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E-64_LCMS_15790_MedChemExpress

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Acq. Operator : Li Shan(LCMS-02) Seq. Line : 53Acq. Instrument : HY-LCMS-02 Location : P1-B-06

Injection Date : 4/23/2015 2:24:27 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/23/2015 9:09:18 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_51(RP-HPLC)(N@P).MLast changed : 4/23/2015 5:11:07 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-15282 Batch#15790 A-RP-132 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

-50-250255075100125 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.D) 1.336

1.707 2.027 2.554 3.159

===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.336 MM 0.0430 422.39676 163.88358 98.4469 2 1.707 MM 0.0456 9.44293e-1 3.44905e-1 0.2201 3 2.027 MM 0.0522 2.02319 6.46030e-1 0.4715 4 2.554 MM 0.0505 1.76413 5.82278e-1 0.4112 5 3.159 MM 0.0623 1.93193 5.16653e-1 0.4503 Totals : 429.06030 165.97344 ===================================================================== *** End of Report ***Data File D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.DSample Name: BIZ2015-423-DJL5

HY-LCMS-02 4/23/2015 5:11:09 PM Li Shan(LCMS-02)Page 1 of 1=============================================================

Acq. Operator : Li Shan(LCMS-02) Seq. Line : 53Acq. Instrument : HY-LCMS-02 Location : P1-B-06

Injection Date : 4/23/2015 2:24:27 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 4/23/2015 9:09:18 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-342_51(RP-HPLC)(N@P).MLast changed : 4/23/2015 5:12:32 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,Positive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-15282 Batch#15790 A-RP-132 Additional Info : Peak(s) manually integrated

min0.511.522.53050000100000150000200000250000300000350000400000 MSD1 TIC, MS File (D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.D) ES-API, Pos, Sca 1.338

Data File D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.DSample Name: BIZ2015-423-DJL5

HY-LCMS-02 4/23/2015 5:12:34 PM Li Shan(LCMS-02)Page 1 of 2MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%.

Retention Mol. WeightTime (MS) MS Area or Ion 1.338 1790603 358.90 I 357.90 I

m/z100200300400500600700020406080100*MSD1 SPC, time=1.325:1.361 of D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.D ES-API,Max: 295381

358.9 357.9

*** End of Report ***Data File D:\AGLIENT 1260\DATA\20150423\20150423 2015-04-23 09-09-18\BIZ2015-423-DJL5.DSample Name: BIZ2015-423-DJL5

HY-LCMS-02 4/23/2015 5:12:34 PM Li Shan(LCMS-02)Page 2 of 2

合集下载

EPZ-6438_LCMS_16818_MedChemExpress

EPZ-6438_LCMS_16818_MedChemExpress

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Acq. Operator : Li Shan(LCMS-02) Seq. Line : 36Acq. Instrument : HY-LCMS-02 Location : P1-D-06

Injection Date : 7/3/2015 1:59:43 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150703\20150703 2015-07-03 09-21-12\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 7/3/2015 9:21:12 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\BLHM-354_10A-H01P01,C2.MLast changed : 7/3/2015 2:44:38 PM by Li Shan(LCMS-02) (modified after loading)Method Info : HM-354_10A-H01P01,C2 Catalog No : HY-13803 Batch#16818 A-RP-132 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

050100150200250300350 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...60\DATA\20150703\20150703 2015-07-03 09-21-12\BIZ2015-703-DJL4.D) 1.616

1.962 2.042 2.304

C646_LCMS_15270_MedChemExpress

C646_LCMS_15270_MedChemExpress

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Acq. Operator : Li Shan(LCMS-02) Seq. Line : 29Acq. Instrument : HY-LCMS-02 Location : Vial 25

Injection Date : 3/11/2015 11:39:48 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150311\20150311 2015-03-11 09-17-51\100-1000MS+3MIN( 0.02%FA)-2.MLast changed : 3/11/2015 9:17:51 AM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HM-297D_4A-H04RS-1(RP-HPLC).MLast changed : 3/13/2015 11:28:20 AM by Li Shan(LCMS-02) (modified after loading)Method Info : hplc Catalog No : HY-13823 Batch#15270 A-RP-32 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

0500100015002000 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...60\DATA\20150311\20150311 2015-03-11 09-17-51\BIZ2015-311-DJL3.D)

2.171

2.404 2.470

===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 B, Sig=214,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 2.171 MM 0.0505 2449.23022 808.68921 98.7884 2 2.404 MM 0.0351 5.18778 2.46304 0.2092 3 2.470 MM 0.0415 24.85140 9.97989 1.0024 Totals : 2479.26940 821.13213 ===================================================================== *** End of Report ***Data File D:\AGLIENT 1260\DATA\20150311\20150311 2015-03-11 09-17-51\BIZ2015-311-DJL3.DSample Name: BIZ2015-311-DJL3

PX-12_LCMS_15244_MedChemExpress

PX-12_LCMS_15244_MedChemExpress

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Acq. Operator : Li Shan(LCMS-02) Seq. Line : 12Acq. Instrument : HY-LCMS-02 Location : Vial 49

Injection Date : 3/9/2015 3:18:15 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150309-1\20150309-1 2015-03-09 14-22-16\100-1000MS+ 3MIN(0.02%FA)-2.MLast changed : 3/9/2015 2:22:16 PM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\DATA\20140609\20140609 2014-06-09 16-50-20\100-1000MS+3MIN. M (Sequence Method)Last changed : 3/9/2015 3:50:43 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃ Catalog No : HY-13734 Batch#15244 A-RP-32 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

050100150200250300350400 DAD1 B, Sig=214,4 Ref=off (D:\AGLIENT...ATA\20150309-1\20150309-1 2015-03-09 14-22-16\BIZ2015-309-DJL8.D) 1.211

HMN-154_LCMS_25778_MedChemExpress

HMN-154_LCMS_25778_MedChemExpress

File ..0805 2017-08-05 18-02-53\BIZ2017-804-WYQ2.D Tgt Mass (CHM): Injection Date : 5 Aug 17 7:46 pm +0800 Seq. Line : 21 Sample Name : BIZ2017-804-WYQ2 Location : P1-A-02 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul

Acq. Method : D:\chem32\1\DATA\20170805\20170805 2017-08-05 18-02-53\1-POS-3MIN.M Analysis Method : D:\CHEM32\1\DATA\20170805\20170805 2017-08-05 18-02-53\1-POS-3MIN.M Catalog No : HY-103001 Batch#25778 ARP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C

min0.511.522.5mAU

0200 DAD1 B, Sig=214,4 Ref=off

1.422

1.503

min0.511.522.5mAU

0100200 DAD1 C, Sig=254,4 Ref=off

1.422

1.504

min0.511.522.50100002000030000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70