File ..3\Data\20171109\20171109\BIZ2017-N08-WYQ7.D Tgt Mass (CHM): Injection Date : 9 Nov 17 12:06 pm +0800 Seq. Line : 37 Sample Name : BIZ2017-N08-WYQ7 Location : P1-B-03 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 10 ul
Acq. Method : D:\LCMS03\Data\20171109\20171109\1-POS-3MIN-(100-2000).M Analysis Method : D:\LCMS03\Data\20171109\20171109\1-POS-3MIN-(100-2000).M Catalog No : HY-P1229 Batch#27154
Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min
Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C
min
00.5
1 1.5
2 2.5mAU 0
5001000
DAD1 A, Sig=214,4 Ref=360,100
0.236
1.1961.259
1.367
1.604
1.7121.765
1.8401.889
2.009
2.1102.168
min
00.51
1.52
2.5mAU 0
20 DAD1 B, Sig=254,4 Ref=360,100min
00.51 1.52 2.5mV 0
500 ELS1 A, ELSD Signal 1.436
min
00.51 1.52 2.50
5000000
10000000 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 120
1.405
min
0.5
1
1.52
2.5-0.1
-0.0500.05 Ion 1, MSD1 1,Target Mass 0 +H Positive, EIC=0.7:1.7 Integration Results for DAD1 A, Sig=214,4 Ref=360,100
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.24 0.01 4.81 -0.69 0.11 235 1.20 0.02 73.28 68.58 1.67 136 1.26 0.01 0.92 1.20 0.02 136 1.37 0.05 4288.82 1461.30 98.01 1231 1.60 0.01 3.53 5.28 0.08 1231 1.71 0.01 2.14 2.52 0.05 258 1.76 0.01 0.50 -0.77 0.01 258 1.84 0.01 0.86 1.30 0.02 1231 1.89 0.01 0.19 0.43 0.00 1231 2.01 0.01 0.26 0.36 0.01 130 2.11 0.01 0.55 0.66 0.01 261 2.17 0.01 0.16 0.28 0.00 431
Integration Results for DAD1 B, Sig=254,4 Ref=360,100
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|
Integration Results for MSD1 TIC, MS File
RetTim Width Area Height Area% MS(+) |-------|--------|--------------|--------------|--------|------| 1.41 0.09 70202144.00 11544694.00 100.00 1231
Ret. Time: 1.41 <<<< POSITIVE SPECTRA >>>>
m/z
200
400
600
800
100012001400160018000
200000
4000006000008000001E61.2E6*ES-API Positive
923.5
1845.9
1230.9
*** End of Report ***