N3PT_HNMR_09325_MedChemExpress

Inhibitors, Agonists, Screening

Safety Data SheetRevision Date:Jul.-03-2017Print Date:Jul.-03-2017

1. PRODUCT AND COMPANY IDENTIFICATION1.1 Product identifierProduct name :Dronedarone

Catalog No. :HY-A0016

CAS No. :141626-36-01.2 Relevant identified uses of the substance or mixture and uses advised againstIdentified uses :Laboratory chemicals, manufacture of substances.1.3 Details of the supplier of the safety data sheetCompany:MedChemExpress USA

Tel:609-228-6898

Fax:609-228-5909

E-mail:sales@1.4 Emergency telephone numberEmergency Phone #:609-228-6898

2. HAZARDS IDENTIFICATION2.1 Classification of the substance or mixtureNot a hazardous substance or mixture.2.2 GHS Label elements, including precautionary statementsNot a hazardous substance or mixture.2.3 Other hazardsNone.

File ..170619 2017-06-19 09-04-59\WW4359-003-1_1.D Tgt Mass (CHM): Injection Date : 19 Jun 17 11:17 am +0800 Seq. Line : 27 Sample Name : WW4359-003-1_1 Location : P2-A-02 Acq. Operator : CLJ_701 Inj : 1 Spec. Reported : MS Integration Inj Volume : 0.5 ul

Acq. Method : D:\chem32\1\DATA\20170619\20170619 2017-06-19 09-04-59\1-POS-3MIN.M

Analysis Method : D:\CHEM32\1\DATA\20170619\20170619 2017-06-19 09-04-59\1-POS-3MIN.M

Catalog No : HY-16973 Batch#25003 A-RP-186

Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)

Gradient: 5% to 95%B within 1.3 min

Flow Rate :1.8ml/min

Column :SunFire C18, 4.6*50mm,3.5um A-RP-186

Oven Temperature : 45C

min0.511.522.5mAU

05001000 DAD1 B, Sig=214,4 Ref=off

1.586

1.7472.084

min0.511.522.5mAU

0200400600 DAD1 C, Sig=254,4 Ref=off

1.455

1.482

1.7412.084

min0.511.522.5050000100000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70

Inhibitors, Agonists, Screening Certificate of Analysis

PHYSICAL AND CHEMICAL PROPERTIES Molecular Formula:C20H17FN2O3SMolecular Weight:384.42Storage:Powder-20°C3 years4°C2 yearsIn solvent-80°C6 months-20°C1 monthChemical Structure:

ANALYTICAL DATA Appearance:White to off-white (Solid)1 H NMR Spectrum:Consistent with structureLCMS:Consistent with structureHPLC:Consistent with structurePurity (LCMS):99.70%Conclusion:The product has been tested and complies with the given specifications.Product Name:MOZ-IN-3Cat. No.:HY-102060CAS No.:2055397-18-5Batch No.:29367Chemical Name:[1,1'-Biphenyl]-3-carboxylic acid, 4-fluoro-5-methyl-, 2-(phenylsulfonyl)hydrazide

Caution: Product has not been fully validated for medical applications. For research use only.Tel: 609-228-6898 Fax: 609-228-5909 E-mail: tech@Address: 1 Deer Park Dr, Suite Q, Monmouth Junction, NJ 08852,

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Acq. Operator : Li Shan(LCMS-02) Seq. Line : 57Acq. Instrument : HY-LCMS-02 Location : P1-D-06

Injection Date : 5/26/2015 6:21:25 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\AGLIENT 1260\DATA\20150526\20150525 2015-05-26 13-55-34\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/26/2015 1:55:35 PM by Li Shan(LCMS-02)Analysis Method : D:\AGLIENT 1260\METHOD\HM-375_6-H01RS10(RP-HPLC.).MLast changed : 5/27/2015 2:50:40 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Negtive,MS:100-1000,Column ID:A-RP108 40℃ Catalog No : HY-A0059 Batch#09645 A-RP-132 Additional Info : Peak(s) manually integrated

min0.511.522.53mAU

02004006008001000 DAD1 C, Sig=254,4 Ref=off (D:\AGLIENT...0\DATA\20150526\20150525 2015-05-26 13-55-34\CPK2015-526-09645.D)