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Dihydroisotanshinone_I_LCMS_24690_MedChemExpress

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File ..0524 2017-05-24 08-45-07\BIZ2017-524-WYQ6.D Tgt Mass (CHM): Injection Date : 24 May 17 1:47 pm +0800 Seq. Line : 47 Sample Name : BIZ2017-524-WYQ6 Location : P1-D-05 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170524\20170524 2017-05-24 08-45-07\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170524\20170524 2017-05-24 08-45-07\1-POS-3MIN.M Catalog No : HY-B1919 Batch#24690 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min*0.511.522.53mAU

0250500750*DAD1 B, Sig=214,4 Ref=off

1.6101.9472.1062.139

min*0.511.522.53mAU

0200400600*DAD1 C, Sig=254,4 Ref=off

1.9251.9502.1062.139

2.431

min0.511.522.530200004000060000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

2.223

min0.511.522.5302000040000 Ion 279, MSD1 279,Target Mass 278 +H Positive, EIC=278.7:279.7

2.222

Integration Results for DAD1 B, Sig=214,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.61 0.03 2.63 1.55 0.19 ND 1.95 0.02 1.06 1.10 0.08 ND 2.11 0.01 3.03 3.54 0.21 ND 2.14 0.02 1406.46 1122.27 99.52 279

Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.92 0.01 0.14 0.22 0.01 ND 1.95 0.02 0.89 0.66 0.08 ND 2.11 0.32 3.53 3.34 0.30 ND 2.14 0.02 1158.67 914.55 99.54 279 2.43 0.04 0.75 0.28 0.06 ND

Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|MS Report from Instrument: LCMS-02

LCMS-02 5/24/2017 13:57:51 CLJ_701Page 1 of 3 2.22 0.06 237659.80 65538.50 100.00 279MS Report from Instrument: LCMS-02LCMS-02 5/24/2017 13:57:51 CLJ_701

Page 2 of 3Ret. Time: 2.22 <<<< POSITIVE SPECTRA >>>>

m/z2003004005006007008000200040006000800010000120001400016000 ES-API Positive

338.1 579.0 280.1 279.1MS Report from Instrument: LCMS-02

LCMS-02 5/24/2017 13:57:51 CLJ_701Page 3 of 3

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Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C17H26N4O3S2Molecular Weight:398.54Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structurePurity (LCMS):99.72%Conclusion:The product has been tested and complies with the given specifications.Product Name:FursultiamineCat. No.:HY-B2082CAS No.:804-30-8Batch No.:27364Chemical Name:Formamide,N–[(4–amino–2–methyl–5–pyrimidinyl)methyl]–N–[4–hydroxy–1–methyl–2–[[(tetrahydro–2–furanyl)methyl]dithio]–1–buten–1–yl]–

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852, USA

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Pranlukast_hemihydrate_COA_22422_MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

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Inhibitors, Agonists, Screening Certificate of Analysis

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Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

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MOZ-IN-3-COA-29367-MedChemExpress

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C20H17FN2O3SMolecular Weight:384.42Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

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