T568-09 Solution 9.2 - RevA

电子电气产品聚合物材料中六溴环 十二烷的测定 裂解-气相色谱- 质谱定性筛选法1 范围本文件规定了电子电气产品聚合物材料中六溴环十二烷的裂解-气相色谱-质谱定性筛选法。

本文件适用于电子电气产品聚合物材料中六溴环十二烷的定性筛选。

2 规范性引用文件下列文件中的内容通过文中的规范性引用而构成文件必不可少的条款。

其中，注日期的引用文件，仅该日期对应的版本适用于本文件；不注日期的引用文件，其最新版本（包括所有的修改单）适用于本文件。

GB/Z 20288电子电气产品中有害物质检测样品拆分通用要求3 术语和定义本文件没有需要界定的术语和定义。

4 方法提要聚合物样品经粉碎后，直接引入热裂解仪器中，以特定的加热程序将六溴环十二烷从聚合物材料中解析出来，进入气相色谱-质谱仪进行定性检测。

5 试剂和材料5.1丙酮：色谱纯。

5.2六溴环十二烷标准品（CAS号：3194-55-6）：纯度≥95%。

5.3标准储备液（1 000 mg/L）：准确称取0.010 0 g六溴环十二烷标准品（5.2），用丙酮（5.1）溶解并转移到10 mL的容量瓶中定容，配制成1 000 mg/L的标准储备液，置于棕色瓶中于4 ℃冰箱内保存。

5.4标准工作溶液（100 mg/L）：准确吸取1.0 mL标准储备液（5.3）置于容量瓶中，用丙酮（5.1）定容至10 mL，配制成100 mg/L的标准工作溶液，置于棕色瓶中于 4 ℃冰箱内保存。

6 仪器和设备6.1气相色谱-质谱联用仪（GC-MS）：配有热裂解器。

6.2分析天平：感量分别为0.1 mg和0.01 mg。

6.3样品制备工具：剪刀、钳子、冷冻研磨机等类似工具。

6.4微量进样针：10 mL。

6.5取样工具：微量勺或镊子。

7 样品制备用于电子电气产品的聚合物材料或根据GB/Z 20288拆分方法所取得的分析样品，选用合适的样品制备工具（6.3），将样品制成粒径0.1 cm以下小片或粉末，混匀备用。

上海拿华电子科技有限公司ADWA埃达华系列酸度/氧化还原（含税公开报价）分类型号配件技术参数公开报价AD1030AD2002B/1 可填充玻璃pH电极，BNC接头和1米电缆，AD5006不锈钢温度探头和1米电缆，pH4.01，pH7.01和pH10.01校正缓冲溶液（20ml/袋），电极冲洗溶液，电极支架，12 Vdc电源适配器和用户手册。

3点校正；范围：－2.00～16.00pH，分辨率：0.01/0.001,精度：±0.01/±0.002；范围：±2000mV,分辨率：0.1～±999.9mV/1,精度：±0.2mV～±699.9mV/±0.5mV～±999.9mV/±2mV4858.00AD1040AD2002B/1 可填充玻璃pH电极，BNC接头和1米电缆，AD5006不锈钢温度探头和1米电缆，pH4.01，pH7.01和pH10.01校正缓冲溶液（20ml/袋），电极冲洗溶液，电极支架，12 Vdc电源适配器和用户手册。

3点校正；范围：－2.00～16.00pH，分辨率：0.01/0.001,精度：±0.01/±0.002；范围：±2000mV,分辨率：0.1～±999.9mV/1,精度：±0.2mV～±699.9mV/±0.5mV～999.9mV/±2mV；带GLP功能5690.00AD1000AD2002B/1 可填充玻璃pH电极，BNC接头和1米电缆，AD5006不锈钢温度探头和1米电缆，pH4.01，pH7.01和pH10.01校正缓冲溶液（20ml/袋），电极冲洗溶液，电极支架，12 Vdc电源适配器和用户手册。

6点校正；范围：－2.00～16.00pH，分辨率：0.01/0.001,精度：±0.01/±0.002；范围：±2000mV,分辨率：0.1～±999.9mV/1,精度：±0.2mV～±699.9mV/±0.5mV～±999.9mV/±2mV；带RS232/USB&GLP功能8465.00AD1200（离子浓度计）AD2002B/1 可填充玻璃pH电极，BNC接头和1米电缆，AD5006不锈钢温度探头和1米电缆，pH4.01，pH7.01和pH10.01校正缓冲溶液（20ml/袋），电极冲洗溶液，电极支架，12 Vdc电源适配器和用户手册。

Quick Guide:This Quick Guide provides DNA Shearing protocols when using microTUBE-130, microTUBE-50, microTUBE-15, microTUBE-500, or miniTUBE and a Covaris E220 Focused-ultrasonicator.Revision History010308 K 1/17 Format Changes; Addition of microTUBE-500 AFA Fiber Screw-Capprotocols; update ‘Additional Accessories’; update Appendix B 010308 L 2/17 Changes to 8 microTUBE-50 Strip V2 protocols; addition of 8 microTUBE-15AFA Beads H Slit Strip V2 and 8 microTUBE-50 AFA Fiber H Slit Strip V2010308 M 5/17 Addition of 96 microTUBE-50 AFA Fiber Plate Thin Foil (PN 520232) and 130ul 96 microTUBE AFA Fiber Plate Thin Foil (PN 520230)010308 N 7/17 Add the names of the well plates definition for 520230 & 520232. Changedyear for Rev M Date.Values mentioned in this Quick Guide are nominal values. The tolerances are as follows: -Temperature +/-2°C-Sample volumeo microTUBE-15: from 15 to 20 µl, +/- 1 µlo microTUBE-50: 55 µl, +/- 2.5 µlo microTUBE Plate, Strip, Snap and Crimp Cap: 130 µl, +/- 5 µlo microTUBE-500: 500 µl, +/- 10 µl or 320 µl, +/- 10 µlo miniTUBE: 200 µl, +/- 10 µl-Water Level +/- 1Sample guidelines-DNA input: up to 5 µg purified DNA (1 µg for the microTUBE-15; minimum 320 ng for the microTUBE-500) -Buffer: Tris-EDTA, pH 8.0-DNA quality: Genomic DNA (> 10 kb). For lower quality DNA, Covaris recommends setting up a time dose response experiment for determining appropriate treatment times.-DO NOT use the microTUBE or miniTUBE for storage. Samples should be transferred after processing. Instrument setup-Refer to the instrument manual for complete setup.-microTUBE and miniTUBE have specific holders or racks associated with them.-E220 and E220 evolution may require the Intensifier (PN 500141). Refer to Appendix C for instructions.-E220 and E220 evolution may require Y-dithering. Refer to Appendix A for instructions.Instrument settings-Recommended settings are subject to change without notice.-Mean DNA fragment size distributions are based on electropherograms generated from the Agilent Bioanalyzer with the DNA 12000 Kit (cat# 5067-1509), with the exception of the 320 µl microTUBE-500 protocol (HighSensitivity DNA Kit, cat# 5067-4626). DNA fragment representation will vary with analytical systems, please carry out a time course experiment based on settings provided in this document to reach desired fragment sizedistribution.See /wp-content/uploads/pn_010308.pdf for updates to this document.130 µl sample volume - from 150 to 1,500 bpVessel microTUBEAFA FiberSnap-Cap(PN 520045)microTUBEAFA FiberCrimp-Cap(PN 520052)8 microTUBEStrip(PN 520053)96 microTUBEPlate(PN 520078)96 microTUBEAFA Fiber PlateThin Foil(PN 520230)Sample Volume 130 µlE220RacksRack 24 PlacemicroTUBESnap-Cap (PN500111)Rack 96 PlacemicroTUBECrimp-Cap(PN 500282)Rack 12 Place 8microTUBE Strip(PN 500191)No Rack needed Plate Definitions“500111 24microTUBEsnap +4mmoffset”“E220_500282Rack 96 PlacemicroTUBE-6mm offset”“E220_500191 8microTUBE stripPlate -6mmoffset”“E220_52007896 microTUBEPlate -6mmoffset”“E220_52023096 microTUBEPlate Thin Foil -6mm offset”Water Level 6Intensifier (PN 500141) YesY-dithering NoE220 evolutionRacks Rack E220e 8 Place microTUBECrimp and Snap Cap (PN 500433)Rack E220e 8microTUBE Strip(PN 500430)Non Compatible Plate Definitions“500433 E220e 8 microTUBECrimp and Snap Cap -3.7mmoffset”“500430 E220e 8microTUBE Strip-6mm offset”N/A Water Level 6Intensifier (PN 500141) YesY-dithering NoAllTemperature (°C) 7Target BP (Peak) 150 200 300 400 500 800 1,000 1,500 Peak Incident Power (W) 175 175 140 140 105 105 105 140 Duty Factor 10% 10% 10% 10% 5% 5% 5% 2% Cycles per Burst 200 200 200 200 200 200 200 200 Treatment Time (s) 430 180 80 55 80 50 40 15Vessel microTUBE-50Screw-Cap (PN 520166)8 microTUBE-50 AFA FiberStrip V2 (PN 520174)8 microTUBE-50 AFA Fiber HSlit Strip V2 (PN 520240)96 microTUBE-50AFA Fiber Plate(PN 520168)96 microTUBE-50AFA Fiber Plate ThinFoil (PN 520232) Sample Volume 55 µlE220RacksRack 24 PlacemicroTUBE Screw-Cap (PN 500308)Rack 12 Place 8 microTUBEStrip (PN 500444) No Rack needed Plate Definitions“E220_500308 Rack24 Place microTUBE-50 Screw-Cap+6.5mm offset”“E220_500444 Rack 12 Place 8microTUBE-50 Strip V2-10mm offset”“E220_520168 96microTUBE-50 Plate-10.5mm offset”“E220_520232 96microTUBE-50 PlateThin Foil -10.5mmoffset”E220evolutionRacksRack E220e 4 PlacemicroTUBE ScrewCap (PN 500432)Rack E220e 8 microTUBE StripV2 (PN 500437) Non Compatible Plate Definitions“500432 E220e 4microTUBE-50 ScrewCap -8.32mm offset”“500437 E220e 8 microTUBE-50 Strip V2 -10mm offset” N/AAllTemperature (°C) 7Water Level 6 -2 0 Intensifier (PN 500141) Yes Yes YesY-dithering No No Yes (0.5mm Y-dither at10mm/s) Target BP (Peak) 150 200 250 300 350 400 550Screw-CapPeak Incident Power(W) 100 75 75 75 75 75 30Duty Factor 30% 20% 20% 20% 20% 10% 10%Cycles per Burst 1000 1000 1000 1000 1000 1000 1000Treatment Time (s) 130 95 62 40 30 50 708-StripPeak Incident Power (W) 75 75 75 75 75 75 50Duty Factor 15% 15% 20% 20% 20% 10% 10%Cycles per Burst 500 500 1000 1000 1000 1000 1000Treatment Time (s) 360 155 75 45 35 52 50 PlatePeak Incident Power (W) 100 100 75 75 75 75 75Duty Factor 30% 30% 20% 20% 20% 10% 10%Cycles per Burst 1000 1000 1000 1000 1000 1000 1000Treatment Time (s) 145 90 70 49 34 50 32 The Y-dithering function is required for shearing with 96 microTUBE-50 plate (PN 520168). This function is only available on SonoLab versions 7.3 and up. Please see Appendix A for detailed instructions.Vessel microTUBE-15 AFA BeadsScrew-Cap (PN 520145)8 microTUBE-15 AFA BeadsStrip V2 (PN 520159)8 microTUBE-15 AFA BeadsH Slit Strip V2 (PN 520241)Sample Volume 15 µlE220Racks Rack 24 Place microTUBEScrew-Cap (PN 500308)Rack 12 Place 8 microTUBEStrip V2 (PN 500444) Plate Definitions“E220_500308 Rack 24 PlacemicroTUBE-15 Screw-Cap+15mm offset”“E220_500444 Rack 12 Place 8microTUBE-15 Strip V2 -1.5mmoffset”Water Level 10 6Intensifier (PN 500141) NoY-dithering NoE220evolutionRacks Rack E220e 4 Place microTUBEScrew Cap (PN 500432)Rack E220e 8 microTUBE StripV2 (PN 500437)Plate Definitions ”500432 E220e 4 microTUBE-15Screw Cap 0.18mm offset”“500437 E220e 8 microTUBE-15Strip V2 -1.58mm offset”Water Level 10 6Intensifier (PN 500141) NoY-dithering NoAllTemperature (°C) 20Target BP (Peak) 150 200 250 350 550Peak Incident Power (W) 18 18 18 18 18Duty Factor 20% 20% 20% 20% 20%Cycles per Burst 50 50 50 50 50Treatment Time (s) 300 120 80 45 22To ensure reproducible DNA shearing, it is required to centrifuge samples before processing DNA in amicroTUBE-15. Please see Appendix B for instructions.Please note that microTUBE-15 requires removal of the Intensifier (PN 500141) from the E220 focused-ultrasonicator. Please see Appendix C for instructions.200 µl sample - 2,000; 3,000 and 5,000 bpVesselminiTUBE Clear(PN 520064)Blue(PN 520065)Red(PN 520066) Sample Volume 200 µlE220Racks Rack 24 Place miniTUBE (PN 500205)Plate Definition “500205 24 miniTUBE +15mm offset”Water Level 11Intensifier (PN 500141) NoY-dithering NoE220evolutionRacks Rack E220e 4 Place miniTUBE (PN 500434)Plate definition “500434 E220e 4 miniTUBE 4.9mm offset”Water Level 11Intensifier (PN 500141) NoY-dithering NoAllTemperature (°C) 7 20 20 Target BP (Peak) 2,000 3,000 5,000miniTUBE Clear Blue RedPeak Incident Power (W) 3 3 25Duty Factor 20% 20% 20%Cycles per Burst 1000 1000 1000Treatment Time (s) 900 600 600Please note that miniTUBE requires removal of the Intensifier (PN 500141) from the E220 focused-ultrasonicator. Please see Appendix C for instructions.320 µl and 500 µl sample volume – from 150 to 600 bpVesselmicroTUBE-500 AFA Fiber Screw-Cap(PN 520185)Sample Volume320 µl 500 µlE220Rack Rack, 24 microTUBE-500 Screw-Cap (PN 500452)Plate Definition “E220_500452 Rack 24 Place microTUBE-500 Screw-Cap +6mmoffset” Water Level6 Intensifier (PN 500141)Yes Y-dithering NoE220 evolutionRackRack E220e 4 microTUBE-500 Screw-Cap (PN 500484) Plate Definition “500484 E220e 4 microTUBE-500 Screw-Cap -9.9mm offset”Water Level6 Intensifier (PN 500141)Yes Y-ditheringNo AllTemperature (°C)7Target BP (Peak)500 - 600150200350550Peak Incident Power (W) 75 175 175 175 175 Duty Factor 25% 20% 20% 20% 5% Cycles per Burst 200 200 200 200 200 Treatment Time (s)7540018055110To fragment DNA to sizes larger than 5 kb, Covaris offers the g-TUBE: a single-use device that shears genomic DNA into selected fragments sizes ranging from 6 kb to 20 kb. The only equipment needed is a compatible bench-top centrifuge.Additional AccessoriesPart Number Preparation stationsmicroTUBE Prep Station Snap & Screw Cap 500330 microTUBE-500 Screw-Cap Prep Station 500510 miniTUBE loading and unloading station 500207 8 microTUBE Strip Prep Station500327 Centrifuge and Heat Block microTUBE Screw-Cap Adapter Fits microTUBE Screw-Caps into bench top microcentrifuges500406 Centrifuge 8 microTUBE Strip V2 Adapter Fits the 8 microTUBE Strip into a Thermo Scientific TM mySPIN TM 12 mini centrifuge 500541 g-TUBEg-TUBEs (10) and prep station520079Appendix A – Using Y-dithering with SonoLab 7.3 and upA Y-dithering step is required for DNA shearing with the 96 microTUBE-50 Plate-This feature is only available on SonoLab versions 7.3 and up.-To obtain a copy of the SonoLab 7.3 and the Plate Definition installers, please employ the Registered Users Login on the Covaris website, -For any assistance in this process, please contact your local representative, or Covaris Global Technical Services at ***********************.Use the following steps to include Y-dithering in sample treatment1.Go into the Method Editor2.Select ‘Add Step’ and enter the treatment settings for the desired fragment sizea.Note: The following steps must be done for each individual treatment3.Select the Motion tab4.Enter the following values into the ‘X-Y Dithering Box’a.Y Dither (mm): 0.5b.X-Y Dither Speed (mm/sec): 10.0c.Both X Dither (mm) and X-Y Dwell (sec) should be set to 0Appendix B – microTUBE-15 centrifugation before DNA Shearing1.Sample loading and centrifugationmicroTUBE-15 AFA Beads Screw-CapLoad and centrifuge microTUBE-15 Screw-Cap as described before placing the tubes in the rack.If some of the sample splashes onto the wall of the microTUBE while removing from centrifuge or placing into rack, repeat centrifuge step. All liquid should be at the bottom of the microTUBE-15 before starting the AFA treatment.8 microTUBE-15 AFA Beads Strip V2The 8 microTUBE-15 AFA Beads Strip V2 will fit into the Covaris Centrifuge 8 microTUBE Strip V2 Adapter (PN 500541) for the Thermo Scientific TM mySPIN TM 12 mini centrifuge. Place the strip in the adapter and spin for a minimum of 1 minute.2.Sample processingUse settings provided in page 4.3.Sample recoveryRepeat the centrifuge step before recovering sample from microTUBE-15.Appendix C – Removing or Installing the Intensifier (Covaris PN 500141) from an E System The 500141 Intensifier is a small inverted stainless steel cone centered over the E Series transducer by four stainless wires. The wires are held by in a black plastic ring pressed into the transducer well.If an AFA protocol requires “no intensifier”, please remove the Intensifier, using the following steps:1.Empty the water bath. Start the E System and start the SonoLab software.2.Wait for the homing sequence to complete (the transducer will be lowered with the rack holder at it home position,allowing easy access to the Intensifier).3.Grasp opposite sides of plastic ring and gently pull the entire assembly out of the transducer well. Do not pull on the steelcone or the wires. The ring is a friction fit in the well – no hardware is used to hold it in place.The 500141 Intensifier (left) shown installed in the E System transducer well and (right) removed.Note the “UP” marking at the center of the Intensifier.If a protocol requires the Intensifier to be present, simply reverse this process:1.Align the black plastic ring with the perimeter of the transducer well. Note that the flat side of the center cone (marked UP)should be facing up (away from the transducer).2.Gently press each section of the ring into the well until the ring is seated uniformly in contact with the transducer, withapproximately 2 mm of the ring evenly exposed above the transducer assembly. Do not press on the cone or wires. The rotation of the ring relative to the transducer assembly is not important.3.Refill the tank. Degas and chill the water before proceeding.Technical Assistance•By telephone (+1 781 932 3959) during the hours of 9:00am to 5:00pm, Monday through Friday, United States Eastern Standard Time (EST) or Greenwich Mean Time (GMT) minus 05:00 hours•By e-mail at ***********************。

华蟾毒素(CBG)酶联免疫吸附检测试剂盒货号：ELK8271规格：96T（本试剂盒仅供体外研究使用，不用于临床诊断）灵敏度：91.3ng/mL检测范围：312.5-20000ng/mL特异性：可检测重组或天然的CBG，且不与其它相关蛋白交叉反应。

试剂盒组成中文名称英文名称规格保存条件48T96T酶标板（可拆）Pre-coated Microplate 6条x8孔12条x8孔4°C/-20°C（6个月）冻干标准品Standard(lyophilized)124°C/-20°C（6个月）标准品&样品稀释液Standard/Sample Diluent Buffer10mL20mL4°C生物素结合物（100×）Biotinylated-Conjugate(100x)30μL60μL4°C/-20°C（6个月）生物素结合物稀释液Biotinylated Conjugate Diluent5mL10mL4°C浓缩HRP酶结合物（100×）Streptavidin-HRP(100×)60μL120μL4°C/-20°C（6个月）酶结合物稀释液HRP Diluent6mL12mL4°C浓缩洗涤液（25×）Wash Buffer(25×)10mL20mL4°C显色底物溶液（TMB）TMB Substrate Solution6mL10mL4°C（避光）反应终止液Stop reagent3mL6mL4°C封板覆膜Plate Covers12常温产品说明书Instruction manual1份1份常温特别说明1.打开包装后请及时检查所有物品是否齐全完整。

所有试剂的批号见标签。

2.试剂盒保存：-20°C（长时间存放，试剂按照标签提示温度保存）；2-8°C（一周内使用）；避免反复冻融，过期后请勿使用。

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小鼠骨保护素ELISA试剂盒说明书，OPGELISA试剂盒小鼠骨保护素ELISA试剂盒说明书，OPGELISA试剂盒供应商：上海乔羽生物有限公司ELISA试剂盒规格：(1) 规格：96T 可以测90个样，5个标准孔，1个空白孔(2) 规格：48T 可以测42个样，5个标准孔，1个空白孔小鼠骨保护素ELISA试剂盒说明书，OPGELISA试剂盒Kit composition:Sealing film: 2 (48) /2 tablets (96)Specification: 1 copiesSealing bag: 1Standard: 2700ng/L 0.5ml * 0.5ml * 1 bottles 1 bottles of stored at 2-8ELISA plates coated: 1 X 48 x 96 1 2-8 stored atSample dilution: 3ml * 1 ml * 1 bottle 6 bottle stored at 2-8Chromogenic agent A: Liquid 3ml * 1 ml * 6 bottle 1 bottles of stored at 2-8 Chromogenic agent B: Liquid 3ml * 1 ml * 6 bottle 1 bottles of stored at 2-8 Stop solution: 3ml * 6ml * 1 bottles 1 bottles of stored at 2-8Concentrated washing liquid: (20ml x 20) x 1 bottles (20ml x 30) x 1 bottles stored at 2-8elisa试剂盒价格，elisa试剂盒说明书，elisa检测试剂盒小鼠骨保护素ELISA试剂盒说明书，OPGELISA试剂盒上海乔羽生物有限公司专业的提供elisa试剂盒，进口/国产elisa试剂盒，elisa试剂盒价格，elisa试剂盒说明书，专业elisa试剂盒说明书生产商,老品牌ELISA试剂盒,ELISA试剂盒报价,elisa试剂盒品牌,生化试剂，血清，标准品|对照品、培养基等科研生化试剂，品质保证，技术严格，无效果退款退货，欢迎来电咨询及订购。

安全技术说明书页: 1/12 巴斯夫安全技术说明书按照GB/T 16483编制日期 / 本次修订: 05.09.2021版本: 7.0日期/上次修订: 01.10.2019上次版本: 6.0日期 / 首次编制: 20.01.2009产品: 巴速耐®LR 9056 六亚甲基二异氰酸酯的聚合物Product: Basonat® LR 9056(30591253/SDS_GEN_CN/ZH)印刷日期 08.08.20231. 化学品及企业标识巴速耐®LR 9056 六亚甲基二异氰酸酯的聚合物Basonat® LR 9056推荐用途和限制用途: 原料, 仅用于工业用途公司:巴斯夫(中国)有限公司中国上海浦东江心沙路300号邮政编码 200137电话: +86 21 20391000传真号: +86 21 20394800E-mail地址: **********************紧急联络信息:巴斯夫紧急热线中心（中国）+86 21 5861-1199巴斯夫紧急热线中心（国际）:电话: +49 180 2273-112Company:BASF (China) Co., Ltd.300 Jiang Xin Sha RoadPu Dong Shanghai 200137, CHINA Telephone: +86 21 20391000Telefax number: +86 21 20394800E-mail address: ********************** Emergency information:Emergency Call Center (China):+86 21 5861-1199International emergency number: Telephone: +49 180 2273-1122. 危险性概述纯物质和混合物的分类:急性毒性: 分类4 (吸入-薄雾)巴斯夫安全技术说明书日期 / 本次修订: 05.09.2021版本: 7.0产品: 巴速耐®LR 9056 六亚甲基二异氰酸酯的聚合物Product: Basonat® LR 9056(30591253/SDS_GEN_CN/ZH)印刷日期 08.08.2023急性毒性: 分类5 (口服)皮肤致敏物: 分类1特异性靶器官毒性-一次接触: 分类3 (对呼吸道系统有刺激性)对水环境的急性危害: 分类3对水环境的慢性危害: 分类3标签要素和警示性说明:警示词:警告危险性说明:H332吸入有害。

SECTION 1 - CHEMICAL IDENTIFICATIONPRODUCT NAME: Dextran SulfateCATALOG #: DSD20020SUPPLIER’S NAME: DOT SCIENTIFIC INC.SUPPLIERS ADDRESS: 4165 Lippincott, Burton, MI 48519EMERGENCY CONTACT: 1-800-424-9300(Reference Customer Number: 18739) OTHER INFORMATION: 1-800-878-1785OTHER INFORMATION: 800-878-1785SECTION 2 - HAZARDS IDENTIFICATION2.1 Classification of the substance or mixtureGHS Classification in accordance with 29 CFR 1910 (OSHA HCS)H315Skin corrosion/irritation Category 2 H319Serious eye damage/eye irritation Category 2 2.2 GHS Label elements, including Hazard and Precautionary Statement(s)PictogramSignal word: WarningHazard statement(s)H315Causes skin irritationH319Eye irritationPrevention, Response, Storage and Disposal Precautionary Statement(s)P264Wash skin thoroughly after handlingP280Wear protective gloves/protective clothing/eye protection/face protection.P302 + P352IF ON SKIN: Wash with plenty of soap and water.P305 + P351 + P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.P321Specific treatment (see. on this label).P332 + P313If skin irritation occurs: Get medical advice/attention.P337+P313If eye irritation persists: Get medical advice/attention.P362 + P364Take off contaminated clothing and wash before reuse.SECTION 3- COMPOSITION/INFORMATION ON INGREDIENTSCAS Number: 9011-18-1SECTION 4 - FIRST-AID MEASURES4.1 Description of first aid measuresGeneral advice: Consult a doctor and show this safety data sheet.i.If inhaled: Remove to fresh air and monitor breathing. If breathing becomes difficult, give oxygen. If breathingstops, give artificial respiration. Consult a doctor.SAFETY DATA SHEETii.In case of skin contact: Immediately wash skin with copious amounts of soap and water for at least 15 minutes.Remove contaminated clothing and shoes and wash before reuse. Consult a doctor.iii.In case of eye contact: Flush with copious amounts of water for at least 15 minutes. Consult a doctor.iv.If swallowed: Rinse mouth with water. Do not induce vomiting unless directed to do so by medical personnel.Never give anything by mouth to an unconscious person. Consult a doctor.4.2 Most important symptoms and effects, both acute and delayed: To the best of our knowledge, the chemical, physical and toxicological properties have not been thoroughly investigated.4.3 Indication of immediate medical attention and special treatment needed: Show this safety data sheet to the doctor in attendance. Immediate medical attention is required.SECTION 5 - FIRE FIGHTING MEASURES5.1 Extinguishing mediaSuitable extinguishing media: Use water spray, alcohol-resistant foam, dry chemical or carbon dioxide5.2 Special hazards arising from the substance or mixture: Carbon oxides. Sulfur oxides.5.3 Precautions for fire-fighters: Wear suitable protective clothing to prevent contact with skin and eyes and self-contained breathing apparatus.5.4 Further information: No data available.SECTION 6 - ACCIDENTAL RELEASE MEASURES6.1 Personal precautions, protective equipment and emergency procedures: Do not take action without suitable protective clothing - see section 8 of SDS. Evacuate personnel to safe areas. Ensure adequate ventilation. Avoid breathing vapors, mist, dust or gas.6.2 Environmental precautions: Do not let product enter drains.6.3 Methods and materials for containment and cleaning up: Cover spillage with suitable absorbent material. Using non-spark tools, sweep up material and place in an appropriate container. Decontaminate spill site with 10% caustic solution and ventilate area until after disposal is complete. Hold all material for appropriate disposal as described under section 13 of SDS.6.4 Reference to other sections: For required PPE see section 8. For disposal see section 13.SECTION 7 - HANDLING AND STORAGE7.1 Precautions for safe handling: Use in a chemical fume hood, with air supplied by an independent system. Avoid inhalation, contact with eyes, skin and clothing. Avoid the formation of dust and aerosols. Use in a well-ventilated area. Keep away from sources of ignition. Avoid prolonged or repeated exposure.7.2Conditions for safe storage, including any incompatibilities: Store in cool, well-ventilated area. Keep away from direct sunlight. Keep container tightly sealed until ready for use. Keep in a dry place.7.3 Specific end use(s): Use in a laboratory fume hood where possible. Refer to employer's COSHH risk assessment.SECTION 8 - EXPOSURE CONTROLS/PERSONAL PROTECTION8.1 Control parametersComponents with workplace control parameters: Contains no substances with occupational exposure limit values.8.2 Exposure Controlsi.Appropriate engineering controls: Use in a fume hood where applicable. Ensure all engineering measuresdescribed under section 7 of SDS are in place. Ensure laboratory is equipped with a safety shower and eye wash station.8.3 Personal protective equipmenti.Eye/face protection: Face shield and safety glasses Use equipment for eye protection tested and approved underappropriate government standards such as NIOSH (US) or EN 166(EU).ii.Skin protection: Wear appropriate protective eyeglasses or chemical safety goggles as described by OSHA's eye and face protection regulations in 29 CFR 1910.133 or European Standard EN166iii.Body Protection: Wear appropriate protective clothing. Complete suit protecting against chemicals, The type ofprotective equipment must be selected according to the concentration and amount of the dangerous substance at the specific workplace.iv.Respiratory Protection: Follow the OSHA respirator regulations found in 29 CFR 1910.134 or European Standard EN 149. Use a NIOSH/MSHA or European Standard EN149 approved respirator if exposure limits are exceeded or if irritation or other symptoms are experienced.v.Control of environmental exposure: Do not let product enter drainsSECTION 9 - PHYSICAL AND CHEMICAL PROPERTIESInformation on basic physical and chemical propertiesVapor Pressure No Data Available Appearance White To Off-WhiteSolidOdor No Data Available Vapor Density No Data Available Odor Threshold No Data Available Relative Density No Data AvailablepH No Data Available Water Solubility No Data Available Melting / Freezing Point No Data Available Partition Coefficient No Data Available Initial Boiling Point Range No Data Available Auto-Ignition Temperature No Data Available Flash Point No Data Available Decomposition Temperature No Data Available Evaporation Rate No Data Available Viscosity No Data Available Flammability (Solid, Gas)No Data Available Explosive Properties No Data Available Upper / Lower FlammabilityNo Data Available Oxidizing Properties No Data AvailableOr Explosive LimitsSECTION 10 - STABILITY AND REACTIVITYStability: Stable under recommended storage conditions.Hazardous Decomposition Products: None under normal use condition.Conditions to avoid: Light.Incompatibilities: strong oxidizing agent.SECTION 11 - TOXICOLOGICAL INFORMATIONAcute ToxicityLD50 Oral LD50 Dermal LD50 Inhalation LD50 Intraperitoneal 20,600 mg/kg (Rat)Not Listed Not Listed Not ListedSECTION 12 - ECOLOGICAL INFORMATIONEco Toxicity: No data availablePersistence and degradability/ Bioaccumlative potential/ Mobility in soil: No data availableResults of PBT and vPvB assessment: No data availableOther adverse effects: No data availableChronic Toxicity: There are no known carcinogenic chemicals in this productSECTION 13 - DISPOSAL CONSIDERATIONSWhatever cannot be saved for recovery or recycling should be managed in an appropriate and approved waste disposal facility. Processing, use or contamination of this product may change the waste management options. State and local disposal regulations may differ from federal disposal regulations. Dispose of container and unused contents in accordance with federal, state and local requirements.SECTION 14 - TRANSPORT INFORMATIONDOT TDG IATA IMDG/IMO Not regulated Not regulated Not regulated Not regulatedSECTION 15 - REGULATORY INFORMATIONINTERNATIONAL INVENTORIESTSCA DSL NDSL ELINCS NLP PICCS ENCS AICS CHINA KECL Listed Listed----Listed Listed Listed ListedUSA FEDERAL REGULATIONTSCA 12(b)/ OSHA/ CERCLA: Not ApplicableSARA 313: Not ApplicableClean Water Act/Clean Air Act: Not ApplicableSARA 311/312 HAZARDOUS CATEGORIZATIONAcute Health Hazard Chronic HealthHazardFire Hazard Sudden Release OfPressure HazardReactiveHazardNo Yes No No NoCalifornia Proposition 65: This product does not contain any Proposition 65 chemicals.HMIS RatingHealth hazard Chronic Health Hazard Flammability Physical Hazard 0000NFPA RatingHealth hazard Chronic Health Hazard Flammability Reactivity Hazard 0000STATE RIGHT TO KNOWMassachusetts New Jersey Pennsylvania Illinois Rhode Island -Listed Listed--US DEPARTMENT OF TRANSPORTATIONREPORTABLE QUANTITY (RQ)DOT MARINE POLLUTANT DOT SEVER MARINE POLLUTANT No No NoU.S. DEPARTMENT OF HOMELAND SECURITY: This product does not contain any DHS chemicals.Canada: This product has been classified in accordance with the hazard criteria of the Controlled Products Regulations (CPR) and the SDS contains all the information required by the CPR.This SDS complies with the requirements of Regulation (EC).SECTION 16 - OTHER INFORMATIONThe above information is believed to be correct but does not purport to be all inclusive and shall be used only as a guide. DOT SCIENTIFIC INC. shall not be held liable for any damage resulting from handling or from contact with the above product. See reverse side of invoice or packing slip for additional terms and conditions of sale. This product is sold for laboratory research and development purposes use only. REV October 2015。