ASTM D6160-98

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ASTM_A_568M-98_碳素钢及高强度低合金钢热冷轧薄钢板带的一般要求

ASTM A568/A568M－98 碳素钢及高强度低合金钢热、冷轧薄钢板、带的一般要求（2）生产厂应对每炉钢进行化学分析（熔炼分析）测定相应规范中所规定的元素含量。

当用户提出要求时应将分析报告提供给用户。

（3）成品分析非镇静钢（如沸腾钢、压盖钢）由于化学成分不均匀，因此不适宜进行成品分析。

除此以外可由用户进行成品分析，允许偏差如下表所示。

一炉钢的不同次测定值对任一元素不应既超过允许最大值又低于允许最低值。

元素Ni Cr Mo V Nb Ti Al N规定的界限值或最大值，％≤1.00≤0.90≤0.20≤0.10≤0.10≤0.15≤0.10≤0.030低于下限－－－0.010.010.010.030.005允许偏差，％高于上限0.030.040.010.010.010.01－0.005*编者说明：本规范98年版的内容中关于成品分析允许偏差是规定了碳、锰、磷、硫、硅、铜等常规元素。

本98年版修改后元素全变，编者疑为改牌时要增加这些内容却将原内容而删掉（因原内容是薄板中主要元素），因此将96年版的成品分析允许偏差表列入（下表）供参考。

允许偏差％元素规定的界限值或最大值％低于下限高于上限碳≤0.15＞0.15～0.40＞0.40～0.80＞0.800.020.030.030.030.030.040.050.06锰≤0.60＞0.60～1.15＞1.15～1.650.030.040.050.030.040.05磷－0.01硫－0.01≤0.300.02 0.03 硅＞0.30～0.600.050.05铜0.02－（4）除非供需双方另有协议，在验证分析或仲裁分析时所使用的方法应按最新版本的ASTM A751。

5 力学性能1.力学性能要求、试样数量及取样位置、试样取向均应按相应产品规范的要求。

（2）除非产品规范中另有规定，试样制备、试验方法及操作应按ASTM A370。

弯曲试验（若有要求）应按ASTM E290。

石脑油检测

石脑油检测一：石脑油(003)石油脑，俗称轻油、白电油。

是石油提炼后的一种油质的产物。

它由不同的碳氢化合物混合组成。

它的主要成分是含5到11个碳原子的链烷、环烷或芳烃。

石油脑可用作提炼煤气之用。

二：主要检测产品主要检测产品：石油产品包括车用汽油、车用柴油、石脑油、溶剂油、甲醇汽油、生物柴油、航空煤油、燃料油、润滑油、润滑脂、石蜡、沥青、石油焦等产品。

? 石化产品包括石油苯、石油甲苯、对（邻、间）二甲苯、混合芳烃、甲基叔丁基醚、甲醇、乙醇、异丙醇、丁醇、乙二醇、二乙二醇、丙酮、丁酮、乙酸乙酯、乙酸异丙酯、乙酸甲酯、乙酸乙烯酯、丙烯酸、丙烯酸酯、乙腈、丙烯腈等产品。

三：主要检测项目辛烷值、抗爆指数、铅含量、馏程、蒸气压、实际胶质、诱导期、硫含量、博士试验或硫醇硫含量、铜片腐蚀、水溶性酸或碱、机械杂质及水分、苯含量、芳烃含量、烯烃含量、氧含量、甲醇含量、锰含量、铁含量。

运动粘度、倾点、表观粘度达150PaS时的温度、闪点、成沟点、粘度指数、起泡性、腐蚀试验、机械杂质、水分、戊烷不溶物、硫酸盐灰分、硫、磷、氮、钙、贮存稳定性、锈蚀试验、抗擦伤实验、承载能力、热氧化稳定性四：部分检测标准石油产品赛波特比色测试方法 ASTM D156-07a石油产品的蒸气压力的试验方法 ASTM D323-08数字密度计测定密度和液体相对密度的试验方法 ASTM D4052-09用毛细管气相色谱法对石油挥发油穿透壬烷详细分析的试验方法 ASTM D5134-98(2008) 大气压下石油产品蒸馏的标准试验方法 ASTM D86-09ε 1轻质石油产品铅含量测定法(原子吸收光谱法) SH/T 0242-1992石脑油中砷含量测定法(硼氢化钾-硝酸银分光光度法) SH/T 0629-1996科标能源检测中心是全国性、综合化、专业性的第三方检测服务机构，提供润滑油的分析测试、品级鉴定、化学分析等服务，为客户提供了准确可靠的检测数据。

HDPE物性数据表

①原料描述部分规格级别：电缆绝缘料外观颜色：本色用途概述：用于低、中、高速绝缘生产线备注说明：性能：由乙烯、丁烯集合而成的双峰高密度聚乙烯，并含有适量助剂的本色粒料。

因为其分子量呈双峰分布,所以它具有优异的加工性能、很好的力学性能及良好的电性能。

②原料技术数据性能项目试验条件［状态] 测试方法测试数据数据单位基本性能密度/ / 0.941—0。

959 g/cm3熔体流动速率/ / ≤1。

0 g/10min机械性能拉伸强度/ / ≥19。

0 MPa 断裂伸长率/ / ≥400% 耐环境应力开裂性48h / ≤2/10/电气性能介电常数1MHz / ≤2.40/体积电阻率/ / ≥1×1013Ω？m①原料描述部分规格级别：挤出级外观颜色：-—-用途概述：用途：供水管，工业用管子。

备注说明：特性：电子光谱法，高冲击和高强度。

②原料技术数据性能项目试验条件[状态］测试方法测试数据数据单位基本性能熔体流动速率/ ASTM D-1238 0。

12 g/10min 密度/ ASTM D—1505 0.950 g/cm3机械性能屈服拉伸强度/ ASTM D—638 220 Kg/cm2断裂拉伸强度/ ASTM D-638 390 Kg/cm2最终拉伸率/ ASTM D-638 〉500 ％挠曲强度/ ASTM D-747 8，500 Kg/cm2洛氏硬度/ ASTM D-785 50 R冲击强度/ ASTM D-256 30 kg？cm/cm 耐环境应力破裂/ ASTM D-1693 〉1,000 F50hr热性能脆化温度/ ASTM D—746 <—80 ℃熔点/ ASTM D-2117 131 ℃维卡软化点/ ASTM D—1525 122 ℃①原料描述部分规格级别：管材级外观颜色：—-—用途概述：农业排灌管、热水管、支架备注说明: 类型：挤塑②原料技术数据性能项目试验条件［状态] 测试方法测试数据数据单位基本性能熔体流动速率/ / 0.15 g/10min 密度/ / 0.954 g/cm3机械性能拉伸强度/ / 18。

ASTM D 98 – 98 Standard Specification for Calcium Chloride

D1This speciﬁcation is under the jurisdiction of ASTM Committee D-4on Road and Paving Materials,and is the direct responsibility of Subcommittee D04.31on Calcium and Sodium Chlorides.Current edition approved June10,1998.Published March1999.Originally published as D98–st previous edition D98–95.2Annual Book of ASTM Standards,V ol04.03.3Annual Book of ASTM Standards,V ol14.02.4Annual Book of ASTM Standards,V ol15.05.5Available from Standardization Documents Order Desk,Bldg.4,Section D, 700Robbins Ave.,Philadelphia,PA19111-5094,Attn:NPODS.6Available from American Trucking Association,Inc.,1616P St.,N.W., Washington DC20036.7Available from Uniform Classiﬁcation Committee,212Union Station,Chi-cago,IL60606.1AMERICAN SOCIETY FOR TESTING AND MATERIALS100Barr Harbor Dr.,West Conshohocken,PA19428 Reprinted from the Annual Book of ASTM Standards.Copyright ASTMand class of calcium chloride required (see Sections 3),4.1.3Quantity of calcium chloride required,4.1.4Whether special sampling for inspection is required (see Section 7),and4.1.5Whether special packaging and marking is required (see Section 10).5.Chemical Requirements5.1The calcium chloride shall conform to the following requirements for chemical composition,except for the toler-ances stated in 7.2.5.1.1CaCl 2content,%–not less than the minimum concen-tration speciﬁed,nor greater than the maximum concentration speciﬁed (when a maximum is speciﬁed).5.1.2Impurities content (not including water)–composition on anhydrous CaCl 2basis,with limits adjusted according to 5.2for the speciﬁc assay:Total alkali chlorides (as NaCl),max,%8.0Total magnesium as MgCl 2,max,%0.5Other impurities (see 5.1.2.1),max,%1.05.1.2.1Other impurities are those compounds,other than water (H 2O),not determined in the analysis of calcium chloride by Test Methods E 449.5.2Calculations for Allowable Impurities :5.2.1If the product assay shows 90.5%or more CaCl 2content,the impurities content in that product shall not exceed the limits shown in 5.1.5.2.2If the product assay shows less than 90.5%CaCl 2content,calculate the maximum allowable impurities concen-tration in that product as follows:A 5A 1SB 1002CD 5A 1S B90.5D(1)where:A 5impurity in assayed product,max %allowable,A 15impurity limit (on anhydrous basis)for that particu-lar impurity as speciﬁed in 5.1,max,%,B 5CaCl 2content in assayed product,%,andC 5total of all impurities permitted in anhydrous prod-uct,%(summation of maximum limits listed in 5.1).5.2.3Other impurities,%5100.0−(%CaCl 2+%NaCl +%KCl +%MgCl 2+%H 2O +%Ca(OH)2).6.Physical Requirements6.1The grading of solid form calcium chloride shall con-form to the requirements of Table 1for the grade and classspeciﬁed in the order.7.Sampling,Examination,and Testing7.1Sampling,examining,and testing of calcium chloride shall be done in accordance with Test Method D 345and E 449.When speciﬁed in the contract or purchase order,sampling for examination shall be performed in accordance with MIL-STD-105at an acceptable quality level speciﬁed by the purchaser.7.2Every facility shall be provided to the purchaser’s representative when the material is sampled at the plant.When the purchaser elects to sample the solid form material after delivery,a tolerance of three percentage points below the minimum CaCl 2requirement shall apply.When the purchaser elects to sample the liquid form material after delivery,a tolerance of one percentage point below the minimum CaCl 2requirement shall apply.8.Inspection8.1Unless otherwise speciﬁed in the contract or purchase order,the supplier shall be responsible for the performance of all inspection requirements as speciﬁed herein.8.2Except as otherwise speciﬁed,the supplier shall use his own facilities or any commercial laboratory acceptable to the purchaser for analysis of material.The purchaser reserves the right to perform any of the inspections set forth in this speciﬁcation where such inspections are deemed necessary to ensure that supplies and services conform to the prescribed requirements.9.Rejection9.1The calcium chloride shall be subject to rejection if it fails to conform to any of the requirements of this speciﬁcation or,in the case of the solid forms,if it has become caked or sticky in shipment.10.Packaging,Package Marking,and Shipping10.1Unless otherwise speciﬁed in the contract or purchase order,the calcium chloride in solid form shall be delivered in moisture proof bags containing not more than 45kg (100lb)nominal capacity each,or in airtight drums weighing not more than 204kg (450lb)nominal capacity each,or in bulk in tank cars,covered hopper cars,or covered trucks;and the calcium chloride in liquid form shall be delivered in bulk in tank trucks,tank cars,or barges.10.2Unless otherwise speciﬁed in the contract or purchase order,the name of the manufacturer,name of the product,netTABLE 1Sieve AnalysisSieve SizeMass %PassingGrade 1—77%min CaCl 2Grade 2—90%min CaCl 2Grade 3—94%min CaCl 2Class A FlakeClass B Granular Class A Flake Class B Pellets Class C Granular Class D Powder Class A Flake Class B Pellets Class C Granular Class D Powder 31.5mm 11⁄4in.............100.........100...9.5mm 3⁄8in.100100100100......100100......4.75mm No.480–1000–8080–10080–1000–510080–10080–1000–51002.36mm No.8...............80–100.........80–1001.18mm No.16..............................850µm No.20.........0–10.........0–10......600µmNo.300–50–50–50–5...0–650–50–5...0–65weight,and percentage of calcium chloride guaranteed by the manufacturer shall be legibly marked on each container for package shipments,or on the invoice or shipping papers accompanying bulk shipments.10.3When speciﬁed in the contract or purchase order as for Federal Government procurement,calcium chloride shall be prepared for shipment in accordance with the provisions speciﬁed in 10.4-10.6.2.10.4Packaging —Packaging for Federal Government pro-curement shall be Level A or C as speciﬁed (see Section 4.1.5).10.4.1Level A :10.4.1.1Unit Packaging —Calcium chloride in solid form shall be packaged in 0.45or 2.25-kg (1or 5-lb)quantities,as speciﬁed (see Section 10.4),in glass bottles conforming to Group A,Class 1,Style 2,Closure A of PPP-C-186.10.4.1.2Intermediate Packaging —Calcium chloride unit,packaged in accordance with 10.4.1.1shall be intermediately packaged in accordance with the Level A requirements of PPP-C-186.10.4.2Level C —Calcium chloride shall be packaged in the quantities speciﬁed (see Section 4.1.5),in accordance with supplier’s standard practice.10.5Packaging —Packing for Federal Government Procure-ment shall be Level A,B,or C as speciﬁed (see Section 4.1.5).10.5.1Level A :10.5.1.1For 0.45or 2.25-kg (1and 5-lb)Quantities —Calcium chloride,packaged in accordance with 10.4.1.1shall be packed in accordance with the Level A requirement of PPP-C-186.10.5.1.2For 36and 45-kg (80and 100-lb)Quantities —Calcium chloride,as speciﬁed (see 4.1.5),shall be packed in appropriate size sacks conforming to construction number 16X or 17X of UU-S-48,bags conforming to bag number P35B/A of PPP-B-35,or ﬁber drums conforming to Type III,Grade A,of PPP-D-723,as speciﬁed (see 4.1.5).Fiber drums shall beprovided with a polyethylene bag liner or other suitable water-vapor-proof liner or interior coating.10.5.2Level B :10.5.2.1For 0.45and 2.25-kg (1and 5-lb)Quantities —Calcium chloride,packaged in accordance with 10.4,shall be packed in accordance with the Level B requirements of PPP-C-186.10.5.2.2For 36and 45-kg (80and 100-lb)Quantities —Calcium chloride,as speciﬁed (see 4.1.5),shall be packed in appropriate size sacks conforming to construction number 8L/W or 14L/W of UU-S-48,bags conforming to bag number P35B of PPP-B-35,or ﬁber drums conforming to Type I,Grade A,of PPP-D-723,as speciﬁed (see 4.1.5).Fiber drums shall be provided with a polyethylene bag liner or other suitable water-vapor-proof lining or interior coating.10.5.3Level C —Calcium chloride shall be packed in quan-tities speciﬁed (see 4.1.5),in a manner which will ensure arrival at destination in satisfactory condition and be accept-able to the carrier at lowest rates.Containers and packing shall comply with the Uniform Freight Classiﬁcation rules or National Motor Freight Classiﬁcation rules.10.6Marking (see 4.1.5):10.6.1Civil Agencies —In addition to any special marking required by the contract or order,the interior packages and exterior shipping containers shall be marked in accordance with Fed.Std.No.123.10.6.2Military Activities —In addition,to any special mark-ing required by the contract or order,the interior packages and exterior shipping containers shall be marked in accordance with MIL-STD-129.11.Keywords11.1calcium chloride;concrete accelerator;concrete ad-mixture;deicing chemical;dessication;dust control;snow and ice removal;stabilizationThe American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connection with any item mentioned in this ers of this standard are expressly advised that determination of the validity of any such patent rights,and the risk of infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every ﬁve years and if not revised,either reapproved or withdrawn.Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM Headquarters.Your comments will receive careful consideration at a meeting of the responsible technical committee,which you may attend.If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards,100Barr Harbor Drive,West Conshohocken,PA19428.。

ASTM D类最新标准目录(一)

ASTM D类最新标准目录( 一）D4-86(2004) 沥青含量试验方法D5-06e1 沥青材料的渗透性试验方法D6-95(2000)e1 油及沥青混合物加热损失试验方法D8-02 与道路和路面材料相关的术语D9-05 与木材相关的术语D12-88(1998) 未加工的桐油D13-02 松节油规范D16-03 与涂料、清漆、亮漆和有关产品相关的术语D20-03 路面焦油的蒸馏试验方法D25-99(2005) 圆木桩D29-98 虫胶树脂的抽样和试验方法D34-91(2003) 白颜料化学分析指南D36-95(2000)e1 沥青软化点试验方法(沥青软化点测定器)D38-94(2000)e1 木材防腐剂的抽样试验方法D41-05 铺屋面、防潮及防水用沥青底层D43-00 屋顶、防潮及防水材料用杂酚油底漆D49-83(2002) 铅丹的化学分析D50-90(2005) 含铁和锰的黄色、橙色、红色和褐色涂料的化学分析试验方法D56-05 泰格密闭闪点试验器测定闪点的试验方法D61-75(2004) 硬沥青的软化点的试验方法(水中方块试验法)D69-01 磨擦带的试验方法D70-03 半固态沥青材料的比重和密度的试验方法D71-94(2004) 固体硬沥青和地沥青的相对密度试验方法(变位法)D75-03 集料的抽样D76-99(2005) 纺织材料的抗拉试验机D79-86(2004) 氧化锌颜料D81-87(2003) 碱性碳酸盐铅白颜料D83-84(2002) 铅丹颜料D85-05 赭色颜料规范D86-05 大气压下石油产品蒸馏试验方法D87-04 石蜡熔点的试验方法(冷却曲线)D88-94(2005) 赛波特粘度的试验方法D91-02 润滑油的沉淀值试验方法D92-05a 用克利夫兰德开杯法测定石油产品的闪点和燃点的试验方法D93-02a 用潘斯基-马丁斯仪闭杯闪点测定器测定闪点的试验方法D94-02 石油产品的皂化值试验方法D95-05e1 蒸馏法测定石油产品及沥青材料中水的试验方法D97-05a 石油的倾点的试验方法D98-05 氯化钙D113-99 沥青材料的延展性的试验方法D115-02 电绝缘用含清漆试验溶剂的试验方法D116-86(2006) 电气设备用上釉陶瓷材料的试验D117-02 产自石油的电绝缘油的试验方法和规范导则D120-02a 橡胶绝缘手套D121-05 煤和焦炭术语D123-03 与纺织材料相关的术语D124-88(1998) 脱胶的豆油D126-87(2002) 含铬酸铅和氧化铬绿的黄、橙和绿色颜料的化学分析方法D127-05 石油蜡包括凡士林滴熔点的试验方法D128-98(2003)e1 润滑脂分析试验方法D129-00(2005) 石油产品中硫含量试验方法(通用氧弹法)D130-04e1 用铜条变色法检测石油产品对铜腐蚀性的测试方法D139-95(2001)e1 沥青材料浮选试验的检测方法D140-01 沥青材料的抽样D143-94(2000)e1 洁净木材小样品的试验D146-04 防水与屋面材料用沥青浸渍的油毡和编织物的抽样与试验方法D149-97a(2004) 固体电绝缘材料在工业电源频率下的介电击穿电压和介电强度的试验方法D150-98(2004) 固体电绝缘材料的(恒久电介质)的交流损耗特性和介电常数的测试方法D153-84(2003) 颜料比重测试方法D154-85(2001) 清漆试验D156-02e1 石油产品赛波特比测试方法(赛波特比色计法)D167-93(2004)e1 块焦比重和孔隙度的试验方法D168-94(2000) 杂酚油焦炭渣的测试方法D173-03 屋顶和防水材料用饱和沥青棉织物D176-00 电绝缘用固体充填化合物与浸渍剂的试验方法D178-01(2005) 橡胶绝缘垫子D185-84(1999 颜料,糊剂及涂料中粗颗粒的试验方法D187-94(2003)e1 煤油燃烧质量的测试方法D189-05 石油产品康拉孙残碳测试方法D197-87(2002) 粉煤的取样方法与细度试验方法D198-05a 结构尺寸木料静力试验法D202-97(2002)e1 电绝缘用未浸渍纸的抽样和试验方法D204-02 缝线的测试方法D209-81(2003) 灯黑颜料D210-05 骨炭颜料D211-67(2002) 铬黄和铬橙颜料D215-91(2002) 白色亚麻籽油涂料的化学分析D217-02 润滑剂针入度的测试方法D225-04 表面有矿物颗粒的沥青屋面板D226-06 铺顶和防水用沥青饱和有机毡D227-03 铺顶和防水用焦油沥青饱和有机毡D228-06 沥青屋面卷材,盖板和瓦的试验方法D229-01 电绝缘用硬质薄板及板材的试验方法D233-02 松脂的抽样和测试试验方法D234-82(1998) 生亚麻子油D235-02 矿物溶剂油(石油溶液油)(烃干洗溶液)规格D237-57(1997) 橙色紫胶和其他虫胶D240-02 弹式量热器测定液烃燃料燃烧热的试验方法D242-04 沥青铺路混合料用矿物填料D243-02 规定残渣渗透性测试方法D244-04 乳化沥青的测试方法D245-06 制定目测分等木材的结构等级及有关允许性能的规程D246-04 杂酚油和杂酚油-煤焦油溶液的蒸馏试验方法D256-06 塑料及电绝缘材料的抗冲击性的测试方法D257-99(2005) 绝缘材料的直流电阻或电导的试验方法D260-86(2001) 熟亚麻籽油D261-75(1999) 铁蓝颜料D262-81(1999) 群青蓝颜料D263-05 氧化铬绿颜料D267-82(2003) 黄青铜粉规格D268-01 涂料及其相关涂层和原料用挥发性溶剂及化学中间体的抽样和测试D269-97(2002) 松香和松香衍生物中不溶物的试验方法D276-00a 纺织品中纤维的鉴定方法(AATCC方法20)D279-02 颜料渗出的试验方法D280-01 颜料吸收的水份(及试验条件下挥发的其他物质)的测试方法D281-95(2002) 用刮刀磨损法测定颜料油吸附性的试验方法D283-84(1999) 一氧化铜和铜涂料化学分析试验方法D287-92(2006) 原油和石油产品API比重的试验方法(液体比重计法)D291-86(2002) 烟煤立方英尺重量的试验方法D293-93(2004) 焦炭筛析分析试验方法D295-99(2004) 电绝缘用棉质漆布的试验方法D297-93(2002)e2 橡胶制品的测试方法.化学方法D299-04e1 石棉纱的标准规范D301-95(2004) 可溶性硝化纤维素的试验方法D304-05 n-丁醇(丁醇)D305-84(2003) 黑色涂料中的溶剂萃取材料的试验方法D312-00 屋顶用沥青D315-95(2004)e1 机织石棉带的标准规范D319-04 合成的戊醇D322-97(2002)e1 蒸馏法测定汽油发动机废机油中汽油稀释剂的试验方法D323-99a 石油产品蒸气压力的测试方法D329-02 丙酮D330-93(2001) 2-丁氧基乙醇D331-05 2-乙氧基乙醇D332-87(2004) 白色颜料着色力的试验方法D333-01 透明漆和着色漆的试验方法D341-03 液体石油产品粘度-温度关系曲线图D344-97(2004) 用擦试外规评定法对涂料相对遮盖力的测试方法D345-02 道路和结构用氯化钙的抽样和试验方法D346-04e1 实验室分析用焦炭试样的收集和制备D347-97 杂酚油和煤焦油的体积和比重修正表D348-00 电绝缘用刚性管的测试方法D349-99(2004) 电绝缘用层压圆棒的试验方法D350-01 电绝缘用经处理软套管的试验方法D351-97(2003) 天然白云母块及薄片目检质量分级D352-97(2003) 电绝缘用涂浆云母的试验方法D358-98 涂料耐大气老试验用木片规格D360-89(2001) 紫胶清漆规范D363-90(2000) 磷酸三甲苯酯规格D365-01(2005) 可溶性硝酸纤维素基溶液的试验方法D367-94(2000)e1 杂酚油中苯不溶物的测试方法D368-89(2002) 杂酚油及油质防腐剂比重的试验方法D369-84(2002) 杂酚油馏份与残渣比重的测试方法D370-02e1 油质防腐剂脱水作用的试验方法D372-00(2006) 电绝缘用经处理的软套管规格D374-99(2004) 固体电绝缘厚度的测试方法D374M-99(2005) 固体电绝缘厚度的标准测试方法(米制)D375-95(2004)e1 石棉粗砂的标准规范D378-00 平型橡胶传送带的测试方法D380-94(2006) 橡胶软管的测试方法D381-04 用喷射蒸发法测定燃烧中原在胶的测试方法D387-00 使用机械研磨机测定有色颜料主色和着力色的试验方法D388-05 用排列法测定煤的分类D390-92(1999) 海上,陆地及淡水中用木桩,电杆和木材的防腐处理用煤柏油杂酚油规程D391-94(2000)e1 杂酚油-煤焦油溶液D395-03 橡胶压缩永久变形特性的试验方法D396-05 燃料油规范D402-02 稀释沥青产品蒸馏的测试方法 Standard Test Method for Distillationof Cut-Back Asphalt ic (Bituminous) ProductsD409-02 粉碎机法测定煤炭可磨性的试验方法 Standard Test Method for Grindabilityof Coal by t he Hardgrove-Machine MethodD411-98(2003) 电绝缘用紫胶片试验方法 Standard Test Methods for ShellacUsed for Electrical I nsulationD412-98a(2002)e1 硫化橡胶、热塑橡胶和热塑合成橡胶的拉伸试验方法 Standard Test Methods f or VulcanizedRubber and Thermoplastic Elastomers—TensionD413-98(2002)e1 橡胶特性-与软质基底粘附性的试验方法 Standard Test Methods for RubberPro perty—Adhesion to Flexible SubstrateD420-98(2003) 土壤粒度分析的测试方法 Standard Guide to SiteCharacterization for Engineering, Design, and ConstructionPurposesD421-85(2002) 土壤粒度分析试验方法 Standard Practice for Dry Preparationof Soil Samples for Particle-Size Analysis and Determination ofSoil ConstantsD422-63(2002)e1 土壤粒度分析试验方法 Standard Test Method forParticle-Size Analysis of Soils D425-88(2001) 土壤离心湿度当量试验方法 Standard Test Method for CentrifugeMoisture Equiva lent of SoilsD427-04 用水银法测量土壤收缩系数的测试方法 Test Method for Shrinkage Factors ofSoils by t he Mercury MethodD429-03e1 橡胶特性与硬质基底粘附性的试验方法 Standard Test Methods for RubberProperty—Adhesion to Rigid SubstratesD430-06 橡胶变质的动态疲劳试验方法 Standard Test Methods for RubberDeterioration-Dynamic FatigueD434-95 Standard Test Method for Resistance toSlippage of Yarns in Woven Fabrics Using a St andard SeamD440-86(2002) 煤的跌落粉碎试验 Standard Test Method of Drop ShatterTest for CoalD441-86(2002) 煤的滚筒试验 Standard Test Method of Tumbler Test for CoalD444-88(2003) 锌黄颜料(铬酸锌黄)的化学分析方法 Standard Test Methods for Chemical Analysis of Zinc YellowPigment (Zinc Chromate Yellow)D445-06 透明和不透明液体运动粘度的测试方法.(包括动态粘度的计算) Standard Test Method for Kinematic Viscosity ofTransparent and Opaque Liquids (and the Calculation of DynamicViscosity)D446-06 玻璃毛细管运动粘度计操作说明书和规范 Standard Specifications and OperatingInstructi ons for Glass Capillary Kinematic ViscometersD448-03a 道路和桥梁建筑的集料尺寸分类 Standard Classification for Sizes ofAggregate for Roa d and Bridge ConstructionD449-03 防潮和防水用沥青规范 Standard Specification for AsphaltUsed in Dampproofing and WaterproofingD450-96(2006) 铺屋面,防潮与防水用硬煤沥青 Standard Specification for Coal-TarPitch Used in Roofing, Dampproofing, and WaterproofingD451-91(2002) 沥青屋顶制品用粒状矿物铺面材料筛分分析试验方法 Standard Test Method for Si eveAnalysis of Granular Mineral Surfacing For Asphalt RoofingProductsD452-91(2002) 沥青层面制品表面修整用非粒状矿物的筛分试验方法 Standard Test Method for Si eveAnalysis of Surfacing for Asphalt Roofing ProductsD453-94(2000)e1 杂酚油-煤焦油溶液中焦油酸含量的测试方法 Standard Test Method for Tar Aci ds inCreosote-Coal Tar SolutionsD454-04 用加热及空气压力测定橡胶变质的试验方法 Standard Test Method for RubberDeteriorat ion by Heat and Air PressureD459-00 肥皂和其它洗涤剂的术语规范 Standard Terminology Relating toSoaps and Other Deter gentsD460-91(2005) 肥皂和其它洗涤剂粒度的试验方法 Standard Test Methods for Samplingand Che mical Analysis of Soaps and Soap ProductsD464-05 松脂油产品包括妥尔油和其他相关产品的皂化值的试验方法 Standard Test Methods for Saponification Number of Naval Store Products Including Tall Oil and Other Related ProductsD465-05 松脂制品包括妥尔油及其它相关产品酸值的试验方法 Standard Test Methods for Acid N umberof Naval Stores Products Including Tall Oil and Other RelatedProductsD470-05 电线和电缆用交联绝缘与套管的测试方法 Standard Test Methods for CrosslinkedInsulati ons and Jackets for Wire and CableD471-98e2 液体对橡胶性能影响的测试方法 Standard Test Method for RubberProperty-Effect of LiquidsD473-02 萃取法测定原油和燃料油中沉积物的试验方法 Standard Test Method for Sediment inCr ude Oils and Fuel Oils by the Extraction MethodD476-00(2005) 二氧化钛颜料规范 Standard Classification for DryPigmentary Titanium Dioxide P roductsD478-02 锌黄(铬酸锌)颜料 Standard Specificationfor Zinc Yellow (Zinc Chromate) PigmentsD480-88(2003) 铝粉和铝粉浆的抽样和试验方法 Standard Test Methods for Samplingand Testin g of Flaked Aluminum Powders and PastesD482-03 石油产品灰分的测试方法 Standard Test Method for Ash fromPetroleum ProductsD483-04 石油制植物喷洒油不磺化残渣的试验方法 Standard Test Method for UnsulfonatedResidu e of Petroleum Plant Spray OilsD490-92(2005) 道路柏油 Standard Specification for Road TarD494-04 Standard Test Method for Acetone Extraction ofPhenolic Molded or Laminated Products Standard TestMethod for Acetone Extraction of Phenolic Molded or LaminatedProductsD495-99(2004) 固体电绝缘材料的耐高压低电流干电弧性能的测试方法 Standard Test Method for High-Voltage, Low-Current, Dry Arc Resistance of Solid ElectricalInsulationD500-95(2003) 磺化油和硫化油的化学分析和试验方法D501-03 碱性洗涤剂的抽样和化学分析试验方法D502-89(2003) 肥皂和其它洗涤剂粒度的试验方法D509-05 松香分级和抽样试验方法D511-03 水中钙镁离子的测试方法D512-04 测定水中氯离子含量的试验方法D513-02 水中二氧化碳溶解量和总量的试验方法D516-02 水中硫酸铁的试验方法D517-98(2003) 沥青厚板材D518-99 橡胶变质表面龟裂的试验方法D519-04 羊毛条中纤维长度的试验方法D520-00(2005) 锌粉颜料规范D521-02 锌粉(金属锌粉)的化学分析试验方法D522-93a(2001) 用锥形心轴仪测定涂覆有机涂层延伸率的试验方法D523-89(1999) 镜面光泽的试验方法D524-04 石油产品中兰氏残炭的试验方向D525-05 汽油氧化稳定性的试验方法(诱导期方法)D528-97(2002) 纸和纸板的机器定向试验方向D529-04 沥青材料的加速风化试验条件和程序的测试方法(碳弧法)D531-00(2005) 普西和琼斯橡胶压缩试验方法D542-00 透明有机塑料的折射指数的试验方法D543-06 塑料耐化学试剂性能的试验方法D545-99(2005) 混凝土用预制伸缩缝纫填料的试验方法(非挤压和弹性型)D546-05 道路和铺砌材料用矿物填料筛分的测试方法D548-97(2002) 纸张水溶解酸碱度的试验方法D555-84(1998) 干性油试验D558-04 土壤水泥混合物的水分与密度关系的试验方法D559-03 压实的掺土水泥混合物的湿润与干燥的试验方法D560-03 压实的掺土水泥混合物的冻融试验方法D561-82(2003) 涂料用炭黑颜料D562-01(2005) 斯氏粘度计测定涂料稠度的试验方法D563-88(1996)e1 醇酸树脂和树脂溶液中苯酐含量的试验方法D564-87(2002) 液体涂料催干剂的试验方法D565-99(2005) 白色矿物油中可碳化物质的试验方法D566-02 润滑脂滴点的试验方法D570-98(2005) 塑料吸水率的试验方法D572-04 用加热法和氧化法进行的橡胶变质的试验方法D573-04 在空气烤炉中作橡胶变质的试验方法D575-91(2001) 橡胶压缩特性的试验方法D578-05 玻璃纤维丝D579-04 原织物玻璃纤维D580-04 机织玻璃纤维带D581-99 机织玻璃纤维套管的编织D584-96(2005) 原毛中羊毛含量实验室测试方法D585-97(2002) 纸张、纸板、纤维板和相关产品的单批取样和验收方法D586-97(2002) 纸中灰分含量的试验方法D589-97(2002) 纸的不透明度的测试方法D590-93(2002) 纸中石油蜡的测试方法D596-01 水分析结果的报告D600-90(2001) 液体涂料催干剂D601-87(1998) 奥气油(永久液体)D602-81(2003) 硫酸钡颜料规范D605-82(2003) 硅酸镁颜料(滑石)D607-82(2003) 湿磨云母颜料D608-05 邻苯二甲酸二丁酯D609-00 涂料、油漆以及改性涂料与相关涂料产品的测试用冷轧钢板的制备D610-01 涂漆钢表面锈蚀程度评价的试验方法D611-04 石油产品和烃类溶剂苯胺点和混合苯胺点的试验方法D612-88(2004) 石蜡中可碳化物质的试验方法D613-05 十六烷法测定柴油燃料燃烧质量的试验方法D618-05 塑料及电绝缘材料的调理方法D619-99(2004) 电绝缘用硫化纤维的测试方法D622-99(2005) 汽车空气制动和真空制动系统用橡胶软管试验方法D623-99e1 橡胶特性-压缩中热的产生及挠曲疲劳的试验方法D624-00e1 橡胶的热塑性弹性的耐老化性的抗撕裂强度的试验方法D628-95(2004)e1 石棉套管的标准规范D629-99 纺织品定量分析试验方法D632-01 氯化钠D633-97(2005) 道路柏油的体积修正表D635-06 自承塑料在水平状态时的燃烧速率或者燃烧蔓延程度及燃烧时间的试验方法D638-03 塑料拉伸性能的试验方法D642-00(2005) 船用集装箱、组合件和单体加载的抗压缩能力的测试方法D643-97(2002) 用厦泊测试仪测试纸的折痕持久性的标准试验方法D644-99(2002) 用烘干法测定纸和纸板中水分的测试方法D645/D645M-97(2002) 纸和纸板厚度的测试方法D646-96(2001) 纸张及纸板的基本重量的试验方法(单位面积的重量)D648-06 在挠曲负荷下塑料的挠曲温度的试验方法D653-05 土壤、岩石和其内部所含液体的相关术语D660-93(2005) 外用漆龟裂程度评价方法D661-93(2005) 外用漆破裂程度评价的试验方法D662-93(2005) 外用漆侵蚀程度评价的试验方法D664-06 电位滴定法测定石油产品酸值的试验方法D665-06 水存在下抑制的矿物油防锈特性的试验方法D668-99(2004) 电绝缘用硬条和硬管尺度测量的测试方法D669-03 层压薄板与层压板的平行于层片的耗散系数和介电常数的试验方法D685-93(2002) 检测调理纸和纸制品D686-93(2002) 纸中矿物填料和矿物涂料的定性测试方法D689-03 纸张的内部耐撕裂的试验方法D692-00(2004) 沥青铺路砌混合用粗集料D693-03a 碎石路面用压碎集料D695-02a 硬质塑料抗压特性的试验方法D696-03 从-30摄氏度到30摄氏度的塑料线性热膨胀系数的试验方法D698-00ae1 实验室中用12000ft-lbt/ft(600KN-m/m)作用力测定土壤压力特性的试验方法D704-99(2004) 三氯氰胺甲醛模制化合物D705-99(2004) 脲甲醛模制化合物D706-05 乙酸纤维素模制和挤压化合物D707-05 醋酸丁酸纤维素模制与挤压料规格D709-01 层压热固材料D710-97(2002) 电绝缘用硫化纤维薄板、条和管D711-89(2004) 路标漆不粘着时间的试验方法D713-90(2004) 路标漆进行路面使用的试验方法D714-02e1 涂料起泡程度的试验方法D715-86(2003) 硫酸钡颜料分析的标准试验方法D716-86(2003) 评定云母颜料的标准试验方法D717-86(2003) 硅酸镁颜料分析的标准试验方法D718-86(2003) 硅酸铝颜料的分析标准试验方法D720-91(2004)e1 煤自由膨胀指数的试验方法D721-05 石油蜡含油量的试验方法D722-93(2002) 纸的抗油脂性标准试验方法D724-99(2003) 纸表面可湿性的测试方法(接触角法)D726-94(2003) 空气中无孔纸的透气性的测试方法D727-96(2001) 真空方法测定屋顶和地板油毡煤油值的试验方法D731-95(1999) 热固模塑料粉末的模塑指数的试验方法D732-02 用穿孔工具测量塑料剪切强度的测试方法D737-04 纺织纤维透气率的试验方法D740-05 丁酮规范D746-04 用冲击法测定塑料及弹性材料的脆化温度的试验方法D747-02 用悬臂梁法对塑料表观弯曲系数的测试方法D748-00(2005)e1 固定式云母介电电容器用天然云母块和云母薄片D750-00 用碳弧型装置和风化装置对橡胶变质的测试方法D751-06 涂层织物的测试方法D763-01 未加工棕土和焙烧棕土颜料D765-87(2003) 未加工黄土和焙烧黄土颜料技术规范D768-01 黄色氧化铁的水合物D769-01 黑色合成氧化铁D770-05 异丙醇规范D772-86(2005) 外部涂料剂落程度评价的试验方法D774/D774M-97(2002) 纸张抗破碎强度的测试方法D776-92(2001) 干热对纸和纸板特性的影响的试验方法D777-97(2002) 经过处理的纸和纸板易燃性的标准试验方法D778-97(2002) 纸萃液(热萃取和冷萃取法)氢离子浓度(pH)的标准试验方法D779-03 纸、纸板和其他印刷材料用干烧指示器法测试耐水性的测试方法D780-95(2003) 纸印刷油墨渗透性的测试方法(蓖麻油试验)D784-03 电绝缘材料用橙色紫胶和其他印度虫胶D785-03 塑料和电绝缘材料的洛氏硬度的测试方法D787-96(2003) 乙基纤维模制和挤压化合物D788-05 甲基丙烯酸酯模制和挤压化合物的分类系统D789-06 聚酰胺相对粘度,熔点和含水量的测试方法D790-03 未增强和增强塑料及电绝缘材料的挠曲性的试验方法D792-00 用位移法测定塑料密度和比重(相对密度)的标准试验方法D800-05 工业用金属除垢剂化学分析试验方法D801-02 二聚戊烯抽样和测试的试验方法D802-02 松油抽样和测试的试验方法D803-03 妥儿油的测试试验方法D804-02 松脂制品包括妥儿油及相关产品的术语D806-00(2006) 掺土水泥混合物中水泥含量的试验方法D807-05 工业锅炉用水引起脆裂倾向的评价方法(美国矿业局的脆变检查器方法)D808-05 新的和使用过的石油产品中氯含量的试验方法(氧弹法)D813-06 测定橡胶龟裂扩展的试验方法D814-95(2005) 橡胶特性挥发性液体蒸汽渗透性的试验方法D816-06 橡胶胶水的试验方法D817-96(2004) 乙酸丙酸纤维素和醋酸丁酸纤维素的试验方法D820-93(2003) 含合成洗涤剂肥皂的化学分析试验方法D822-01 用经过过滤明光碳弧灯和水中曝光装置对涂料及相关涂层和材料上做的导电试验D823-95(2001) 色漆,清漆,喷漆及有关产品制成厚度均匀漆膜试片的方法D824-94(2002) 用皱文纸测定吸水率的测试方法D828-97(2002) 纸和纸板拉力破坏强度的测试方法D829-97(2002) 纸和纸制品湿抗拉断裂强度的标准试验方法D831-94(2004) 电缆及电容器油的气体含量的测试方法D832-92(2001)e1 低温状态下的橡胶试验D841-02 甲苯的硝化定级D843-06 硝化二甲苯D847-04 苯,甲苯,二甲苯,溶剂石脑油和类似的工业芳烃酸度的试验方法D848-03 工业芳烃的酸洗颜色的标准试验方法D849-05 工业芳烃对铜条腐蚀的标准试验方法D850-03 工业芳轻及相关物质的蒸溜法D852-02 苯凝固点的试验方法D853-04 工业芳烃中硫化氢和二氧化硫含量(定性)的标准试验方法D854-06 土壤比重的试验方法D857-02 水中铝含量的测试方法D858-02 水中锰含量的试验方法D859-05 水中二氧化硅的测试方法D861-01a 用特克斯制命名纤维,纱的半制品,纱和其它纺织品线度D865-99(2005) 橡胶的空气中加热变质试验方法(试管法)D866-99(2004) 电线及电缆用丁苯合成橡胶套D868-85(2003) 路标漆渗色程度评价的试验方法D869-85(2004) 涂漆沉降程度评价试验方法D870-02 水浸渍法涂层耐水试验D871-96(2004) 测试乙酸纤维素的试验方法D873-02 航空燃料的氧化稳定性的测试方法D874-06 润滑油和添加剂中硫酸盐类灰分的测试方法D876-00 电绝缘用刚性氧化乙烯聚合物管的测试方法D877-02e1 用圆盘电极测定电绝缘液体介电击穿电压的试验方法D878-01e1 绝缘油中无机氯化物和硫酸盐的测试方法D880-92(2002) 船用集装箱的冲击试验的试验方法D882-02 塑料薄板材抗拉特性的试验方法D883-00 塑料相关术语D885-06 由人造有机纤维制成的轮胎帘子线,轮胎帘布和工业长纱线的测试D887-82(2003)e1 水沉积物抽样D888-05 水中溶解氧的试验方法D889-99(2004) 松香中油挥发性的试验方法D890-98(2003) 液体松脂中水含量的试验方法D891-95(2004) 液态工业化合物的比重,表观比重的测试方法D892-05 润滑油发泡特性的标准试验方法D893-05a 用过的润滑油中不溶物的试验方法D896-04 胶粘剂耐化学试剂粘法的试验方法D897-01e1 胶粘剂粘结力的抗拉性的测试方法D898-05 胶粘剂固体单位面积涂用重量的试验方法D899-00 单位面积涂用液体胶粘剂的重量的测试方法D902-00 电绝缘用挠性涂树脂玻璃布和玻璃布带的测试方法D903-98(2004) 胶粘剂粘结抗剥落或爆皮强度的试验方法D904-99(2005) 人造光(碳弧型)和自然光对胶粘剂试样的曝光D905-03 用压缩荷载法测定胶粘剂的抗剪切强度性能的试验方法D906-98(2004) 用拉力负荷法测定胶合板结构中胶粘剂剪切强度特性的试验方法D907-05e1 胶粘剂术语D909-01e1 增压进料法测定航空汽油抗震性的试验方法(联邦试验方法No.791b) D910-04a 航空汽油技术规范D912-81(1999) 防污涂料用氧化亚铜D913-03e1 路标漆耐磨程度的评价方法D914-00(2006) 乙基纤维的试验方法D918-99(2003) 纸和纸板的抗粘结性试验方法D919-97(2002) 纸和纸板的铜值测试方法D922-00a(2006) 非硬质聚氯乙烯管D923-97 电绝缘液体的抽样方法D924-04 电绝缘液体的损耗因数(或功率因数)和介电常数(电容率)的测试方法D925-06 橡胶特性.表面着色(接触、色移和扩散)的试验方法D926-04 用平行板法测量橡胶的塑性和弹性D928-03 碳酸氢钠D932-85(2002) 水和水沉积物中嗜铁细菌含量试验方法D933-84(2003) 水沉积物的检验和分析结果的报告方法D934-80(2003) 用X射线衍射法作水沉积物中结晶化合物的识别方法D937-04 石油脂的针入度试验方法D938-05 石油蜡(包括凡士林)凝固点的测试方法D942-02 氧弹法测定润滑脂氧化稳定性的试验方法D943-04a 防腐蚀矿物油氧化特性的试验方法D945-06 用机械示波器测定在压缩应力和剪切应力下橡胶特性的试验方法D946-82(2005) 路面建造用按贯入度级配的沥青膏D950-03 胶粘剂抗冲击强度的试验方法D951-99(2004) 用喷射法测定船运集装箱的耐水性的试验方法D952-02 薄板塑料和电绝缘材料粘结强度的试验方法D953-02 塑料支承强度的测试方法D955-00 模制塑料模型尺寸收缩率的测量方法D957-95(2006)e1 塑料生产用模型表面温度的测定D960-02a 生蓖麻油D961-86(2001) 脱水蓖麻油D962-81(2003) 涂料用铝粉和铝浆颜料D964-03 防污漆用铜粉D968-05 用落沙磨蚀法测定有机涂层耐磨性的试验方法D969-85(2003) 路标漆渗色程度的实验室试验方法D971-99a(2004) 环法测定油水界面张力的试验方法D972-02 润滑脂和润滑油蒸发损失的测试方法D974-04 用颜色指示剂滴定法测定酸碱值的标准试验方法D975-06 柴油技术规范D976-04be1 馏分燃料正十六烷指数的计算方法D977-05 乳化沥青D979-01(2006)e1 沥青铺面混合料的取样方法D982-05 Standard Test Method for Organic Nitrogen in Paper andPaperboard D984-97(2002)。

钢号对照表

SK1
W2-13,
W1-121/2
1200Y2135
Y13
T7A
1105Y165
Y7A
T8A
C80W1(1.1525)
(VDEh)
1104Y175
Y8A
T8MnA
C85WS(1.1830)
(VDEh)
Y8ГA
T9A
1103Y190
9YA
T10A
C105W1(1.1545)
(VDEh)
Y10A
T11A
35Г2
40Mn2
Smn443 (SMn3)
1340
1340
1340
40Г2
45Mn2
Smn443 (SMn3)
1345
1345
1345
45Г2
50Mn2
1052
1052
1552
(1052)
50Г
(2)硅锰钢组
27SiMn
27CГ
35SiMn
37MnSi5(1.5122)
35CГ
42SiMn
46MnSi4(1.5121)
080A15
Fe 360 B
Fe 360 C
Fe 360 B
Fe 360 C
Q 235 B
Fe 360 D
CT3KP-3
CT3PC-3
CT3CP-3
Gr.D
SS 400
(SS41)
SM 400A
(SM41A)
Fe 360 B
Fe 360 C
080A15
Fe 360 B
Fe 360 C
Fe 360 B
1021,
1022
1021,
1022

CBR试验规程

室内载重比试验1.目的：于试验室进行载重比试验，以求得贯入杆贯入土壤的阻抗和贯入标准碎石阻抗之比值(载重比)与土壤干密度之关系，以提供现场填土品质控制之参考。

2.设备：a.夯实试验设备：包括标准夯实试验或改良式夯实试验设备。

b.CBR试验模具：包括内径15.2cm，高度12.7cm之试体夯模6组，及配合夯模使用之延伸环、垫块、多孔底钣、膨胀延伸器、膨胀架等。

c.贯入杆：断面积3in2之圆柱形贯入杆。

d.超载基钣：直径约150mm之圆形铅钣，中央打孔，孔径50.8mm(2 in)，钣重4.54kg(10lb)。

e.抗压主机：采用计测公司制造之机械式抗压主机，负载能力5吨以上。

f.量测系统：包括冲程5.0cm、精度0.01mm，量测轴向变位之测微表，以及负载容量5吨以上、精度0.1kg量测贯入阻抗之压力衡圈。

g.其他：药刀、戒尺、水槽、调土设备、大型电子秤、含水量量测设备等。

3.试验方法：a.依据设计求进行土壤夯实试验，并求得试验土壤之最佳含水量(OMC)及最大乾密度(rdmax)。

b.依据所得土壤最佳含水量调配土样，并将土样分成三层(五层)，各以每层10下、30下、65下之夯击次数，将土样夯入下衬垫块之CBR模具中，重模三组不同夯实能量之试体。

c.去除模具延伸环，将试体表面刮平後翻转试体，并去除模具底部垫块。

d.将翻转後之试体固定於底钣上，加上超载基钣後将其安装於抗压主机上，并以手动控制使试体表面与抗压机上之贯入杆微微接触。

e.启动抗压机，以1.27mm/min之速率使贯入杆压入试体中。

f.利用量测系统读取贯入杆贯入量及其对应之贯入阻抗，至贯入阻抗下降或贯入量达12.7mm以上为止。

g.将土样自模具中顶出，分上、中、下三部份分别采取部份土样一并进行含水量测定。

h.重复b~c步骤，并於试体上下加装滤纸後，将试体固定於多孔底钣上，加上膨胀延伸器、超载基钣、膨胀架及测微表後将全部设备置於水槽中，加水使水淹过试体顶部，同时记录土体膨胀量达96小时或膨胀量不再增加为止。

(完整版)ASTMD类最新标准目录(四).doc

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带连续线性封合的包装件用持久扭矩测量的测试方法D2064-91(2003) 建筑涂料抗污染性的标准试验方法D2065-03 在表面活化剂加速潮湿应力下测量组合木材产品边棱性能的测试方法D2066-06 印刷油墨色散的相对着色力测试方法D2067-97(2003) 印刷油墨分散剂中粗颗粒的测试方法D2068-04 馏出燃料油过滤器阻塞倾向的测试方法D2070-91(2001) 液压油热稳定性的试验方法D2071-87(1998) 脂族氮制品的试验方法D2072-92(1998)e1 脂族氮化合物中水的试验方法D2073-92(1998)e1 仲裁电势测定法测定脂肪胺,酰胺基胺及二元胺的总胺值,伯胺值,仲胺值和叔胺值的试验方法D2074-92(1998) 交替指示剂法测定脂肪胺中总胺值,伯胺值,仲胺值和叔胺值的试验方法D2075-92(1998) 脂肪胺,酰胺基胺及二元胺碘值的试验方法D2076-92(1998) 脂族季铵氯化物中酸值和胺值的测试方法D2077-92(1998) 脂族季铵氯化物中灰分的测试方法D2079-92(1998) 脂族季铵氯化物中不挥发物质(固体)的测试方法D2080-92(1998) 脂族季铵氯化物平均分子量的测试方法D2081-92(1998) 脂族季铵氯化物中pH值的测试方法D2082-92(1998) 脂族氮化合物中非胺物百分比的测试方法D2083-92(1998) 脂肪胺中伯,仲,叔胺百分比的计算测试方法D2084-01 橡胶性能的测试方法.用振动圆盘硫化计测量硫化作用。

astmd类最新标准目录（二）doc

ASTM D类最新标准目录(二）.docD985-97(2002) 纸浆、纸和纸板亮度的试验方法(方向反射系数457nm)D991-89(2005) 橡胶特性.导电橡胶及抗静电橡胶制品的体电阻系数测试方法D994-98(2003) 混凝土用预制伸缩缝填充料(沥青型)D995-95b(2002) 热搅拌、热铺沥青铺面混合料用搅拌设备D996-04 包装及分配环境的术语D999-01 船运集装箱的振动试验方法D1000-04 电气设备用压合敏感胶粘剂涂覆带的试验方法D1002-05 用拉力负载测定金属之间胶粘剂抗剪切强度特性的试验方法D1003-00 透明塑料混浊度和透光系数的测试方法D1004-03 塑料薄膜和薄板的抗撕裂强度的测试方法D1005-95(2001) 用千分尺测量有机涂层干膜厚度的试验方法D1006-01 木材表面涂料的室外暴露试验D1007-05 仲丁醇D1013-93(1998) 树脂和塑料中总氮量的测试方法D1014-02 钢材表面涂料室外暴露试验方法D1015-05 高纯度烃冻结点的测试方法D1016-05e1 冻结点测定烃纯度的试验方法D1018-00(2005) 石油馏分中氢含量的测试方法D1025-00(2004) 聚合级丁二烯中不挥发性残余物的试验方法D1030-95(1999) 纸和纸板纤维分析的试验方法D1036-99(2005) 木电杆的静态试验方法D1037-99 木质纤维板和刨花板的性能评定方法D1038-83(2005) 薄板和胶合板相关术语的定义D1039-94(2004) 电绝缘用玻璃粘合云母的试验方法D1042-01a 在加速使用状态下塑料线性尺寸变化的标准试验方法D1043-02 用扭转试验法测定温度对塑料强度变化的试验方法D1044-05 透明塑料表面耐磨蚀性的试验方法D1045-95(2001) 塑料用增塑剂的取样与试验方法D1047-95(2001) 电线及电缆用聚氯乙烯套管D1048-05 橡胶绝缘毡层D1049-98(2002)e1 橡胶绝缘封盖物D1050-05e1 橡胶绝缘衬里套管D1051-02 橡胶绝缘管D1052-05 用罗斯挠曲装置测定橡胶切口扩展的试验方法D1053-92a(2001)e1 橡胶特性试验.挠性聚合物和涂覆制品的低温劲度测试方法D1054-02e1 用回跳摆锤法测定橡胶弹性的试验方法D1055-04 韧性多孔材料.泡沫胶乳D1056-00 韧性多孔材料-海绵状或膨胀橡胶D1059-01 基于短长度样品的纱线支数试验方法D1060-96(2005) 为测定净毛纤维百分率从成包原毛中心取样D1061-95(2004)e1 石棉卷标准规范D1062-02 金属间粘结力抗裂强度的标准试验方法D1065-96(2001) 松脂制品(包括松香、松油和相关产品)中不可皂化物的测试方法D1066-97(2001) 蒸汽的抽样方法D1067-02 水的酸性和碱性的测试方法D1068-05e1 水中铁的测试方法D1070-03 气体燃料相关密度的试验方法D1071-83(2003) 气体燃料试样容积的测量方法D1072-06 燃料气中总硫量的测试方法D1073-06 沥青铺面混合料用细集料D1074-02 沥青混合料抗压强度的测试方法D1075-96(2005) 水对压实的沥青混合料粘结力影响的试验方法D1076-06 橡胶.浓缩的、氨储存的、乳状的和离心处理的天然胶乳D1078-05 挥发性有机液体馏程的试验方法D1079-05a 铺屋面材料、防水材料和沥青材料的相关术语D1082-00(2005) 云母耗散因数和介电常数的测量方法D1084-97(2005) 胶粘剂粘度的测试方法D1091-00(2005) 润滑油和添加剂中磷含量的测试方法D1092-05 润滑脂表观粘度的试验方法D1093-04 液态烃和它们的蒸馏残余物酸度的测试方法D1094-00(2005) 航空燃料水反应性的试验方法D1101-97a(2006) 室外用层压结构木制品的胶合接头完整性的试验方法D1102-84(2001) 木材中灰分的测试方法D1105-96(2001) 无提取物木材的制备D1106-96(2001) 木材中酸不溶木素的测试方法D1107-96(2001) 木材的醇苯可溶性试验方法D1108-96(2001) 木材中二氯甲烷溶解物的测试方法D1109-84(2001) 木材在百分之一的烧碱中可溶性的试验方法D1110-84(2001) 木材水溶解度的测试方法D1113-90a(2001) 洗净羊毛中植物性物质和其它碱性不溶杂质的测试方法D1117-01 无纺织物试验方法D1118-95(2004)e2 石棉纤维和石棉织物磁参数的标准测试方法D1119-05 发动机冷却剂与防锈剂的灰分含量的测试方法D1120-94(2004) 发动机冷却剂沸点的测试方法D1121-98(2003) 发动机抗冻剂、防锈剂和冷却剂储备碱度的测试方法D1122-97a(2002) 用液体比重计测量发动机冷却剂及其浓缩物比重的试验方法D1123-99(2003) 用KarlFischer试剂法测试发动机冷却剂浓缩物的试验方法D1125-95(2005) 水的电导性和电阻率的测试方法D1126-02 水硬度的测试方法D1129-06 与水相关的术语D1133-04 烃类溶剂的贝壳杉脂丁醇值的测试方法D1135-86(2004) 蓝色颜料化学分析的标准试验方法D1139-00(2004) 单层或多层沥青表面处理用集料D1140-00 土壤中小于200号(75微米)筛孔的材料总量的测试方法D1141-98(2003) 海水代用品D1142-95(2006) 露点温度法测定气体燃料中蒸汽含量的试验方法D1143-81(1994)e1 静态轴向压力荷载下桩柱的试验方法D1144-99(2005) 胶粘剂粘结强度提高的测定方法D1146-00 有效粘结层粘结点的试验方法D1148-95(2001) 橡胶变质.受热及紫外线使浅颜色表面退色的试验方法D1149-99 橡胶变质试验.在小室中橡胶表面臭氧龟裂D1151-00 潮气和温度对胶粘剂粘结能力影响的试验方法D1152-06 甲醇(甲基醇)D1153-06 甲基异丁基甲酮D1155-03 玻璃球圆度的测试方法D1157-91(2004) 轻质烃总抑制剂含量(TBC)的测试方法D1159-01 电化学滴定法测量石油馏分及商用脂族烯烃的溴值试验方法D1160-06 石油产品减压蒸馏方法D1165-03 生活中用硬木和软木的命名法D1166-84(2001) 木材及有关材料中甲氧基团的测试方法D1168-99(2003) 电绝缘用石蜡的测试D1169-02e1 电绝缘液体电阻率(电阻系数)的测试方法D1171-99 橡胶变质试验.室外或小室内橡胶表面臭氧龟裂(三角形试样)D1172-95(2001) 肥皂和洗涤剂水溶液pH值的测试方法D1173-53(2001) 表面活性剂起泡性试验方法D1176-98(2002) 试验用发动机冷却剂或防锈剂水溶液的取样和制备方法D1177-05 发动机冷却剂溶液冻结点的测试方法D1179-04 水中氟化物离子的测试方法D1183-03 胶粘剂耐周期性实验室老化条件的标准试验方法D1184-98(2004) 胶粘剂粘结的层压部件抗挠强度的试验方法D1185-98a(2003) 在材料搬运和船运中托盘和有关设备的试验方法D1186-01 铁基非磁性涂层干膜厚度的无损测量方法D1187-97(2002)e1 金属保护涂层用沥清乳液D1188-96(2002)e1 用涂石蜡样品测定压实的沥青混合料的体积比重和密度的试验方法D1193-06 试剂水(联邦试验方法No.7916)D1195-93(2004) 用于公路路面和机场跑道设计和评定的土壤与韧性路面成份的往复静态平板荷载的测试方法D1196-93(2004) 用于公路和机场路面设计和评定的土壤与韧性路面成份的非往复静立平板荷载试验方法D1198-93(1998) 胺基树脂溶剂容限的测试方法D1199-86(2003) 碳酸钙颜料技术规范D1200-94(2005) 福特粘度杯测定粘度的试验方法D1201-99(2004) 热固聚酯模制化合物D1203-94(2003) 用活性碳法测定塑料的挥发损失的试验方法D1204-02 高温下非硬性热塑塑料薄板或薄膜线性尺寸变化的测试方法D1208-96(2002) 某些颜料通性的试验方法D1209-05 透明液体色度的试验方法(铂钴标度)D1210-05 颜料载体体系分散细度的测试方法D1212-91(2001) 木材用透明硝基清漆漆膜耐温度变化的试验方法D1214-04 有机涂层湿膜厚度的测试方法D1217-93(2003)e1 用宾汉比重法测定液体密度和相对密度(比重)的试验方法D1218-02 液态烃的折射率和折射分散度的测试方法D1223-93(1998) 75度下纸和纸板镜面光泽的试验方法D1224-92(2001) 纸中锌和镉的试验方法D1227-95(2000) 屋面保护涂层用乳化沥青D1229-03 橡胶特性试验方法.低温时的压缩变形率D1230-94(2001) 服装纺织品的易燃性的测试方法D1234-85(2001) 含脂羊毛的手扯长度的取样和试验方法D1238-04c 用挤压塑性计测定热塑性塑料流率的测试方法D1239-98 用化学制剂测量塑料薄膜的抗萃取性测试方法D1240-02 包括松香,高脂油和相关产品中心存储的松香酸含量的测试方法D1241-00 土壤集料次底层、底层和表层用料D1243-95(2000)e1 氯乙烯聚合物的稀溶液粘度的试验方法D1244-98(2005) 纱线结构的名称D1245-84(2003) 用化学显微镜作水沉积物的检验D1246-05 水中的溴化物离子的测试方法D1248-05 聚乙烯塑料模制和挤压材料D1249-92(1999) 辛基正酞酸酯增塑剂D1250-04 石油测量表D1252-06 水化学氧需要量(重铬酸盐氧需要量)的测试方法D1253-03 水中残余氯的测试方法D1257-90(2001) 高比重甘油D1258-05 高比重甘油的试验方法D1259-06 树脂溶液的不挥发物含量的测试方法D1263-94(2005)e1 汽车轮轴承润滑脂泄漏倾向的试验方法D1264-03e1 润滑脂水洗出性能的试验方法D1265-05 液化石油(LP)气取样(手工法)D1266-98(2003)e1 石油产品中硫的试验方法(燃灯法)D1267-02 液化石油(LP)气气压的测试方法(液化石油气法)D1272-56(2002) 五氯苯酚D1274-95(2000) 五氯苯酚的化学分析方法D1275-06 电绝缘油中腐蚀性硫的测试方法D1278-91a(2002)e1 天然橡胶的试验方法.化学分析D1280-00 浸槽式金属除垢剂的全浸腐蚀试验的试验方法D1282-05 用气流阻力表示羊毛毛条,生条和洗净羊毛的平均纤维直经的测试方法D1283-05 羊毛碱溶性的测试方法D1287-91(2002) 发动机冷却剂和防锈剂的pH值的试验方法D1290-95(2002) 用离心机测定水乳化抛光剂中沉积物的试验方法D1291-01 氯的需求量或水的需求量或两者兼有的评估D1292-05 水的气味的测试方法D1293-99(2005) 水的pH值测试方法D1294-05 在1英寸(25.4毫米)长度内羊毛纤维拉伸强度和断裂强度试验方法D1296-01 挥发性溶剂和烯释剂气味的试验方法D1298-99(2005) 用石油密度计法测定原油和液体石油产品密度,相对密度(比重)或API比重的试验方法D1301-91(2003) 白铅颜料化学分析的标准试验方法D1304-99(2005) 与电绝缘试验相关的胶粘剂D1305-99(2004) 电绝缘纸和纸板.硫酸盐(牛皮纸)层型D1306-88(1996)e1 醇酸树脂和含有其它二元酸的酯类的酞酸含量测试方法(重量法)D1308-02e1 家用化学品对透明和着色有机面漆影响的试验方法D1309-93(2004) 贮藏期间交通标志用色漆的沉淀特性的测试方法D1310-01 用泰格开口杯装置测定液体闪点和燃点的测试方法D1312-93(1998) 涂层用合成酚醛树脂或溶液中表观游离酚的测试方法D1316-06 用美国油墨研究会研磨测量计测定油墨研磨细度的测试方法D1318-00(2005) 测定残留燃料油中钠试验方法(火焰光度测定法)D1319-03e1 用萤光指示剂吸附法测定液态石油产品中烃类物质的试验方法D1321-04 石油蜡针入度测试方法D1322-97(2002)e1 航空涡轮机燃料烟点的试验方法D1325-94(2000) 氨化砷酸铜D1326-94(2000) 氨化砷酸铜的化学分析法D1327-04 铺屋面和防水用浸沥青物质的机织粗麻布D1329-02 评定橡胶特性的试验方法.低温下的回缩(TR试验)D1330-04 薄橡胶衬垫D1331-89(2001) 表面活性剂溶液的表面张力与界面张力的试验方法D1334-05 原毛毛含量的测试方法.商业尺度D1335-05 毛绒地毯绒毛束粘合试验方法D1336-97(2003) 机织纱线扭曲度试验方法D1337-04 用稠度和粘结强度测定胶粘剂贮藏寿命的试验方法D1338-99(2005) 用稠度和粘结强度测定液态或糊状胶粘剂使用寿命的试验方法D1342-92(2002) 巴西棕榈蜡中石蜡型烃含量的测试方法D1343-95(2006) 用落球法测定纤维素衍生物粘度的测试方法D1348-94(2003) 纤维素中湿度的测试方法D1349-99(2005) 橡胶.试验温度D1351-02 电线和电缆用聚乙烯绝缘材料D1352-02 电线和电缆用耐臭氧的丁基橡胶绝缘材料D1353-03 色漆,清漆,喷漆及相关产品用挥发性溶剂中不挥发物质的试验方法D1356-05 与大气取样和分析相关的术语D1357-95(2005) 制定外围大气的取样计划D1360-98(2004) 涂料阻燃性试验方法(小室法)D1363-06 丙铜和甲醇的高锰酸盐时间的测试方法D1364-02 挥发性溶剂中水的测试方法(费歇尔试剂滴定法)D1366-86(2003) 颜料粒度特性报告D1367-96(2001)e1 石墨润滑质量的测试方法D1369-84(2006) 沥青表面处理用材料的数量D1370-00 沥青材料间接触相容性的试验方法(奥林萨斯试验)D1384-05e1 玻璃器皿中发动机冷却剂腐蚀试验的测试方法D1385-01 水中肼含量的测试方法D1386-98(2004) 合成和天然蜡的酸值(经验)的测试方法D1387-89(2002) 合成和天然蜡皂化值(经验)的测试方法D1388-96(2002) 织物硬挺性测试方法D1389-97a(2004) 薄固体电绝缘材料的校验电压试验的试验方法D1392-92(1998) 红花油D1394-76(2003) 钛白颜料化学分析的标准试验方法D1396-92(1998) 聚乙烯缩丁醛化学分析的标准试验方法D1397-93(1998) 醇酸树脂和树脂溶液中不皂化物的测试方法D1398-93(1998) 醇酸树脂和醇酸树脂溶液的脂肪酸含量测试方法D1399-95(2000) 磷酸三甲苯酯不可皂化物含量的测试方法D1400-00 非铁金属基表面非传导涂层干膜厚度无损测量的测量方法D1401-02 石油和合成液体水溶解性的试验方法D1403-02 用1/4和1/2标度锥形设备测定润滑脂锥入度的试验方法D1404/D1404M-99(2003) 评定润滑脂中有害粒子的测试方法D1405-01(2006) 平定航空燃料净燃烧热的测试方法D1411-04 分级集料筑路搅拌物中作为掺合物的溶水氯化物的测试方法D1412-04 在96%-97%相对湿度和30℃时煤的平衡湿气的测试方法D1413-05b 用实验室土块培养法测试木材防腐剂D1414-94(2003) O型橡胶圈的试验方法D1415-05 橡胶特性的测试方法.国际硬度D1417-03a 合成橡胶胶乳的测试方法.D1418-06 橡胶和橡胶胶乳.命名D1422-99 退捻加捻法测定单纱捻数的试验方法D1423-02 直接计算法测定纱线捻数的试验方法D1424-96(2004) 埃尔曼多夫落锤仪测定机织物抗撕裂的试验方法D1426-03 用电容测试设备测定纱线条干不匀度的测试方法D1429-03 水中氨态氮的测试方法D1430-03 水和盐水的比重的测试方法D1434-82(2003) 聚氯三氟乙烯(PCTFE)塑料D1435-05 测定塑料薄膜和薄片透气性能的测试方法D1436-97(2002) 塑料的室外风化D1439-03 试验用乳胶地板基质抛光剂的使用D1440-96(2002) 羧甲基纤维素钠盐的测试方法D1441-06 棉纤维长度和长度分布的试验方法(列阵法)D1442-06 试验用棉纤维取样D1445-05 棉纤维成熟度的试验方法(烧碱膨胀与偏振光法)D1447-00 用纤维照相法测定棉纤维的长度和长度均匀度的测试方法D1448-05 棉纤维的马克隆尼读数的试验方法D1452-80(2000) 用螺旋钻作土壤勘探和取样D1455-87(2002) 乳化地板抛光剂60度镜面光泽度的试验方法D1456-86(2005) 橡胶特性的测试方法.特定应力下的延伸D1458-01 电绝缘用完全硫化硅橡胶涂层的玻璃布与玻璃带的试验方法D1459-93(2003) 电绝缘用硅清漆涂层的玻璃布和玻璃带D1460-86(2005) 橡胶性能的测试方法.液体浸没期间的长度变化D1461-85(2006) 沥青铺砌混合料中水份或挥发性馏份含量的测试方法D1462-92(1998) 精制豆油技术规范D1464-90(2002) 棉花染色差异性的试验方法D1465-04 石油蜡的熔点和粘着点的测试方法D1468-93(2001) 磷酸三甲苯酯中挥发物质的试验方法D1474-98(2002) 有机涂层压印硬度的试验方法D1475-98(2003) 色漆,清漆,喷漆及相关产品密度的试验方法D1476-02 喷漆溶剂的庚烷混溶性试验方法D1478-02 滚珠轴承润滑脂低温转矩的试验方法D1480-02e1 用宾汉比重计测定粘性材料密度和相对密度(比重)的试验方法D1481-02 用利普金双毛细管比重计测定粘性材料密度和相对密度(比重)的试验方法D1483-95(2002) 用加纳尔--科尔曼法测定颜料的吸油量的试验方法D1485-86(2002) 从天然原料中获取橡胶的方法.取样和样品制备D1488-00 胶粘剂中淀粉物质的测试方法D1489-97(2004) 含水胶粘剂不挥发物含量的测试方法D1490-01 脲甲醛树脂溶液中不挥发物含量的测试方法D1492-02 库仑计滴定法测定芳烃溴指数的测定方法D1494-97(2001)e1 增强塑料板的散射光透射系数的测试方法D1498-00 水的氧化还原潜能D1499-05 操纵塑料暴露用曝光和曝水装置(碳弧型)D1500-04a 石油产品ASTM颜色的试验方法(ASTM比色度)D1505-03 用密度梯度法测定塑料密度的试验方法D1506-99 碳黑的测试方法.灰分含量D1508-02e2 粒状碳黑的测试方法.精粒含量D1509-95(2000) 碳黑的测试方法.加热损耗D1510-06a 炭黑碘吸收值的测试方法D1511-00(2006) 碳黑的测试方法.片状尺寸分布D1512-05 碳黑的测试方法.pH值D1513-05 片状碳黑的测试方法.顷注密度D1514-04 碳黑测试方法.筛渣D1516-05 皮革宽度的测试方法D1517-04e1 与皮革相关的术语定义D1518-85(2003) 纺织材料的热传导的试验方法D1519-95(2004)e1 橡胶化学制品的试验方法.溶化范围D1523-00 工作温度为90℃的电线和电缆用合成橡胶绝缘材料D1524-94(2004) 用过的石油制电绝缘油的现场目测检查的方法D1525-06 塑料维卡(Vicat)软化温度的测试方法D1527-99(2005) 丙烯腈-丁二稀-苯乙稀塑料管.40号表和80号表D1531-01e1 用液体位移法测定介电常数与耗散系数的试验方法D1533-00(2005) 绝缘液体中水的试验方法(卡耳费瑟反应法)D1534-95(2002)e1 用比色指示剂滴定法测定电绝缘液近似酸度的试验方法D1535-06 用孟塞尔制规定颜色的测试方法D1537-60(1998) 蒸馏的大豆脂肪酸D1538-60(1998) 蒸馏的亚麻籽脂肪酸D1539-60(1998) 脱水蓖麻籽脂酸D1541-97 干性油及其衍生物总碘值的试验方法D1544-04 透明液体颜色的测试方法(加德纳色度)D1545-98 用起泡时间法测定透明液体粘度的试验方法D1546-96(2003) 透明地板密封剂的性能试验D1550-94(2005) ASTM丁二烯测量表D1552-03 石油产品中硫含量的试验方法(高温法)D1554-01(2005) 与木基纤维和刨花板材料相关的名词术语定义D1555-04a 工业芳烃体积和重量的计算方法D1555M-04a 工业香烃类计量的体积和重量计算的标准测试方法D1556-00 用砂锥法现场测定土壤密度和单位重量的测试方法D1557-02e1 用修正作用力56000ft-Ibf/ft(2700 KN-m/m)测量土壤实验室压实性能的测试方法D1558-99(2004)e1 细粒土水含量渗透阻力关系的试验方法D1560-05e1 用赫维门(Hveem)装置测定沥青混合物抗变形和粘结性的试验方法D1561-92(2005)e1 用搅拌压实机法制作沥青混合物试样D1562-05 纤维素丙酸盐模制和挤压物D1566-06 与橡胶相关的术语D1568-05 烷基苯磺酸盐的取样与化学分析的标准试验方法D1569-05 烷基洗涤剂的试验方法D1570-95(2003) 脂肪烷基硫酸盐的取样与化学分析的测试方法D1571-95(2004)e1 石棉布的标准规范D1573-95(2004)e1 石棉织物热老化的标准测试方法D1574-04 Standard Test Method for Extractable Matter in Wool andOther Animal Fibers D1575-90(2001) 洗净羊毛及生条中羊毛纤维长度的测试方法D1576-90(2001) 用炉烘干法测定羊毛内水分的试验方法D1577-01 纺织纤维线密度的测试方法D1578-93(2006)e1 绞纱形式下纱线的断裂强度的试验方法D1579-01 苯酚,间苯二酚和三聚氰胺胶粘剂中填料含量的测试方法D1582-98(2004) 液相苯酚,间苯二酚和三聚氰胺胶粘剂中不挥发物含量的测试方法D1583-01 干粘膜中氢离子浓度的测试方法D1585-96(2003) 中心仓库中松香,妥尔油和相关产品的脂肪酸含量测试方法D1586-99 渗透试验和土壤开管取样的试验方法D1587-00 泥土薄壁管抽样D1593-99 非硬性氯乙烯塑料薄板D1596-97(2003) 包装材料减震性能的试验方法D1598-02 恒定内压下塑料管的破裂时间的测试方法D1599-99(2005) 塑料管,管道和配件的短时破裂水压的测试方法D1600-99 与塑料相关的缩略名词术语D1601-99(2004) 乙烯聚合物稀溶液粘度的测试方法D1603-06 烯烃塑料中碳黑测试方法D1607-91(2005) 大气中二氧化氮含量的测试方法(格里斯-沙耳茨曼反应)D1608-98(2003) 气态燃烧产物中氧化氮的测试方法(苯酚二磺酸法)D1610-01 试验用皮革和皮革制品的修整D1611-00(2005) 皮革与金属接触时产生腐蚀的试验方法D1612-05 甲醇(木精)中丙酮含量的测试方法D1613-06 色漆,清漆,喷漆和有关产品用挥发性溶剂和化学介质中酸度的试验方法D1614-03 丙酮中碱度的试验方法D1617-90(2001) 溶剂和稀释剂酯化值的试验方法D1618-99(2004) 碳黑的可萃取性测验方法.甲苯脱色D1619-03 碳黑的测试方法.硫含量D1621-04a 硬质泡沫塑料的压缩特性的试验方法D1622-03 硬质泡沫塑料的表观密度的测试方法D1623-03 硬质泡沫塑料张力和张力粘合性能的试验方法D1624-71(2000) 酸性铬酸铜D1625-71(2000) 铬酸盐砷酸铜D1627-94(2000) 酸性铜铬酸盐的化学分析D1628-94(2000) 铬酸盐砷酸铜的化学分析的测试方法D1630-06 橡胶特性的试验.耐磨性(NBS磨损机)D1631-99(2004) 用碘试剂法测定苯酚和有关原料中水分的试验方法D1632-96 试验室中水泥土压缩试样和挠曲试样的制作和养护D1633-00 模制水泥土圆筒的抗压强度的试验方法D1634-00(2006) 用横梁弯曲断裂部分测定水泥土抗压强度的试验方法(改良立方体法) D1635-00(2006) 用简支梁三点负荷法测定水泥土抗挠强度的试验方法D1636-99(2004)e1 烯丙基模制化合物D1639-90(1996)e1 有机涂料酸值试验方法D1640-03 室温下有机涂料干燥,固化及成膜试验方法D1641-04 外用清漆耐用性的试验方法D1644-01(2006) 清漆中不挥发物含量试验方法D1646-04 橡胶的测试方法.粘度和硫化特性(穆尼粘度计)D1647-89(1996)e1 清漆干膜耐水性和耐碱性试验方法D1648-86(2003) 碱式硅铬酸盐颜料D1649-01 铬酸锶颜料D1652-04 环氧树脂中环氧含量的试验方法D1653-03 有机涂层薄膜水蒸气渗透性测试方法D1654-05 腐蚀环境中涂漆或加涂层样件评估的标准试验方法D1655-06a 航空涡轮机燃料D1657-02 用压力液体比重计测定轻烃类物质的密度或相对密度的标准试验方法D1662-92(2002) 切削润滑油中活性硫的测试方法D1665-98(2003) 柏油制品的恩氏比粘度的测试方法D1666-87(2004) 木材和木基材料的传导机械试验D1667-05 软质泡沫材料.氯乙烯聚合物及共聚物(闭孔泡沫)D1668-97a(2006) 铺屋面和防水用玻璃织物(机织和经处理)D1669-03 沥青材料在加速风化与室外风化用试片的制备D1670-04 沥青材料在加速风化与室外风化中端点损坏的测试方法D1673-94(2004) 电绝缘用充气泡沫塑料的介电常数与耗散系数的测试方法D1675-03 聚四氟乙烯管的试验方法D1676-03 带绝缘薄膜的磁性导线的测试方法D1677-02 电绝缘用未处理云母纸的取样和试验D1679-02 工作温度为75℃的电线和电缆用合成橡胶耐热防潮绝缘材料D1681-05 按阳离子滴定程序对洗涤剂中合成阴离子活性成分的测试方法D1683-04 机织物缝纫接缝瑕疵的试验方法D1684-96(2002) 颜色分级用棉分级室的照明D1685-05 用分光光度计测定苯中微量噻吩的试验方法D1686-96(2004) 溶融状态中固体芳烃与相关材料的颜色的测试方法(铂钴标度) D1687-02 水中铬含量的测试方法D1688-02 水中铜含量的测试方法D1691-02 水中锌含量的测试方法D1693-05 乙烯塑料的环境应力破裂的试验方法D1694-95(2000) 玻璃纤维(玻璃纤维增强热固树脂)管用60度螺纹(短管)D1695-96(2001) 纤维素和纤维素衍生物的术语D1696-95(2006) 纤维素在氢氧化钠中溶解度的试验方法D1698-03 用过的老化绝缘油中沉淀物与可溶性淤渣的试验方法D1708-06 用微型抗拉试样对塑料抗拉特性的测试方法D1709-04 用钢锥自由下落法对塑料薄膜的抗冲击强度的测试方法D1710-02 聚四氟乙烯(PTFE)基本型材,棒材和厚壁管材D1711-02 电绝缘术语D1712-03 塑料抗硫化物污染D1718-03 乙酸异丁酯(95%)D1719-05 异丁醇D1720-03 &%。

ASTMD类最新标准目录(四).doc(最新整理)

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Designation:D6160–98Standard Test Method forDetermination of Polychlorinated Biphenyls(PCBs)in Waste Materials by Gas Chromatography1This standard is issued under theﬁxed designation D6160;the number immediately following the designation indicates the year of original adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.A superscript epsilon(e)indicates an editorial change since the last revision or reapproval.1.Scope1.1This test method2is a two-tiered analytical approach to PCB screening and quantitation of liquid and solid wastes, such as oils,sludges,aqueous solutions,and other waste matrices.1.2Tier I is designed to screen samples rapidly for the presence of PCBs.1.3Tier II is used to determine the concentration of PCBs, typically in the range of from2to50mg/kg.PCB concentra-tions greater than50mg/kg are determined through analysis of sample dilutions.1.4This is a pattern recognition approach,which does not take into account individual congeners that might occur,such as in reaction by-products.This test method describes the use of Aroclors31016,1221,1232,1242,1248,1254,1260,1262, and1268,as reference standards,but others could also be included.Aroclors1016and1242have similar capillary gas chromatography(GC)patterns.Interferences or weathering are especially problematic with Aroclors1016,1232,and1242and may make distinction between the three difficult.N OTE1—Aroclor is a registered trademark of Monsanto.1.5This test method provides sample clean up and instru-mental conditions necessary for the determination of Aroclors. Gas chromatography(GC)using capillary column separation technique and electron capture detector(ECD)are described. Other detectors,such as atomic emission detector(AED)and mass spectrometry(MS),may be used if sufficient performance (for example,sensitivity)is demonstrated.Further details about the use of GC and ECD are provided in Practices E355,E697, and E1510.1.6Quantitative results are reported on the dry weights of waste samples.1.7Quantiﬁcation limits will vary depending on the type of waste stream being analyzed.1.8This standard does not purport to address all of the safety concerns,if any,associated with its use.It is the responsibility of the user of this standard to establish appro-priate safety and health practices and determine the applica-bility of regulator limitations prior to use.2.Referenced Documents2.1ASTM Standards:D4059Test Method for Analysis of Polychlorinated Biphe-nyls in Insulating Liquids by Gas Chromatography4E203Test Method for Water Using Karl Fischer Reagent5 E288Speciﬁcation for Laboratory Glass Volumetric Flasks6E355Practice for Gas Chromatography Terms and Rela-tionships6E697Practice for Use of Electron-capture Detectors in Gas Chromatography6E969Speciﬁcation for Glass V olumetric(Transfer)Pipet6 E1510Practice for Installing Fused Silica Open Tubular Capillary Columns in Gas Chromatography62.2U.S.EP A Standards:Method608Organochlorine Pesticides and PCBs Environ-mental Monitoring and Support Laboratory,Cincinnati, Ohio.EPA Report600/4/82–057.7Method680Determination of Pesticides and PCBs in Water and Soil/Sediment by Gas Chromatography/Mass Spec-trometry8Method3620Florisil Column Clean-Up9Method3630Silica Gel Clean-Up9Method3660Sulfur Clean-Up9Method8082Determination of PCB in Water and Soil/1This test method is under the jurisdiction of ASTM Committee D02on Petroleum Products and Lubricants and is the direct responsibility of Subcommittee D02.04on Hydrocarbons Analysis.Current edition approved Nov.10,1998.Published January1999.Originally published as D6160–st previous edition D6160–97.2This test method is based largely on EPA8080(and the proposed modiﬁcation for the use of capillary columns,EPA8081)and EPA Report600/4–81–045by Bellar,T.and J.Lichtenberg,reported in1981.The report is titled,“The Determination of Polychlorinated Biphenyls in Transformer Fluid and Waste Oils”and provides signiﬁcant support to the protocol below.3Aroclor Standards may be purchased as1000ug/mL in iso octane.4ASTM Annual Book of Standards,V ol.10.03.5ASTM Annual Book of Standards,V ol.15.05.6ASTM Annual Book of Standards,V ol.14.02.7EPA Report600/4/82–057.“Organochlorine Pesticides and PCBs”Environ-mental Monitoring and Support Laboratory,Cincinnati,OH.8“Determination of Pesticides and PCBs in Water and Soil/Sediment by Gas Chromatography/Mass Spectrometry”,Ann Alford-Stevens et al,Physical and Chemical Methods Branch,Environmental Monitoring and Support Laboratory Office of Research and Development,USEPA,Cincinnati,OH45268.6 9U.S.EPA,“Test Methods for Evaluating Solid Waste,Physical/Chemical Methods,”SW-846.1Copyright©ASTM International,100Barr Harbor Drive,PO Box C700,West Conshohocken,PA19428-2959,United States.Sediment by Gas Chromatography:Capillary Column Technique93.Terminology3.1Deﬁnitions of Terms Speciﬁc to This Standard:3.1.1Aroclors,n—commercial mixtures of polychlorinated biphenyl congeners marketed and trademarked by Monsanto prior to1977.3.1.1.1Discussion—Speciﬁc Aroclors are usually desig-nated by a four-digit number,with theﬁrst two digits usually designating the number of carbon atoms and the last two digits providing the chlorine content(for example,Aroclor1260is60 %(weight)chlorine).3.1.2congeners,n—compounds related by structural simi-larities.3.1.2.1Discussion—All polychlorinated biphenyls(PCBs) share the same C12structure and vary only by the number and position of the chlorine atoms attached to the aromatic rings.3.1.3continuing calibration standard(CCS)—a known blend or one or more Aroclors at aﬁxed concentration that is injected into the gas chromatograph to demonstrate the validity of the calibration.3.1.4dry weight,n—concentration of PCBs after factoring out the water content.3.1.4.1Discussion—This correction assumes that all PCBs originated from nonaqueous sources and any water present has been added subsequently,diluting the original concentration. This correction can be described using the formula:Aroclor~mg/Kg!~dry!5Aroclor~mg/Kg!~wet!~1002%water!/100(1)3.1.5instrument performance standard(IPS),n—a known low level of an Aroclor in a clean solvent used as a comparator to determine which qualitative(screening)results are of sufficient magnitude to require quantitative analyses.3.1.6surrogate,n,n—compound or compounds that are similar to analytes of interest in chemical composition,extrac-tion,and chroatography,but that are not normally found at signiﬁcant levels in the matrices of interest.3.1.6.1Discussion—Surrogates may be spiked into blanks, standards,samples,or matrix spikes prior to analysis to allow a determination of a quantitative recovery rate.Surrogates are also used to document matrix effects and method control. 3.1.7waste material,n—any matter,within the scope of this test method,that is in the process of being recycled or disposed.4.Summary of Test Method4.1The sample is extracted with solvent and the extract is treated to remove interfering substances,if needed.The sample extract is injected into a gas chromatograph.The components are separated as they pass through the capillary column and polychlorinated biphenyl compounds,if present,are detected by an ECD.N OTE2—Portions of this test method are similar to EPA Methods608, 680,and8082.4.2For screening(Tier I),instrument performance is moni-tored by a2-uL injection of a standard containing Aroclors 1016and1260.For low level work(1ppm)the instrument is checked with a standard concentration of0.01ug/mL(each) and for higher level work(10ppm),the instrument is checked with a0.1ug/mL standard.4.3Identiﬁcation involves a pattern comparison of the chromatograms of an unknown sample with that of a standard obtained under identical instrumental conditions.4.4When quantiﬁcation is required(Tier II),an external standards method(ESTD)is used.The quantitation technique typically requires a comparison ofﬁve peaks(minimum of three)between the chromatograms of an unknown sample and that of standard Aroclor obtained under identical conditions. Quantitation of either Aroclors1016or1260is performed using aﬁve-point calibration of a mixed Aroclor standard containing Aroclors1016and1260.All remaining Aroclors are quantitated from single point calibrations.Calibration is veri-ﬁed daily by comparison of results obtained for analysis of the midpoint calibration standard of Aroclar1016and1260to the ﬁve-point calibration curve.(See Appendix X1for an example chromatogram and calibration table.)5.Signiﬁcance and Use5.1This test method provides sufficient PCB data for many regulatory requirements.While the most common regulatory level is50ppm(dry weight corrected),lower limits are used in some locations.Since sensitivities will vary for different types of samples,one shall demonstrate a sufficient method detection limit for the matrix of interest.5.2This test method differs from Test Method D4059in that it provides for more sample clean-up options,utilizes a capillary column for better pattern recognition and interference discrimination,and includes both a qualitative screening and a quantitative results option.6.Interferences6.1The ECD has selective sensitivity to alkyl halides, conjugated carbonyls,nitrogen compounds,organometallics, and sulfur.Therefore,the chromatogram obtained for each sample shall be carefully compared to chromatograms of standards to allow proper interpretation.6.2Solvents,reagents,glassware,and other sample process-ing hardware may yield artifacts or interferences,or both,to standard analysis.All these materials shall be demonstrated to be free from interferences under the conditions of analysis by analyzing method blanks.6.3Interferences from phthalate esters may pose a major problem in Aroclor determinations when using ECD.Phtha-lates generally appear in the chromatogram as broad late eluting peaks.Since phthalates are commonly used as plasti-cizers and are easily extracted from plastic,all contact of samples and extracts with plastic should be avoided.6.4While general clean-up techniques are provided as part of this test method,some samples may require additional clean-up beyond the scope of this test method before proper instrumental analysis may be performed.7.Apparatus7.1Gas Chromatograph,a temperature programmable gas chromatograph suitable for splitless injections;equipped with anECD.7.2Data System,a data system capable of measuring peak areas.7.3Regulator(Make-up Gas)—N2or Ar:Methane(95:5); two stage regulator rated at20MPa(3000psi)inlet and35to 860kPa(5to125psi)outlet.7.4Regulator(Carrier Gas)—H2,two-stage regulator rated at20MPa(3000psi)inlet and35to860kPa(5to125psi) outlet.7.5Gas Puriﬁers,to remove moisture and particulates. Depending on the levels and types of interferences encoun-tered,these might involve molecular sieves(moisture),acti-vated carbon(organics),or other commercially-available me-dia.7.6Flow Meter,to measure gasﬂow.Typical range is from 0.5to50mL/min.60.1mL/min.7.7Column,crosslinked5%phenyl methyl silicone,30m by0.32mm id by0.25umﬁlm thickness.7.7.1It is possible that other columns will provide sufficient separating power,but this shall be demonstrated before use.7.8Analytical Balance,capable of weighing to0.0001g.7.9Volumetric Flasks,10,50,100,200mL,(see Speciﬁca-tion E288)Class A with ground-glass stoppers.7.10Vortex Mixer:7.11Vials,glass,20mL and40mL capacity with TFE-ﬂuorocarbon-lined caps.7.12Septum Inserts—Inserts shall be treated with a si-lynization reagent before use or after cleaning.(See Annex A2 for possible procedure.)They may be purchased already treated.7.13Volumetric Pipette,1,5,10mL(see Speciﬁcation E 969),Class A.7.14Syringe,500uL,mechanical guide.8.Reagents and Materials8.1Purity of Reagents—Reagent grade chemicals shall be used in all tests.Unless otherwise indicated,it is intended that all reagents conform to the speciﬁcations of the Committee on Analytical Reagents of the American Chemical Society where such speciﬁcations are available.10Other grades may be used, provided it isﬁrst ascertained that the reagent is of sufficiently high purity to permit its use without lessening the accuracy of the determination.8.2Acetone—See Note3.N OTE3—Warning:Extremelyﬂammable.Vapors may causeﬂashﬁre.8.3Activated Magnesium Silicate(Florisil),Pesticide resi-due(PR)grade(60/100mesh);store in glass containers with ground glass stoppers or foil lined screw caps.8.3.1Just before use,activate each batch at least4h at 130°C in a glass container loosely covered with aluminum foil. Alternatively,store the magnesium silicate in an oven at 130°C.Cool the magnesium silicate in a desiccator for30min before use.8.4Hexane—See Note4.N OTE4—Warning:Extremelyﬂammable.Harmful if inhaled.May produce nerve cell damage.Vapors may causeﬂashﬁre.8.5Isooctane—See Note5.N OTE5—Warning:Extremelyﬂammable.Harmful if inhaled.Vapors may causeﬂashﬁre.8.6Methanol—See Note6.N OTE6—Warning:Flammable.Vapor harmful.May be fatal or cause blindness if swallowed or inhaled.Cannot be made nonpoisonous.8.7Silynization Reagent(for example,5%dimethyldichlo-rosilane in toluene).See Annex A2for instructions.8.8Sodium Sulfate,granular,anhydrous(maintained at 130°C for at least24h prior to use).Cool the sodium sulfate ina desiccator for30min before use.8.9Sulfuric Acid(concentrated):8.10Acetone/Hexane,10%acetone/90%hexane(v/v). 8.11Gases,Hydrogen(zero grade;99.995%purity)and nitrogen(zero grade;99.998%purity)or argon/methane(95:5; ECD grade).8.11.1Care shall be given to ensure purity of the carrier gas. For example,an in-lineﬁlter may be required.8.12Aroclor Standards3,Aroclor1016,1221,1232,1242, 1254,1260,1262,1268.8.13Decachlorobiphenyl(DCB)(surrogate)Optional: 8.13.1Surrogate Stock Standard(15ug/mL)Preparation—Accurately dilute1.5mL of1000ug/mL DCB concentrate in 100mL volumetricﬂask andﬁll to the mark with methanol, yielding a15ug/mL solution.8.13.2Surrogate Working Standard(1.5ug/mL) Preparation—Accurately dilute10mL of the15ug/mL DCB stock standard in a100mL volumetricﬂask andﬁll to the mark with methanol,yielding a1.5ug/mL working DCB standard. N OTE7—Sample preparations will normally use0.1mL of this solu-tion.The resulting concentration in the sample extract is0.005ug/mL before any further dilutions.The following calculations show this.1.5ug/mL30.l mL50.15ug0.15ug~3.0mL sample127mL!50.005ug/mL(2) 8.14Calibration Standards:8.14.1Intermediate Stock Standard(50ug/mL):If high level standards(for example,commercially available standards at2000to5000ug/mL)have been purchased, prepare solutions of50ug/mL concentration.8.14.1.1The surrogate calibration standard may be added (optional)to the Aroclor1016/1260intermediate stock stan-dard at a concentration of2.5ug/mL.For preparation of the standard,add500uL of50ug/mL surrogate to a10mL volumetricﬂask containing 3.0mL of iso octane.Add the Aroclor1016/1260standard(5.0mL at100ug/mL)to the ﬂask.Dilute to10mL volume with iso octane and mix well.8.14.1.2To prepare the continuing CCS,dilute200uL of the intermediate stock standard to100mL.Volume add into Ar-1016/1260concentration Surrogate concentration the100mLﬂask ug/mL ug/mL 200uL0.100.00510Reagent Chemicals,American Chemical Society Speciﬁcations,American Chemical Society,Washington,DC.for suggestions on the testing of reagents not listed by the Amerian Chemical Society,See Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,U.K.,and the United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.8.14.2Instrument Performance Standard(IPS)(Tier I–Screening)—An iso octane solution of Aroclors1016and 1260is prepared at a concentration of0.01ug/mL(each)or0.1 ug/mL(each)(depending on whether the minimum level of interest is2ug/mL or20ug/mL)from the appropriate stock standard.8.14.2.1If the surrogate(decachlorobiphenyl,(DCB))is used,it shall be added to the IPS to result in a concentration of 0.005ug/mL.8.14.2.2To prepare the IPS along with DCB,add10mL of Aroclor1016/1260at0.1ug/mL and0.033mL of DCB at15 ug/mL into100mL volumetricﬂask.Dilute to100mL volume with iso octane.Mix well.This yields0.01ug/mL IPS and 0.005ug/mL of DCB.8.14.2.3The following additional standards shall be run once(at0.1ug/mL)to demonstrate the Aroclor patterns and be mixed if preferred.Aroclor Mix with the following:12681221or1232or1242or1248or125412621221or1232or1242or1248125412218.14.3Individual Working Standards(Tier 2–Quantitation)—Working standards are typically prepared in iso octane at concentrations of0.02ug/mL,0.05ug/mL,0.1 u/mL,0.3ug/mL and0.5ug/mL for Aroclors1016and1260. All other Aroclors are prepared at the mid level concentration (0.1ug/mL)for the single point calibration.An alternative calibration range may be used as long as the criteria for linearity of the calibration range is documented.8.14.3.1Aroclors1016and1260shall be a mixed standard. The following additional standards shall be run once(at0.1 ug/mL)to demonstrate the Aroclor patterns and may be mixed, if preferred.Aroclor May be mixed with:12681221or1232or1242or1248or125412621221or1232or1242or1248125412218.15Quality Control Standards:8.15.1Calibration Check Standard(CCS)(Tier 2–Quantitation)—This standard contains0.1ug/mL(those who are interested in the20mg/Kg level with no compositing, use0.2ug/mL each)each of Aroclors1016and1260in hexane.8.15.1.1The surrogate concentration,if used,is0.005 ug/mL.8.15.1.2Example—To prepare the CCS along with DCB, add20mL of Aroclors1016/1260to0.5ug/mL and0.05mL of DCB at10ug/mL into100mL volumetricﬂask.Dilute to 100mL volume with iso octane.Mix well.This yields a0.1 ug/mL of CSS and0.005ug/mL of DCB.8.15.2Matrix Spiking Standard(Tier2–Quantitation)—The matrix spiking standard is to contain Aroclor1268at a concentration of50ug/mL in boratories working at lower calibration ranges will need to dilute this(for example, to25ug/mL).8.16Copper Powder,200mesh,99%min..8.17Silica Gel,100to200mesh.9.Sampling9.1PCBs are hydrophobic compounds.Therefore,when sampling,all organic phases,including bottom sludge beneath aqueous phases,shall be sampled.Given the possible presence of alcohols and glycols,it is typically not acceptable to sample the organic phase only.9.2Headspace above stored standards and samples or ex-tracts should be minimized such that the volume is less than50 %.9.3Three mL of sample are required for each determination. No special sample preservation is required other than storage in a closed container with minimal headspace.It is accepted practice to use borosilicate glass containers with TFE-ﬂuorocarbon-lined lids.10.Preparation of Apparatus10.1General Gas Chromatographic Conditions—Theﬁrst temperature proﬁle(12min run time)is used for Tier I screening method for the presence of Aroclor.The longer second temperature proﬁle(17min run time)is used for Tier II to quantitate the Aroclors present,but may also be used for Tier I,if desired.10.1.1Rapid Screen Capilary Column Oven Temperature Proﬁle(Tier I,12min run time):Initial value130°CInitial time2minProgram rate20°C/minFinal value270°CFinal time3minCarrier gas hydrogenHead pressure depend on DCB RT(approximately105KPa(15psi))columnﬂow:3.1-3.2mL/minMake-up gas nitrogen or argon:methaneMake-up gas rate approximately65mL/min.Splitless modePurge off0minPurge on 1.0minPurge vent 2.5mL/minSplit vent50mL/minSample injection 2.0uLInjector inlet system250°CDetector315°C10.1.2Quantitation Capillary Column Oven Temperature Proﬁle(Tier II,17min run time;may also be used for Tier I analysis:Initial value125°CInitial time3minLevel IProgram rate12°C/minFinal value270°CFinal time2minCarrier gas hydrogenHead pressure Depend on DCB RT(approximately,105KPa(15psi))Columnﬂow 3.1mL/min(approximately at270°C)Make-up gas nitrogenMake-up gas rate approximately65mL/minSplitless modePurge off0minPurge on 1.0minPurge rate50mL/minSample injection 2.0uLInjector inlet system250°CDetector315°C11.Calibration and Standardization11.1Calibration:11.1.1Tier1–Screening Method—Aroclors are multi-peak chemical mixtures that have very unique identiﬁcation pat-terns.All Aroclors shall be run individually or in mixtures at 0.1ug/mL on each channel performing screening to produce reference patterns.It is important to note that some of these patterns have the same constituents and that some Aroclors are quantitated using the same peaks(such as Aroclors1016and 1232or1242).When screening for Aroclors,a visual determi-nation is made by the following key items:11.1.1.1Aroclor pattern—(a)same singlets,doublets,and triplets present in the reference chromatograms,and(b)same relative peak heights between peaks in the sample chromato-gram and the reference chromatogram.11.1.1.2Retention time shifts should be very consistent between the standard and the sample peaks.11.1.1.3All samples in which an Aroclor is detected(using Tier I)require a judgment concerning the amount.The recog-nized Aroclor pattern shall be compared to the IPS(0.01ug/mL or0.1ug/mL).If the overall level of the suspected Aroclor pattern is equal to or greater than overall level of the IPS pattern,then Tier II analysis may be used to quantitate the sample.If multiple Aroclors are suspected,a Tier II analysis may be run to help resolve the mixture.11.1.1.4Recovery control limits for the surrogate are40to 150%recovered.If the recovery is outside of these limits,see Annex A1.11.1.2Tier I Calibration Check—An instrument perfor-mance standard(IPS)at0.01ug/mL of Aroclor1016and1260 is used to check the instrument sensitivity once a day or every 20samples,whichever is more frequent(typically laboratories using ten samples compositing shall use the0.01ug/mL standard to achieve a detection limit of5ug/mL of Aroclor in any individual sample).Sample results will be compared qualitatively with the daily IPS.(See the Calculation section 13).11.1.2.1Tabulate the sum of the areas or the data system calculated amount of theﬁve major peaks for each of the Aroclors1016ad1260in the instrument performance standard. The response shall be within50%of the initial response. Initial response shall be established by averaging the response of a minimum ofﬁve injections of the instrument performance standard(IPS).If the limit is exceeded,new limits may need to be established.11.1.2.2Likewise,the expected response for the surrogate, if used,is established by averaging the areas of DCB in theﬁve initial IPS analyses.11.1.2.3The surrogate also may be used for retention time control.It is recommended that columnﬂow be adjusted so DCB elutes between10.5to11.5min using the12min GC program.(This will typically require a column head pressure of 105to112kPa.)(Alternatively,the retention time should be15 to16.5min using the17min program.)11.1.3Tier2–Quantitative Method—The GC data system must be calibrated for both Aroclors1016and1260,usingﬁve peaks for each Aroclor.[For example,when using an integra-tor,divide the standard amount by the number of peaks being ingﬁve peaks on a0.5ug/mL standard would assign 0.1ug/mL to each peak.This will allow for a calibration table to be made,yielding response factors for each peak at theﬁve levels of calibration.Set up a calibration table in the method ﬁle of the integrator or data system that is to be used.Calculate an average response factor for each ofﬁve peaks for both Aroclors.Calculate the standard deviation of the average response factor for each peak of the Aroclor using the following calculation.S5Œ(i51n~X i2X!2n21(3)where:S=standard deviation,X i=each observed value,X=the arithmetic mean of observed values,andn=total number of calibration points.11.1.3.1Calculate the percent relative standard deviations (%RSDs)for the response factors of the calibrated peaks for each Aroclor from the formula below.The acceptance criteria for the%RSD for each Aroclor is#20%.If the average% RSD is greater than20%for either Aroclor,then linearity over the desired calibration range for that instrument has not been demonstrated.N OTE8—The%RSD is100%multiplied by the result of Eq3(s) divided by the arithmetic mean(X).11.1.3.2When samples are to be analyzed,instrument control is veriﬁed by analyzing the CCS and the percent difference(%D)is calculated.The acceptance criteria is within+30%for each AROCLOR in the CCS(1016and 1260).11.1.3.3If either Aroclor1016or1260is out of control for the daily CCS,corrective action shall be taken and a CCS reanalyzed.If corrective action does not correct the problem, then a newﬁve point calibration curve shall be created. Percent difference(%D)%D5Amt I2Amt CAmt I3100%(4)where:Amt I=amount in standard,andAmt C=calculated amount from current CCS.11.1.3.4Calibration for Aroclors other than Aroclor1016 and Aroclor1260will be performed by analyzing standards at the concentration representing the midpoint of the calibration range selected.For example,if calibration is desired over the range of0.02ug/mL to0.5ug/mL,then the0.1ug/mL standards shall be used for calibration.Therefore,aﬁve point calibration shall be performed for Aroclors1016and1260and a one-point calibration shall be performed for all remaining Aroclors.11.1.3.5After the linearity of the system has been demon-strated,and each of the remaining Aroclors has been analyzed using middle level concentration,recalibration will be required only when the calibration check standard criteria is met.Oldcalibration curves may not be used again,other than to review data generated using those calibration curves.11.2Standardization:11.2.1Surrogate Recovery—Recovery control limits for the surrogate are40to150%recovered.11.2.1.1If the recovery is outside of these limits,see Annex A1.11.2.2Method Blank—For every20samples or batch, whichever is more frequent,a method blank shall be prepared by processing the extraction solvent(with surrogate,if used) through the same clean-up as that used for the samples.This is to detect possible contamination picked up during the sample clean-up process.N OTE9—A batch is the group of samples prepared at the same time.A batch may not exceed20samples.11.2.3Calibration Check Standard(CCS)(Tier II only)—A 0.1ug/mL standard(or0.2ug/mL)obtained from a source separate from the intermediate standard and containing Aro-clors1016and1260is the CCS which is used to verify the validity of theﬁve-point calibration curve.The calculated results for the CCS shall agree with the current calibration curve to within630%percent difference(%D).If the CCS results indicate that the calibration is outside control limits,and routine maintenance does not correct the problem,then the GC/ECD must be recalibrated.11.2.4Matrix Spike(MS)Samples(Tier II only)—For every batch or twenty samples,whichever is more frequent,a sample requiring Tier II analysis shall be selected in an unbiased manner and spiked with Aroclor1268.These results shall be documented,with an example shown in Appendix X2.11.2.4.11.0mL of50ug/mL of Aroclor1268(25ug/mL,if working at lower calibration range)is added to the sample chosen for spiking.Matrix spiked sample recovery limits are from60to140%,providing any Aroclor present in the sample before spiking does not exceedﬁve times the spike level.%Recovery5Recovered amountSpiked amount3100%(5)11.2.5Matrix Spike Duplicate(MSD)Sample(Tier II only)—Every batch or20samples,whichever is more frequent, precision data is generated using a matrix spike duplicate. Acceptance criteria is20%relative percent difference(RPD) for the duplicate analyses.11.2.5.1RPD is calculated from the absolute difference between duplicate percent recovery results D1and D2divided by the mean value of the duplicates.RPD5?D12D2?~D11D2!/23100%(6)12.Procedure12.1Compositing—It is common to analyze mixtures of multiple samples,called composites,if a large number of samples are analyzed.This approach is described in Annex A3.12.2Sample Preparation Procedure:12.2.1Liquid Samples—Accurately pipette 3.0mL of sample into a tared40mL vial(ﬁtted with a TFE-ﬂuorocarbon-lined cap)and weight.If the results are calculated by weight accurately weigh the sample and record the weight.Spike this sample with100uL of decachlorobiphenyl surrogate working standard.12.2.1.1Add27mL acetone/hexane to the vial,producing a 1:10dilution.Cap it and vortex vigorously for at least30s.If the sample is not completely miscible with acetone/hexane, add more acetone to reach a total of approximately30mL extract and vortex again.(Alternatively,place capped vial in sonic bath for5min.)12.2.2Solid,Semi-solids,Sludge Samples—Weigh accu-rately 3.0g of sample into a40mL vialﬁtted with a TFE-ﬂuorocarbon-lined cap.Spike this sample with100uL of decachlorobiphenyl surrogate working standard.Add30mL of acetone/hexane to the vial for a1:10dilution.V ortex for at least 30s.12.2.2.1If the sample does not totally dissolve,vortex again or place capped vial in sonic bath for5min.This shall provide adequate contact whether or not any further dissolution occurs.12.2.3Matrix Spike and Matrix Spike Duplicate Samples—Add1.0mL of spiking solution to the sample just after the addition of the surrogate and prior to the addition of the acetone-hexane solvent.12.2.4Centrifuge—If sediment is visible,centrifuge the extract to separate out the sediment.12.3Sample Clean-up—Clean-up is not required for all samples;however,interference problems due to the presence of other chemical species may usually be addressed using the procedures found in Annex A4.12.4Gas Chromatographic Analysis Sequence—Samples are analyzed in a set referred to as an analysis sequence. 12.4.1Tier1–Screening:12.4.1.1Standards Sequence(initially and optionally with recalibrations)—(a)Aroclor1016/1260,at selected IPS level (5times)and(b)The following may be mixed as described below and shall be analyzed at0.1ug/mL each(for20mg/Kg level of interest use0.2ug/mL).Aroclor1221Aroclor1232Aroclor1242Aroclor1248Aroclor1254Aroclor1262Aroclor126812.4.1.2Some of the standards in12.4.1.1may be run as mixed standards:Aroclor May be Mixed With12681221or1232or1242or1248or125412621221or1232or1242or12481254122112.4.1.3A Typical Analysis Sequence—A typical analysis sequence includes(a)reagent blank(optional),(b)Instrument Performance Standard(IPS)(every20samples or every day, whichever is more frequent),(c)method blank,and(d) Samples1to20.12.4.1.4Repeat this sequence as long as the system meets the IPS criteria.12.4.2Tier2–Quantitation:12.4.2.1Standards Sequence—The standards sequence in-cludes(a)reagent blank,(b)Aroclor1016/1260(5point。