406 MM 0.0515 1.01024 3.27196e-1 0.0306 2 1.546 MM 0.0502 7.49705e-1 2.48766e-1 0.0227 3 1.687 MM 0.0650 3302.52612 846.39136 99.8716 4 2.012 MM 0.0482 5.39957e-1 1.86535e-1 0.0163 5 2.247 MM 0.0419 1.69974 6.75505e-1 0.0514 6 2.579 MM 0.0361 2.44617e-1 1.13004e-1 7.397e-3Totals : 3306.77038 847.94236===================================================================== *** End of Report ***=======================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 43Acq. Instrument : HY-LCMS-02 Location : P1-A-03Injection Date : 4/21/2015 6:05:06 PM Inj : 1Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150421\20150421 2015-04-21 15-02-14\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/21/2015 3:02:15 PM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\100-1000MS+3MIN-1.5-286NM_(0.02%FA).M Last changed : 4/22/2015 10:39:08 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃Catalog No : HY-14981 Batch#06980 A-RP-132Additional Info : Peak(s) manually integratedmin0.511.522.53100000200000300000400000500000600000700000800000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150421\20150421 2015-04-21 15-02-14\CPK2015-421-06980.D) ES-API, Pos, Sc1.700MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts.Reportable Ion Abundance: > 10%.Retention Mol. Weight Time (MS) MS Area or Ion1.700 6340813 463.90 I 462.90 I 232.00 Im/z10020030040050060070020406080100*MSD1 SPC, time=1.671:1.744 of D:\AGLIENT 1260\DATA\20150421\20150421 2015-04-21 15-02-14\CPK2015-421-06980.D ES-API Max: 343219463.9 462.9232.0*** End of Report ***。

Inhibitors, Agonists, Screening Librarieswww.MedChemExpress.com

Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES 

Molecular Formula:C21H18O13

Molecular Weight:478.36

Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA 

Appearance:Light yellow to yellow (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.50%Conclusion:The product has been tested and complies with the given specifications.

Product Name:MiquelianinCat. No.:HY-13930CAS No.:22688-79-5Batch No.:24762Chemical Name:β-D-Glucopyranosiduronic acid, 2-(3,4-dihydroxyphenyl)-5,7-dihydroxy-4-oxo-4H-1-benzopyran-3-yl

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@MedChemExpress.comAddress: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852, USA